Escolar Documentos
Profissional Documentos
Cultura Documentos
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AMENDMENT RECORD
Clause
S.No. Nature of Amendment Date Authorisaton
Amended
1 Heading SP-DP12-0001(FE) changed to SP-FE-0001as per IMS requirement 30/11/2011 HOS
2 All Clause SOPs numbring system changed from three digit number to four digit number system. 30/11/2011 HOS
3 - Added two SOP-FE-2345 & 2346 with the price 30/11/2011 HOS
4 - Added Chlorate(ClO30) and Chorite(Cl20) to SOP-FE-1130 30/11/2011 HOS
5 Reference Change standard method 18th to 21 th 30/11/2011 HOS
6 All Clause Added Government cost to list 18/11/2012 HOS
7 - Added Physical analysis fees 18/11/2012 HOS
Test duration (days) modified from 4 to7 days increased in SOP-FE-3105. 18/11/2012 HOS
Eliminated salmonella spp by Rabit technique and added 10 or as per dilution factor to solid
18/11/2012 HOS
8 Part 1-FMAU part of SOP-FE-3117.
Modified tittle of two SOPs (3119 and 3120) 18/11/2012 HOS
Added three new SOPs-FE-(3122 &3123,3124) with the price in FMAU 18/11/2012 HOS
Test duration (days) incrased in Food chemical Analysis unit. Reference for
9 18/11/2012 HOS
SOPs(2260,2261,2262,& 2263) replaced AOAC, 17th Edn. 2000 to AOAC, 16th Edn. 1998
Part 2-FCAU
10 Added sSOP-FE-2324 & SOP-FE-(2265,2347) & BSEN 13805:2002 to list 18/11/2012 HOS
Standard methods- 21 ST Edition instead of 18 th edition and MOOPAM 4th instead of 3rd
22/11/2012 HOS
edition in Env list
Added two new SOPs-FE-(1132,1133,1134) with the price in Env.unit 22/11/2012 HOS
11 Part 3 -Env
Added method detection of Cu -Cd ,Zn , Pb,N i,Cr & modified test duration (days) from 4 to 5
22/11/2012 HOS
days incrased in SOP-FE-1304 in Env.unit.
Added SOP-FE-(1132,1133,1134,1135) with price in ENVU 22/11/2012 HOS
12 3.1 Added drinking water analysis with price in ENVU 22/11/2012 HOS
13 - Changed input time for Legionella from 2.2 to 2.30 hrs 22/11/2012 HOS
14 - Added remarks to list 22/11/2012 HOS
15 Discontinuation the production of KIT from company for SOP-FE-3119 20/01/2014 HOS
Part 1-FMAU
16 Added new SOP-FE-(3125,3126,3127,3128,3129) with the price of tests 20/01/2014 HOS
Added SOP-FE-2206 & Determination of traces elements of As*,Cd*,Hg*,Pb* by BS EN
17 15763:2009 with the price of tests
20/01/2014 HOS
Part 2-FCAU
18 Added new SOPs (SOP-FE-2370 & 2371) to list 20/01/2014 HOS
Method detection changed from 5 to 7,Changed reporting unit in SOP-FE-1124 from mg/l to
ug/L and removed waster water in sample type. Chaged method detection in SOP-FE-1128
19 Part 3 -Env z(Cd from 0.04 to 0.08,Zn from 0.04 to 0.05 ,Co from 0.1 to 0.12). Reduced method detection 20/01/2014 HOS
in SOP-FE-1130 for (BrO3 from 5 to 3). TDS / EC Meter replaced of APHA-2130B in SOP-
FE-1105 for drinking water. Added sampling with price to list.
Added new SOP-FE(3130 & 3131) with the price of tests and changed Test duation in
20 Part 1-FMAU 09/02/2015 HOS
Yersinia entrocolitica.
Adde methosd detedtion to SOPs and replaced SOP-FE-2230 by AAS to SOP-FE-2231 by
21 Part 2-FCAU ICPOES methods,added 3 SOP-FE-( 2231,2282,2372and 2392) to list.
09/02/2015 HOS
Changed the titles ,sample type and Duration time. Added Determination of salinity in water to
22 Part 3 -Env 09/02/2015 HOS
the list.
Recalculated cost as 20% discount of analysis for all types of foods,drining water, animal
23 All Clause 04/04/2016 HOS
feed and food supplement as per law no14 year 2009.
Added detection of pork and horse as per SOP-FE-3132 &3133 ,Removed Detection of
24 Pari 1-FMAU 04/04/2016 HOS
Cronobacter sakazakii in Powdered Infant Formula for liquid.
Added Determination of Acrylamide & NSAIDS as SOP-FE-2373 &2374, corrected
standard method & input time (hrs) in the BS EN 15763:2009,pestiside residues in the
25 Part2-FCAU 04/04/2016 HOS
different foods as SOP-FE-2348,2349,2350 ,Determination of Residual Monomers
Migration from Food Packging into Food as SOP-FE-2450.
Added Enumeration of Legionella spp. & L pneumophila in water and wastewater by
(RT-PCR) as SOP-FE-1610 & Determination of Volatile Organic Compounds in Water
26 Part 3 -ENVU as SOP-FE-1136 & 1137. 04/04/2016 HOS
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LIST OF ANALYSIS PARAMETERS WITH REFERENCE METHODS
Dubai Central laboratory Rev. No: 6
page :3 of 23
Doc.Ref : SP-FE-0001
Issue Date :04/04/2016
AMENDMENT RECORD
Clause
S.No. Nature of Amendment Date Authorisaton
Amended
REVIEW RECORD
Next Review
REVIEW DATE Outcome of Review Authorisation
Date
- 03/08/2009 -
-
18/10/2010 Reviewed no change required 18/10/2011 HOS
Associated Document
IMS-DP-12-Laboratory Work Operations
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Dubai Central laboratory
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Dubai Central laboratory
Doc.Ref : SP-FE-0001 Rev. No: 6
Detected or
FDA (BAM - 8thed.) Liquid Not Detected 1
Method for Isolation and in 25ml
Detection of Listeria FE-3111* 1 140 5
Species. Detected or
th
FDA (BAM - 8 ed.) Solid Not Detected 1
in 25gm
Detected or
FDA (BAM - 8thed.) Liquid Not Detected 1
Isolation of Thermophilic
in 25ml
Campylobacter species FE-3112 1.5 210 5
from Foods Detected or
th
FDA (BAM - 8 ed.) Solid Not Detected 1
in 25gm
Detected or
FDA (BAM - 8thed.) Liquid Not Detected 1
Isolation and Identification
in 25ml
of E.coli O157:H7 in FE-3113* 1.5 210 5
Detected or
Foods th
FDA (BAM - 8 ed.) Solid Not Detected 1
in 25gm
Detected or
FDA (BAM - 8thed.) Liquid Not Detected 1
Detection of Yersinia
in 25ml
entrocolitica in Food FE-3114 1 140 15
Samples Detected or
FDA (BAM - 8thed.) Solid Not Detected 1
in 25gm
Enumeration of
Pseudomonas aeruginosa
FE-3115* 1992 (APHA- 20thed.) Liquid cfu /250ml 1 0.5 70 4
and Pseudomonas species
in Food and water
Analysis of Food Samples
using Rapid Automated Don Whitley SC. 1997 Liquid cfu / ml 1
Bacterial Impedance FE-3117* 0.5 70 2
Technique (RABIT) - 10 or as per
(Enumeration of Mesophilic Don Whitley SC. 1997 Solid cfu / gm
dilution factor
Aerobic Colony Count /
Analysis of Food Samples
Don Whitley SC. 1997 Liquid cfu / ml 1
using Rapid Automated
Bacterial Impedance FE-3117* 0.5 70 2
Technique (RABIT) - 10 or as per
Don Whitley SC. 1997 Solid cfu / gm
(Enumeration of Coliforms) dilution factor
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Dubai Central laboratory
Doc.Ref : SP-FE-0001 Rev. No: 6
Detected or
Liquid Not Detected 1
Detection of Salmonella AOAC Official Method in 25ml
FE-3122* 2 280 2
species by Using BAX 2003.09 Detected or
Solid Not Detected 1
in 25gm
Analysis of Food using
petriflim method 3M USFDA- 8thed or AOAC Liquid cfu / ml 1
( Enumeration o f FE-3123* 0.5 70 2
Mesophilic Areobic Colony 10 or as per
USFDA- 8thed or AOAC Solid cfu / gm
Count / ACC) dilution factor
Detected or
USFDA- 8thed or AOAC Liquid not detected / 1
Analysis of Food using ml
petriflim method 3M (
Detection of E.coli Bacteria ) Detected or
USFDA- 8thed or AOAC Solid not detected / 1
FE-3123* gm 0.5 70 2
Detected or
Solid Not Detected 1
Detection of Listeria
AOAC Official Method in 25gm
monocytogenes in Food FE-3125* 2 280 2
2003.09 Detected or
using BAX System
Liquid Not Detected 1
in 25ml
Detected or
Solid Not Detected 1
Detection of Salmonella
AOAC Official Method in 25gm
spp. by VIDAS UP FE-3126* 2 280 2
2012.08 Detected or
Technique
Liquid Not Detected 1
in 25ml
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Dubai Central laboratory
Doc.Ref : SP-FE-0001 Rev. No: 6
Detected or
Solid Not Detected 1 ng
Detection of Bacterial Enter in 10gm
AOAC Official Method
Toxin in food Using FE-3127 2 280 2
993.06
TECRA Kit Method Detected or
Liquid Not Detected 1 ng
in 10ml
Detected or
Detection of Different Micro- Solid Not Detected 1
organisms by Using Bac in 25gm
SyLab Operation Manual
Trac Method FE-3128 1.5 210 2
BacTrac 4000 Series
(Detection of Salmonella Detected or
spp) Liquid Not Detected 1
in 25ml
Detected or
Solid Not Detected 1
in 25gm
Detection of E .coli
AOAC Official Method
O157:H7 in Food Using FE-3130* 2 280 2
2009.11
BAX System
Detected or
Liquid Not Detected 1
in 25lm
Detected or
Solid Not Detected 1
Detection of Cronobacter in 25gm
AOAC Official Method
sakazakii in Baby Food FE-3131* 2 280 2
2012
Using BAX System
Detected or
Liquid Not Detected 1
in 25 ml
PPM: Pour Plate Method. SPM: Spread Plate Method. MPN: Most Probable Number .
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Dubai Central laboratory
Doc.Ref : SP-FE-0001 Rev. No: 6
Determination of moisture /
AOAC , 17th Ed., (2000),
total solids in foods by FE-2205 Solid / Liquid % w/w 0.02 0.4 56 4
Gaithersburg, USA.
Vacuume -oven method
0.05 moisture
Determination of Moisture
0.3 fat
Fat Protein and ash by FT- FE-2206* AOAC, 17th Edn.2000 Solid / Liquid % 0.15 21 5
NIR 0.5 protein
0.1 Ash
Determination of Fat content
in Foods by Ammonia FE-2207 * AOAC, 17th Edn. 2000 Solid / Liquid %w/w 0.1 0.8 112 4
Digestion method
AOAC , 19 th Ed.,2012,
Determination of total
FE-2213* Gaithersburg, USA. 2. Solid / Liquid %w/w 0.05 0.3 42 3
acidity in foods
David Pearson, The
Chemical Analysis of
Foods, 7th Ed., 1976
Determination of pH of
FE-2214* APHA 4500 B-18th Edition Solid / Liquid - 0.1 0.3 42 2
foods
Fructose &
Determination of Sugars by Leatherhead Food RA, 2nd.,
FE-2216* Liquid %w/w Glucose 1% and 1.5 261 4
HPLC in Honey 1987
Sucrose 0.5%
Determination of reducing
sugar and sucrose by Lane AOAC, 15th Edn,1990, Solid / Liquid %w/w - 1.5 210 4
& Eynon's Journal of the Society of
Determination of Non FE-2217 Chemical Industry, by J.
reducing Lane and L. Eynon, 42, 325
AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 2.5 350 4
sugar(Sucrose),Titrimetric
method
Determination of Water-
FE-2218 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.2 168 4
Soluble Ash
Determination of Acid-
FE-2219 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.25 175 4
Insoluble Ash
Determination of Alkalinity
FE-2220 AOAC, 15th Edn. 1990 Solid / Liquid %w/w - 1.5 210 4
of Water-Soluble Ash
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Dubai Central laboratory
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Determination of water
FE-2222 AOAC, 17th Edn.2000 Solid / Liquid %w/w - 0.55 77 4
extract of tea and coffee
Determination of
Extraneous matter and FE-2224 AOAC, 17th Edn.2000 Solid %w/w - 0.5 70 3
defects in Food grains
Determination of stones
(seeds) and shell content in FE-2225 - Solid / Liquid %w/w - 0.5 70 3
fruits/dried fruits and nuts.
Determination of Salt
content in edible Salt and FE-2226 AOAC, 19th Ed ,2012 Solid / Liquid %w/w - 0.4 56 3
Foods
Determination of Drained
Weight in canned / Bottled FE-2228 - Solid / Liquid %w/w - 0.25 35 3
Foods
210 (Dhr)
Determination of Minerals for first
in Fortified Food Products J. of AOAC International, element, 32
FE-2231* Solid / Liquid mg/kg As per standard 1.5 210 5
by ICPOES after Microwave vol 95, No. 1, 2012 (Dhr) per
Digestion extra
element
Detection and
AOAC Official Method
Determination of Titanium FE-2232* Solid / Liquid mg/kg 10 1.5 210 5
973.36 (2012)
Dioxide in Food
Determination of Refractive
FE-2260* AOAC, 17th Edn. 2000 Solid / Liquid nD - 0.25 35 4
Index of Oils and Fats
Determination of Peroxide
FE-2262* AOAC, 19th Ed ,2012 Solid / Liquid mq/Kg 0.1 0.4 56 4
Value of Fats and Oils
Determination of Melting
FE-2263* AOAC, 17th Edn. 2000 Solid / Liquid °C - 0.5 70 4
Point of Fats
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Determination of Fatty Acid AOAC, 17th Edn. 2000 Solid / Liquid % 0.2 1 140 4
Profile of oils and fats,
omega fatty acids in FE-2264*
Journal of AOAC
selected foods and food
International,volume1 , Solid / Liquid % 0.2 1 140 4
supplements
2012. chapter 41, 27-28.
For one
Official Methods of AOAC vitamin 140
Determination of Water international, 19th Edition, AED and
Refer validation
Soluble Vitamins in Foods FE-2282* 2012 Solid / Liquid mg/kg 1 140 5 35AED for
procedure
and food supplements each
additional
vitamin
Identification of water
soluble Synthetic Colours in Pearson's Chemical Analysis
FE-2285 * Solid / Liquid - - 0.5 70 2
Foods by Paper of food, 7th Ed, 1976
Chromatography
Determination of Aflatoxins
0.3 for B1 & G1 /
(B1, B2, G1, G2) in foods FE-2320* AOAC, 17th Edn. 2000 Solid µg/kg 3.5 490 4
0.1 for B2 & G2
by HPLC method
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AOAC - BS EN
Determination of Patulin in
FE-2323 14177:2003 , BS EN Solid / Liquid µg/kg 1 3.5 490 5
Apple products
15890:2010
Determination of 1-AED:490
Mycotoxins indifferent food for one toxin
2-115 for
Commodities by Ultra- As per Annex-2
FE-2324* RCM-2009; 23:1801-1809 Solid µg/kg 3.5 490 7 each extra
Performance lquied of SOP toxins ( total
Chromatography and Tirple for 11 toxins
Quadrupole Detector 1755 Dh)
Determination of
Organochlorine and
As per
Organophosphorous FE-2342 AOAC,15th Edn,1990 Cereals & Dry foods mg/Kg 8 1120 7
Annex(III)of SOP
Pisticide Residue in Cereals
(NON-Fatty dry Foods)
Determination of N-
AOAC 90, No. 2, 2007 In 560 ( Dhr)
Methylcarbamatesin Fruits
house modified. Tripple for N-
and Vegetable Quenchers FE-2343 * Fruits & Vegetable mg/kg As per SOP 4 560 7
Quadrupole LC/MS System. Methylcarba
Technique using LC-
matesin only
MS/MS
Determination of
Organochlorine Pestiside Solid
AOAC,Vol.88, No 2,2005 As per Annex of
and Polychlorinated FE-2345* mg/kg 4 560 7
In house modified. SOP
Biphenyl Residue in Milk - Liquid
Quechers.
Multiresidue method for
analysis of pesticide residues
in fruits & Vegetables by
Acetonitrile extraction & AOAC,Vol.90, No 2,2007. As per Annex
FE-2346* Fruits & Vegetable mg/kg 8 1120 7
detection & GC- In house modified. ( I & II ) of SOP
ECD/NPD/MSD/PFPD
Detection -A QuEChERS
Approach
Determination of N-
Methylcarbamatesin Fruits
and Vegetable Quenchers
For SOP-
Technique using LC-
FE-2343
MS/MS and Multiresidue AOAC 90, No. 2, 2007;In
10 and As per (560 Dhr) +
method for analysis of FE-2343 * & house modified. Tripple
Fruits & Vegetable mg/kg Annex ( I &II) of 12 1680 7 SOP FE-
pesticide residues in fruits & FE-2346* Quadrupole LC/MS System. SOP 2346 (1120
Vegetables by Acetonitrile
(AED) =
extraction & detection &
1680
GC-ECD/NPD/MSD/PFPD
Detection -A QuEChERS
Approach
Multiresidue method for
analysis of pesticide residues
AOAC 90, No.2, 2007 In
in fruits & Vegetables by
house modified. Single
Acetonitrile extraction & FE-2347* Fruits & Vegetable mg/kg As per SOP 6.75 945 7
Quadrupole GC/MS
detection & GC-MSD
System.
Detection -A QuEChERS
Approach
AOAC Official Method
Analysis of Pesticide
2007.012. In house
Residues in Spices by
FE-2348* modified. Triple Spices mg/kg As per SOP 8 1120 7
Multiresidue Method -A
Quadrupole GC/MS
QuEChERS Approach
System.
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Dubai Central laboratory
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Detection of Tetracycline
arm II Test Operator’s
antibacterial in Raw Milk by FE-2361 Liquid µg / L _ 1.5 210 4
Manual for Tetracyclines
Charm II Test
Charm II Test
Detection of β-Lactams
TBL8MRL06,
Antibacterial in Raw Milk FE-2362 Liquid µg / L _ 1.5 210 4
Rev.November 2004
by CharmII Test
(Charm Sciences Inc.)
Detection of Macrolide
Antibacterial in Raw & Charm II Test Operator’s
FE-2364 Liquid µg / L _ 1.5 210 4
Pasteurized Milk By Charm Manual for Macrolides
II Test
Liquid µg /L
Determination of Analysis of veterinary drug
Sulfonamides & residues in shrimp, Journal As per Appendix-
FE-2369* 5 700 5
Trimethoprim in Milk and of Chromatography B, 836 2 of SOP
Tissues by LC-MSMS (2006) 22–3
Solid µg /L
Determination of
Antihelmintics- As per Appendix
FE-2372* Agilent Application Note Solid/Liquid µg/kg 5 700 5
Averrmectins- Residues in of SOP
Foods by LC-MSMS
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Determination of
NSAIDS(Non-Steroidal As per Appendix
Anti-Inflammatory Drugs) FE-2374 Anal. Biochem 2012 Solid/Liquid µg/kg 5 700 5
2 of SOP
Residues in Milk by
LCMSMS
Determination of 3-MCPD
FE-2391* AOAC, 17th End 2000 Liquid mg/Kg 0.03 6 840 5
in Soy Sauce by GC-MS
Determination of Polycyclic
BS EN ISO 25302 :2010. In
Aromatic Hydrocarbons in FE-2392* Solid / Liquid µg/kg Refer SOP 4.5 630 5
house modified.
Edible Oils and fats
Statutory Analysis
Determination of Sudan
Government Chemist
Dyes in Selected
FE-2400* Programme – LGC Limited Solid / Liquid mg / Kg 1 2 280 7
Spices/Condiments &
2006- Food Standards
Selected Foods
Agency - information
Hg 15
Pb 15
David Pearson, the
Chemical Analysis of Foods
Idenfication of
, 7th Edn, (1976),Churchill
Rhodamine B in Foods
FE-2403* Livingstone , Solid / Liquid mg/kg 2 0.5 70 3
by paper
Developments in food
Chromatography
colours, Vol I & II, Avi.
Publishers.
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Determination of Aflatoxins
0.3 for B1 & G1 /
(B1, B2, G1, G2) in foods FE-2320* AOAC, 17th Edn. 2000 Solid µg/kg 3.5 490 4
0.1 for B2 & G2
by HPLC method
Determination of 1-AED:490
Mycotoxins indifferent food for one toxin
2-115 for
Commodities by Ultra- As per Annex-2
FE-2324* RCM-2009; 23:1801-1809 Solid µg/kg 3.5 490 7 each extra
Performance lquied of SOP toxins ( total
Chromatography and Tirple for 11 toxins
Quadrupole Detector 1755 Dh)
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Water µS/cm 5 52 3
Determination of
FE-1102* APHA-2510 B Drinking water µS/cm 5 0.3 42 3
Conductivity in water
Determination of salinity in
FE-1102 Salinity meter Water / Waste water ppt 5 0.3 52 3
water
Drinking water 35 3
Determination of Total
Suspended Solids in water FE-1104 * APHA-2540 D Water / Waste water mg/L 11 0.6 104 5
and waste water
Water mg/L 10
FE-1105 * APHA-2540 C 0.6 104 5
Determination of Total Waste water mg/L 51
Dissolved Solids in water
and waste water
FE-1105 TDS / EC Meter Drinking water mg/L 5 0.6 84 5
Determination of Total
Solids in water and waste FE-1106 APHA-2540 B Water / Waste water mg/L 51 0.6 104 5
water
Determination of Acidity in
FE-1108 APHA-2310 B Water / Waste water mg/L 5 0.5 87 3
water and waste water
Determination of Alkalinity
FE-1109 APHA-2320 B Water / Waste water mg/L 5 0.5 87 3
in water and waste water
Determination of Nitrogen-
Ammonia in water and FE-1112 APHA-4500-NH3- B, C Water / Waste water mg/L 0.2 0.64 111 5
waste water
Determination of Nitrate-
Nitrogen in water FE-1113 APHA-4110 Water / Waste water mg/L 0.05 0.77 134 5
wastewater
Determination of Total T.R.Parsons 2.1, 1984,
FE-1115 Water / Waste water mg/L 0.13 0.9 157 5
Nitrogen APHA 4110 B
Determination of Total
FE-1116 APHA - 4500 - Norg B, C Water / Waste water mg/L 1 1.2 209 5
Kjeldahl Nitrogen
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Dubai Central laboratory
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Determination of Phosphate-
MOOPAM 4th ED. 3.2.8-A Water / Waste water mg/L 0.02 0.64 111 5
phosphorous
FE-1117
Determination of Total
Phosphorus in water/ waste APHA - 4500 - P (B, D) Water / Waste water mg/L 0.1 0.99 172 5
water
Determination of Sulfide FE-1120 APHA - 4500 S2- F Water / Waste water mg/L 1 0.5 87 5
Determination of
FE-1125 T.R.Parsons (4.1,4.2), 1984 Water mg/m3 0.5 1.2 209 5
Phytopigments
Determination of Cadmium
Water / Waste water mg/L 0.08
(Cd) *
Determination of
Water / Waste water mg/L 0.05
Manganese (Mn)* 87 AED for
one Element
Determination of Nickel & 44 AED
FE-1128 APHA - 3030 E, 3111 Water / Waste water mg/L 0.2 0.5 87 7
(Ni) * for each
extra
elements
Determination of Chromium
Water / Waste water mg/L 0.2
(Cr)*
Determination of Cobalt
Water / Waste water mg/L 0.12
(Co)*
Determination of Silver (Ag)* FE-1128 APHA - 3030 E, 3111 water / waste water mg/L 0.1 0.5 87 5
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Determination of Fluoride (
F)* in water by Ion Dionex manual water mg/L 0.1
chromatography
Determination of Chloride
(Cl)* in water by Ion Dionex manual water mg/L 0.1
chromatography
Determination of Nitrate
(NO3) * in water by Ion Dionex manual water mg/L 0.1
chromatography
Determination of Sulfate 131 AED
(SO4)*in water by Ion Dionex manual water mg/L 0.1 for one
chromatography Element &
FE-1130 0.75 131 5
Determination of Bromate 44 AED for
(BrO3)* in water by Ion Dionex manual water ug/L 3 each extra
chromatography elements,
Determination of Bromide
(Br)* in water by Ion Dionex manual water mg/L 0.1
chromatography
Determination of Chlorite
(ClO2)in water by Ion Dionex manual water ug/L 5
chromatography
Determination of
Chlorate(ClO3) in water by Dionex manual water ug/L 5
Ion chromatography
Determination of Chloride
(Cl)* in water by Ion Dionex manual Drinking water mg/L 0.1
chromatography
Determination of Nitrate
(NO3) * in water by Ion Dionex manual Drinking water mg/L 0.1
chromatography
Determination of Sulfate 105 AED
(SO4)*in water by Ion Dionex manual Drinking water mg/L 0.1 for one
chromatography Element &
FE-1130 0.75 105 5
Determination of Bromate 35 AED for
(BrO3)* in water by Ion Dionex manual Drinking water ug/L 3 each extra
chromatography elements,
Determination of Bromide
(Br)* in water by Ion Dionex manual Drinking water mg/L 0.1
chromatography
Determination of Chlorite
(ClO2)in water by Ion Dionex manual Drinking water ug/L 5
chromatography
Determination of
Chlorate(ClO3) in water by Dionex manual Drinking water ug/L 5
Ion chromatography
Determination of Heavy
Metals (Cu, Cd, Pb, Ni, Zn, as per each
APHA - 3030 E, 3120 Water / Waste water mg/L 131
Cr)* in water / waste water element
by ICP-OES
FE-1131 0.75 5
Determination of Metals
as per each
(Cu, Fe, Zn, Ca, Mg, Na)*in APHA - 3030 E, 3121 Drinking water mg/L 105
element
drinking water by ICP-OES
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water µg/L 5
Determination of Silver
(Ag*) by ICP-OES
Waste water mg/L 0.1
Determination of Arsenic
water / waste water µg/L 8
(As) by ICP-OES
Water µg/L 2
Determination of Cadmium
131 AED
(Cd*) by ICP-OES
for one
Waste water mg/L 0.05 Element &
FE-1131 APHA 3120 0.75 131 5
44 AED for
each extra
Water µg/L 2 elements
Determination of
Manganese (Mn*) by ICP-
OES
Waste water mg/L 0.1
Water µg/L 6
Determination of Lead (
Pb*) by ICP-OES
Waste water mg/L 0.1
Determination of Calcium
Water mg/L 0.05
(Ca*) by ICP OES
Determination of
Magnesium (Mg*) by ICP- water mg/L 0.05
OES
Determination of Zinc
Waste water mg/L 0.05
(Zn*) by ICP-OES
Determination of Nickel
Waste water mg/L 0.1
(Ni*) by ICP-OES
131 AED
Determination of for one
Chromium (Cr*) by ICP- Waste water mg/L 0.1 Element
OES 1131 APHA 3120 0.75 131 5 &44AED
for each
Determination of Copper
Waste water mg/L 0.05 extra
(Cu*) by ICP-OES
elements,
Determination of
Molybdenum (Mo) by ICP- water µg/L 10
OES
Determination of Sodium
water µg/L 10
(Na) by ICP-OES
Determination of
water µg/L 10
Barium(Ba) by ICP OES
Determination of
water µg/L 10
Potassium(K) by ICP OES
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Determination of Calcium
Drinking water mg/L 0.05
(Ca*) by ICP OES
Determination of
Magnesium (Mg*) by ICP- Drinking water mg/L 0.05
OES
Determination of Nickel
Drinking water µg/L 10
(Ni*) by ICP-OES
105 AED
Determination of Iron (Fe*) for one
Drinking water mg/L 0.05 Element
by ICP-OES
1131 APHA 3120 0.75 105 5 &35 AED
Determination of Zinc for each
Drinking water µg/L 10
(Zn*) by ICP-OES extra
Determination of elements,
Chromium (Cr*) by ICP- Drinking water µg/L 10
OES
Determination of Copper
Drinking water µg/L 10
(Cu*) by ICP-OES
Determination of
Molybdenum (Mo) by ICP- Drinking water µg/L 10
OES
Determination of Sodium
Drinking water µg/L 10
(Na) by ICP-OES
Determination of
Drinking water µg/L 10
Barium(Ba) by ICP OES
Determination of
Drinking water µg/L 10
Potassium(K) by ICP OES
Determination of Carbonate
and Bicarbonate in water FE-1134 AOAC 920.194 Water mg/L 5 0.5 87 3
by Titrimetry
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Determination of Volatile
Organic Compounds in
FE-1136 APHA 6200 B Drinking water ug/L As per SOP 7 890 7
Water with Headspace Trap
GCMS
Determination of total
organic carbon(TOC) in FE-1137 APHA - 5310 B water / waste water mg/L 1 1 174 5
water
Chemical analysis of
Determination of Moisture
FE-1301 polluted soils. EPA- Soil/ Sludge/Sediment % - 0.5 87 5
in Soil
Publication.139-4.
Determination of pH in
FE-1302 EPA-SW-846-9045 C Soil/ Sludge/Sediment - 1 to 14 0.5 87 5
Soil
Cu-4
Determination of Total Cd-2
Heavy Metals [Copper EPA-139-13
(Cu), Cadmium (Cd), Melbourne.1981, Soil / Sludge / Zn-4
FE-1304* mg/kg 2.1 585 10
Lead (Pb),Nickel MOOPAM 4th edition & Sediment Pb-15
(Ni),Zinc (Zn), Chromium APHA -3111
(Cr)] in Soil / Sediment Ni-16
Cr-9
Determination of Total th
MOOPAM 4 ED. Soil / Sludge /
Petroleum Hydrocarbons in FE-1305 mg/Kg 0.2 2.1 365 7
–Section 6.7, 6.9 Sediment
Soil
Determination of Oil and Soil / Sludge /
FE-1306 APHA - 5520 E mg/kg ** 1.1 191 7
Grease in Soil / Sludge Sediment
Determination of Sludge- Soil / Sludge /
FE-1307 DM, EPSS TG-No-43 mg/L - 4.55 792 7
Leachate test Sediment
Determination of Heavy
Metals [Copper (Cu), MOOPAM 4th ED. - Section Fish / Biological
FE-1401 mg/g ** 2.1 497 10
Cadmium (Cd), Lead (Pb), 5.3, 5.4 Sample
Zinc (Zn) ] in fish
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Determination of Heavy
Metals [Copper (Cu), MOOPAM 4th ED. - Section Fish / Biological
FE-1401 mg/g ** 2.1 497 10
Cadmium (Cd), Lead (Pb), 5.3, 5.4 Sample
Zinc (Zn) ] in fish
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1Hr 174
3 Hr 522
** The method detection limit will be calculated during the analysis depending on the
type and weight of sample.
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TECHICAL APPOVALS
This procedure was Prepared, Reviewed and Approved for technical content by the following Staff:
Prepared By:
2 Dr.Alamuri Gopalakrishnamacharyulu -
Reviewed By:
Approved By HOUs( Food Chemical Analysis , Food Microbiology Analysis and Environment Unit)
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