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SAE TECHNICAL
PAPER SERIES 982673

Shear Stability of Automatic Transmission


Fluids -- Methods and Analysis
A Study by the International Lubricants
Standardization and Approval
Committee (ILSAC) ATF Subcommittee
Joseph W. Spry!; Nobuyoshi Hoshikawa James L. Linden
Ford Motor Company Fuji Heavy Industry Co. General Motors

Jyunichi Doi Tracey King Yasuhiro Murakami


Mazada Motor Co. Chrysler Corporation Mitsubishi Motors

Mitsumasa Furumoto Hideo Kurashina Fumio Ueda


Honda Research and Development Co.Mitsubishi Motors Corp. Toyota Motor Company

Reprinted From: Automatic Transmission Fluids (ATF)


(SP-1394)

mA E The Engineering Society International Fall Fuels and Lubricants


For Advancing Mobility
Land Sea Air and Space, Meeting and Exposition
I N T E R N A T I O N A L San Francisco, California
October 19.22,1998

400 Commonwealth Drive, Warrendale, PA 15096-0001 U.S.A. Tel: (724) 776-4841 Fax: (724) 776-5760
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982673
Shear Stability o.f Automatic Transmission Fluids -- Methods and Analysis
A Study by the International Lubricants Standardization and Approval
Committee (ILSAC) ATF Subcommittee

Joseph W. Sprys Hideo Kurashina


Ford Motor Company Honda Research and Development Company

Jyunichi Doi James Linden


Mazda Motors Company General Motors Research and Development Center

Mitsumasa Furumoto Yasuhiro Murakami


Honda Research and Development Company Nissan Motors Company

Nobuyoshi Hoshikawa Fumio Ueda


Fuji Heavy Industry Company Toyota Motor Company

Tracey King
Chrysler Corporation

Copyright 0 1998 Society of Automotive Engineers, Inc.

ABSTRACT adequate performance in vehicle systems used in automobiles


and other transportation equipment.
This paper discusses four methods for measuring the
To obtain optimum transmission performance over a wide
resistance of transmission fluids to permanent viscosity loss
operating temperature range, transmission fluids must be
through shear. The four methods include the Fuel Injector
blended to have good low temperature fluidity as well as
Shear Stability test, the Sonic shear test, the DEXRONB-III adequate fluid viscosity at high temperatures. The most
Cycling test and the KRL test. Each of these methods and their common method of obtaining this viscosity-temperature
advantages are discussed and data provided for many OEM relationship is to use relatively low viscosity base oil for low
fluids and the effects of these methods on the final viscosity. temperature performance and then add viscosity modifiers,
The data indicates the KRL generates the maximum shear often referred to as viscosity index improvers (VII) to enhance
stress on the fluids compared to the other methods. The data the viscosity at elevated temperatures. Viscosity modifiers,
also indicates the sonic shear method results are similar to typically long chain polymeric materials, are added to increase
those of the KRL test. The fuel injector test imparts the least the viscosity at elevated temperatures. Additionally, to
stress to the fluid. Data is presented to show the correlation enhance the overall performance characteristics of the base
between viscosity changes obtained using these methods and oils, additive treatments have been developed, which improve
viscosity changes observed with mileage accumulation in the anti-wear, the anti-foaming, the friction modification and
vehicle transmissions. the oxidation resistance characteristics of the fluid.

INTRODUCTION Each base oil has its own viscosity vs. temperature pattern that
needs to be altered to provide optimum fluidity as the
operating environment changes. As transmission performance
Transmission fluids are composed of two major constituents:
operating conditions have been expanded to include a wide
basestock and additives. The basestocks are typically mineral
range of operating temperatures and with the incorporation of
oils from refined crudes but can also be produced either from
electronic controls, automatic transmission fluids (ATF’s)
100% synthetic materials or mixes of synthetic and mineral
have been required to exhibit better low-temperature fluidity
oils. The mineral oil crude sources come from various parts of
while providing adequate high temperature viscosity (I)
the world and are refined in many places. The refining process
These requirements have typically been met through the use of
of these crudes has been developed over the years and
viscosity modifiers. In conjunction with lower viscosity base
includes various techniques such as solvent refining,
oils these viscosity modifiers provide the viscosity
hydrotreating and hydrocracking. Each process produces a
requirements needed m today’s automatic transmissions.
certain quality of basestock that can be used as a basis for
lubricant development. Because of the molecular construction Shear stability refers to retention of viscosity of a fluid in any
of these basestocks the molecules do not provide the desired mechanical system and is important for the life of the
characteristics needed for proper lubrication under all components that make up that system. During the operation of
circumstances. The basestocks impart the low temperature a transmission, the fluid experiences high shear stresses during
fluidity and oxidation resistance characteristics of lubricants. flow between components such as the pump, friction clutches,
Unfortunately these characteristics alone are insufficient for hydraulic and electronic valves, planetary gear sets, and

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bushings. The high molecular weight components undergo 5. Show very good correlation to actual vehicle performance
chain scission, which fractures the long chain molecules and data
changes the viscosity of the fluid. 6. Be accurate for many different types of transmission
Application of the correct method of stressing the fluid in designs
bench tests to determine the effect on viscosity is important 7. Be developed on equipment that is available worldwide
for the development of new fluids and to ensure that sufficient
stress has been applied during the test to properly simulate that In our efforts to evaluate test procedures and equipment that
effects of transmission operation. The development of the will meet these criteria four techniques have been tested. Each
correct bench tests also allows effects of stress to be evaluated technique has been tried on samples representing typical
at a much less costly method than using vehicle tests. factory fill fluids used either by JAMA or AAMA. This paper
also provides a status report ‘of this work in progress.

SHEAR STABILITY MEASUREMENT TECHNIQUES

Four bench techniques for degrading transmission fluids were


investigated (2-5). These are::
1. FISST ( Fuel Injector Shear Stability Test)
2. Sonic Shear Test
3. DEXRONB-III Cycling Test
4. KRL Tapered Roller Bearing Test

Details of each procedure are shown in Table 1. Each of the


individual techniques will be described and results will be
presented which show the comparison of the viscosity changes
generated by the individual test method to the viscosity
changes obtained from vehicles with various mileages. In the
conclusion of the paper, an overall comparison of the
techniques and discussion will be presented.

TABLE 1: COMPARISON OF SHEAR STABILITY TESTS


FIGURE 1. Effects of Poor Shear Stable Fluids on
Transmission Performance.

SHEAR TEST TECHNIQUES

The viscosity of transmission fluid plays a critical part in the


20.9 534 mL/min
performance of all systems. It is responsible for maintaining Amounl of Fluid 100 mL 30mL 11 L 40 mL
fluid film thickness to prevent contact of sliding or moving Flu Id ‘Tern pcrnutc
Test Duration
30-3s “C
20 Cycles
40 T
6 0 mtn
130 “C S u m p
20.000 cyclcr O”Cr
6 0 “C
1740): r~v~l~t~~ns
components, for assisting in maintaining pump capacity as I 222 HIS over 20 Hrs
Typlcnl User Ford Japanrrc GM M erccdcr
temperatures of operating systems increases and for iMERCON VI OEM’S VW.ZF

maintaining its properties when exposed to severe shear


environments. For the development of new transmission fluids 516 Tbi,
techniques need to be developed and evaluated to properly test
the fluid viscosity resistance to changes. These techniques Note on viscosity plots: Since the times to degrade the
must show a good correlation to the viscosity changes
various fluids with these techniques is a variable controlled by
experienced by the fluids in the transmissions under customer
the shear stresses imposed by the method, the horizontal axis
operating conditions. labels are variable for each data figure. In certain instances the
The selection of the proper laboratory technique to degrade horizontal axis is adjusted to make the viscosity resulting from
fluids to match the viscosity degradation found in the technique match the viscosity of the fluids from the
transmissions has been one of the many efforts expended vehicles. In all cases the horizontal axis conditions will be
within the ILSAC community. Techniques evaluated had to at indicated for ease of understanding. The fluids used in this
least meet the following criteria: report are a series of reference fluids provided by members of
the team. In most cases the fluids provided are OEM factory
1. Preferably require small sarnple size fill fluids and they are identified as fluids A through E.
2. Produce statistically repeatable results
3. Degrade the fluid in a reasonable time period
4. Be able to degrade fluids at different temperatures
Fuel Injector Shear Stability Test (FISST,
ASTM D 3945)

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Description and Test Procedure

This test, first introduced in 1980, was developed through the


ASTM Committee on Petroleum Products and Lubricants. The
test is one of two procedures, procedure A and procedure B,
included in the ASTM D 3945 - 80, titled, “Shear Stability of
Polymer-Containing Fluids Using a .Diesel Injector Nozzle”.
Test Procedure A is identified as the “European Diesel
Injector Test” and Procedure B is identified as the “Fuel
I I /
Injector Shear Stability Test (FISST:l. The first test procedure ! I
was not evaluated for this program and will not be discussed I
further. 0 20 40 60 80 loo 120

flSST Passes
Nozzle Holder
+ I
Figure 3A: Viscosity Changes with FISST Passes - Fluid B
Viscosity measurement were also made of fluid B removed
from transmissions with different kilometer accumulations to
Lower
establish whether a correlation exists between the viscosity
Reservoir changes produced by FISST and those produced by action of
passage through the vehicle components. The viscosity of
+
Drain fluids was measured after accumulations of up to 100,000
miles (62500 Kilometers). The results of the viscosity
measurement of fluid from vehicles are reported as Figure 3B.

Figure 2: Schematic of the FISST Apparatus

A schematic of the test apparatus for the FISST is shown in


Figure 2. The fluid is introduced into the device through a ii4
% I
pump and repeatedly forced through the fuel injector until a
specified number of passes have been completed. The fluid is -5 2 f
then drained from the apparatus throu.gh the solenoid drain ii
.- I
> *
valve and its kinematic viscosity measured. 0 20000 40000 60000 80000 100000
The injector design and details are provided in the ASTM Vehicle Mileage
Specification D-4983 and are not repeated here. The
clearances of the injector are adjusted to a preset level using
the shearing of a reference fluid by passage through the
system a preset number of times at controlled temperature and Figure 3B: Viscosity Changes with Vehicle Mileage - Fluid B
pressure. The viscosity is then measured and must fall within In this instance it is evident that the viscosity of fluid degraded
set parameters for the reference fluid. The performance by FISST at 20 passes matches the viscosity of the fluid from
characteristics of the injector equipment having been verified vehicles using Fluid B after 5,000 miles (3125Km). We can
the fluid whose shear resistance is to be measured is then put also say that FISST at 20 passes using Fluid B matches the
through the injector for a prearranged number of passes. The viscosity of the fluid from vehicles at 5,000 miles (3125Km).
fluid viscosity is then measured and reported as a function of
FISST passes. The identification of the reference fluids and Based on 20 passes as a good correlation point between the
the repeatability and reproducibility parameters of the test FISST results and the vehicle performance results, this number
results are provided in the ASTM specification. of passes was applied to other reference fluids supplied by
ILSAC members. The fluid viscosity for these fluids are all
reported in Table 2 and indicate that several fluids exhibit
Results shear degradation after 20 passes through the injector while
others show little or no effect.
Fluid B was investigated by one OEM using this technique.
The fluid was subjected to many passes through the FISST
and the viscosity changes as a function of those passes plotted
on figure 3A.

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the fluid held at a specified temperature and time. The


Table 2. Viscosity losses of 5 ILSAC fluids after 20 pass viscosity at 100°C is measured and reported after testing.
FISST Some details of the device and the operating parameters are
~~ shown in Figures 5.
Kinematic Viscosity at 100°C, cSt

Unused After 20 passes Viscosity Loss %


Fluid A 7.655 7.54 4.12
Fluid B 7.68 5.88 23.42
Fluid C 7.39 7.:36 0.40
Fluid D 7.53 6.03 19.92
Fluid E 7.68 5.69 25.91

Fluid B and C have been evaluated in vehicles and the


I I I I I I
viscosity plotted simultaneously with the viscosity changes
noted after FISST in Figure 4. ‘The correlation between the
FISST and the vehicle performance with Fluid B is very good.
There, however, is no correlation between the FISST and the Figure 5. Sonic Shear Stability Test Device (Schematic)
vehicle viscosity changes for Fluid C. Fluid C is not The JASO specification used for this procedure is identified as
sufficiently stressed by the process. JASO M347-95. The system is calibrated using a reference
fluid that must undergo a 30% viscosity reduction at 100°C
8 within 10 minutes. When the reference fluid has been placed
in the beaker surrounded by cooling water at 40°C, it is
7.5 7 radiated for 1 hour and checked for viscosity loss. When the
Ll
system has been stabilized to reduce the standard viscosity
sample by 30% the system is ready to receive the candidate.
The candidate fluid is placed in the cleaned beaker and cooled
as the standard fluid. The oscillator cone is positioned above
the fluid sample and the oscillator is started for 60 minutes.
The sample is then removed and its kinematic viscosity
measured at 100°C. The % viscosity loss is calculated and
reported. The ILSAC reference fluids were examined using
this device and the results are reported in Table 3.

Table 3. Viscosity Loss Measured After Sonic Shear


Testing

Kinematic Viscosity at l.OO°C, cSt

Unused After Sonic Test Viscosity Loss, %


Figure 4. The Relationship of Vehicle Kilometers to Number Fluid A 7.55 6.80 9.9
of FISST Passes for Fluid B and Fluid C Fluid B 7.89 5.22 33.8
Fluid C 7.47 7.09 5.1
Sonic Shear Test Fluid D 7.11 5.29 25.6
Fluid E 7,97 4,78 40.0
Description and Test Procedure

The FISST requires that the fluid being degraded come in


contact with the parts of the devices that are shearing the Results
additive components. A second shear-generating device has
been developed and it too has been derived from an ASTM In addition to the standard one-hour test from which the data
procedure. This technique uses acoustic emissions to alter the in Table 3 are obtained, two of the ILSAC fluids, A and C,
molecular weights of the additive system components and were subjected to extended Sonic Shear Tests of 3,5 and 10
therefore change the viscosity of the fluid. Sound waves of a hours. The viscosity loss data from the extended tests are
specific energy and frequency are directed into a container of compared to viscosity loss data for those same fluids after

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vehicle test. The comparison is shown in Figure 6. The data


indicates a good correlation between the Sonic test and the
vehicle tests. There is no comparison of viscosity data after 10
hours which corresponds to viscosity changes measured at
55,000 kilometers.

50,000 100,000
VehicleDistance in Kilometers

Fluid A Fluid C Sonic -Fluid A Sonic - Fluid C


-a-- + -.+..-
Figure 7. Cycling Test Apparatus

Figure 6. Viscosity of ILSAC Fluid A and C as Function of


Vehicle Kilometers and After Sonic Shear Hours The results from the cycling test are plotted against vehicle
kilometers for IISAC reference fluids A and E are shown in
figure 8. The results indicate good correlation between the
DEXRON@lII Cycling Test vehicle kilometers and the cycling test for approximately
10,000 kilometers. As the test progresses, used oil viscosity
Description and Test Procedure begins to increase as previously mentioned. Thus the cycling
test correlation with the vehicle distance in kilometers is not
The DEXRON III cycling test incorporates the use of an very good at high kilometers.
operational transmission driven by an automotive engine
similar to that seen in figure 7. Two major components of the
assembly (the engine and transmission) can be seen in the
photograph. The cycling test consists of 20,000 cycles, each
about 45 seconds in duration, using forty percent throttle
accelerations through 1-2,2-3,and 3-4 shifts. The transmission
test begins with a complete rebuilt transmission, new friction
material and fresh fluid. Fluid samples are removed from the
transmission at 5000 cycle intervals and the viscosity
measured at 40°C and 100°C. The cycling test primarily
evaluates friction characteristics, but includes requirements of
fluid viscosity as well as fluid effects on overall transmission
performance. Since the cycling test evaluates fluid shear
stability in an operating transmission, it should be the best
indicator of fluid shear stability in actual vehicle use.
However, because the cycling test is conducted at sump fluid I I I i
44
temperature of 130°C, fluid oxidation results in fluid
0
thickening as the test progresses so that the fluid viscosity may
never reach the lowest possible sheared viscosity. In addition
to the high test temperature drawbaclc to the cycling test, two
other factors preclude the use of the cycling test as a “bench- I -+-MA +-R.idE +-FWA-qdpg +WdE-qdirg
type” shear stability test. Those factors are the time involved
to run the test, about 222 hours, and the high cost of the test. Figure 8. Comparison of viscosity of fluids tested in cycling
test vs viscosity of fluids from vehicle used in field.

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Table 4. Viscosity Loss Measured After Cycling Test Table 5. Shear stability changes after KRL test.

Kinematic Viscosity at 100°C, cSt Kinematic Visocisity at 100°C, cSt

Unused After 20k cycles Viscosity Loss % Unused After 20 hrs KRL Viscosity Loss %
Fluid A 7.51 7.13 5 Fluid A 7.51 6.36 15
Fluid C 7.49 7.41 1 Fluid B 7.88 5.017 36
Fluid E 7.85 5.50 30 Fluid C 7.49 6.58 12
Fluid D 7.35 4.93 33
Fluid E 7.85 4.55 42

KRL Tapered Roller Bearing Test


reported above and are reported in Table 5. Fluid C shows the
Description and Test Procedure greatest resistance to shear using this method with Fluid A
showing the second best resistance.

The KRL device uses a tapered bearing driven by a Shell 4-


ball tester which continually passes fluid through the roller
surfaces and the inner and outer race of a tapered roller
bearing. The test bearing is totally immersed in the fluid to be
tested. The test is conducted at 160°C under a constant load of
5000 N for fixed numbers of revolutions. High stresses,
created between the rolling mernbers of the bearing and the
races, shear the molecules and reduce the viscosity of the
fluid. The fluid kinematic viscosity is measured before and
after the test to determine the arnount of permanent
degradation. Details of the test can be found in the DIN
specification DIN 5 l-350 and are not reported here. The
length of time for the test can be set at one of three options of
4, 8 or 20 hours. The 20-hour test time was chosen for this
test and it is equivalent to 1,740,OOO revolutions of the motor.
The viscosity of the degraded fluid is obtained at 100°C and
+ R&A +RudE +RudA-KFL x FkidE-IR
the relative viscosity decrease can be reported as percentage
loss from the original sample. The repeatability and
reproducibility are indicated in the specification.
Figure 10. Chart showing viscosity changes of fluids from
vehicles and corresponding viscosity changes after 20 hours
KRL.

The sheared viscosity of ILSAC Reference Fluids A and E


after 20 hours in the KRL are placed on the plot of the
viscosity data from the vehicles as a function of kilometers.
The points at which the KRL viscosity data matches the
vehicle viscosity data, a correlation is said to be established..
This is shown in Figure 10 for these two fluids.

Discussion:

Four different methods of degrading transmissions fluids have


been presented. Each in order of presentation represents
improvement in the capabilities to degrade very shear stable
fluids as well as match viscosity changes noted in fluids
removed from customer vehicles.
FISST. This report indicates that this test is adequate for
Figure 9. Schematic of KRL App$a.ratus fluids with non-shear resistant or easily sheared additives but
provides insufficient stresses to degrade more stable fluid

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additives. The fuel injector set up as used in this test


procedure, however, is inadequate for fluids such as Fluid C. 2. The SONIC shear test is adequate for more shear stable
Regardless of the number of passes through the injectors no fluids than FISST but still is not capable for some very
measurable effect on the viscosity was evident. Adjustments stable fluids.
may be made to the nozzle geometry to increase the shear
stresses imposed on fluids passing through the injector but no 3. The DEXRONB -111 Cycling Test is better than the
experiments were conducted to determine their effect. One FISST but requires a substantial investment in equipment,
advantage of this test is that all the fluid passes through the and takes a significantly longer time to run.
injector orifice and is subjected to the same shear stresses as
any other part of the fluid. This may not be the case in the 4. The KRL test is able to reduce viscosity of all fluids
other techniques discussed in this paper. tested, including the most shear stable.

5. Extended length Sonic Shear test results match those


Sonic Shear Tests: The sonic shear test imparts a more
obtained with the KRL.
severe stress to the fluids. The intensity of the sonic waves
generated in the apparatus has been found adequate to change
6. The KRL data is easily correlated to vehicle viscosity
the viscosity of Fluid A and C whereas little effect was
changes regardless of vehicle type and will be the most
observed on these fluids when tested using the FISST
probable method of choice for future shear stability tests
procedure. Fluid B, D and E have similarly undergone a
for ILSAC members companies
further reduction of viscosity than with the FISST using this
method. As was noted with the former method, no tests were
conducted to determine if the test procedure could be changed
References:
by increased intensity of the sonic wa.ves. The advantages of
using the sonic shear test include small sample size and
1. J.L. Linden, S.P. Kemp, “Improved Transaxle
sufficient stress to degrade fluids not affected by the FISST.
Performance at Low Temperature with Reduced Viscosity
DEXRON@ III Cycling Test: The: cycling test has an Automatic Transmission Fluids”, SAE Paper 870356
advantage over the other tests discussed in that it is performed
in a functioning transmission operation driven by an engine. It 2. MERCON Automatic Transmission Fluid Specification,
provides a direct measurement of viscosity loss with cycles of available form Ford Motor Company, Livonia MI 48 15 1
the transmission while the test is being conducted. All the
other techniques require that samples be removed from 3. DEXRON -111 Automatic Transmission Fluid
vehicles to determine viscosity change correlation between the Specification, GM-6297M, available form GM ATF
vehicles and the test apparatus. However because this test is Committee, GM Global Research and Development
run at 130°C, fluid oxidation and the resultant thickening can Center, M/C 480-106-160, Warren, MI 48090, April 1993
mask the shear stability (or lack of) of the test fluid.
Disadvantages of the Cycling Test over other test methods are 4. JASO Test Method 348-95, Japanese Automobile
the volume of fluid required, the cost of required equipment to Standard Test Method for Friction Properties of
perform the test, and time to complete the test. Automatic Transmission Fluids, available from Japanese
Automobile Manufacturers Association, Tokyo, Japan
KRL Tapered Roller Bearing Test: The KRL test provides 5. CEC Test Method CEC L-45-T-93 - Viscosity Shear
the greatest shear stresses to any fluid. investigated., This Stability of Transmission Lubricants (KRL-Tapered
procedure is capable of degrading the most shear stable fluid Roller Bearing Test Rig) Shear Stability Test, 1993,
available. The KRL test is relatively easy to perform. Since Available from Coordinating European Council, Madou
the KRL is capable of shearing the most stable of fluids in a Plaza - 25* Floor , Place Madou 1 B-1030 Brussels,
bench test guarantees that it can provide a relationship to shear Belgium
degradation measured for any vehicle as a function of usage.

CONCLUSION ACKNOWLEDGEMENTS
Although many techniques are available for evaluating the The authors wish to recognize the efforts of the AAMA and
shear stabililty of transmission fluids, the KRL test procedure the JAMA staff for keeping the information flowing between
is the most acceptable. It requires a small volume of oil, is the two committees and for their patience while we conducted
capable of being used at high temperatures, is capable of the necessary work of ILSAC. We particularly wish to thank
shearing the most shear stable fluid available and is becoming Mr. James Steiger of AAMA and Mr. Hirokazu Furukawa of
more widely used. Of the 5 fluids examined Fluid C was JAMA.
found to be the most shear stable.

1. FISST is not able to shear very stable fluids although it


may reduce viscosity to match field performance with
some non-shear stable fluids.

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