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OBJETIVO

- Determinar la intensidad y comparar con la intensidad calculada.

𝒉𝟐 + 𝒌𝟐 𝐬𝐢𝐧 𝜽
Línea hkl + 𝒍𝟐 𝐬𝐢𝐧 𝜽𝟐
𝐬𝐢𝐧 𝜽 𝜽 𝝀
1 100 1 0.055 0.235 13.6 0.152
2 110 2 0.084 0.289 16.8 0.187
3 111 3 0.118 0.343 20.1 0.223
4 200 4 0.197 0.444 26.4 0.288
5 211 6 0.271 0.521 31.4 0.338
6 211 6 0.281 0.530 32.0 0.344
7 -- 7 0.306 0.553 33.6 0.359
8 300,221 9 0.398 0.631 39.1 0.409
9 300,221 9 0.403 0.635 39.4 0.412
10 310 10 0.448 0.669 42.0 0.434
11 222 12 0.545 0.738 47.6 0.479
12 320 13 0.578 0.760 49.5 0.493
13 320 13 0.579 0.761 49.6 0.493
14 321 14 0.635 0.797 52.8 0.517
15 321 14 0.654 0.809 54.0 0.524
16 400 16 0.708 0.842 57.3 0.546
17 411,330 18 0.801 0.895 63.5 0.580
18 411,330 18 0.833 0.913 65.9 0.592
19 331 19 0.882 0.939 69.9 0.609
20 420 20 0.888 0.942 70.4 0.611
21 420 20 0.929 0.964 74.6 0.625
22 421 21 0.935 0.967 75.2 0.627
23 421 21 0.947 0.973 76.7 0.631
24 421 21 0.952 0.976 77.4 0.633
Hallamos el factor de polarización.

- Para ello hallamos la función con los valores de la tabla 9.8.

35
29
factor de polarizacion

30 25.9
25 21.6
17.9
20 15.2
13.3
15 11.7 10.2
10
5 y = -138.89x6 + 721.15x5 - 1182.2x4 + 836.84x3 - 238.27x2 - 14.449x + 29
0
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8
𝐬𝐢𝐧𝜽/𝝀

𝐬𝐢𝐧 𝜽
Línea hkl 𝒉𝟐 + 𝒌𝟐 + 𝒍𝟐 𝐬𝐢𝐧 𝜽𝟐 𝐬𝐢𝐧 𝜽 𝜽 𝝀 f
1 100 1 0.055 0.235 13.6 0.152 23.6
2 110 2 0.084 0.289 16.8 0.187 22.1
3 111 3 0.118 0.343 20.1 0.223 20.7
4 200 4 0.197 0.444 26.4 0.288 18.3
5 211 6 0.271 0.521 31.4 0.338 16.8
6 211 6 0.281 0.530 32.0 0.344 16.6
7 -- 7 0.306 0.553 33.6 0.359 16.2
8 300,221 9 0.398 0.631 39.1 0.409 15.0
9 300,221 9 0.403 0.635 39.4 0.412 15.0
10 310 10 0.448 0.669 42.0 0.434 14.5
11 222 12 0.545 0.738 47.6 0.479 13.7
12 320 13 0.578 0.760 49.5 0.493 13.4
13 320 13 0.579 0.761 49.6 0.493 13.4
14 321 14 0.635 0.797 52.8 0.517 13.0
15 321 14 0.654 0.809 54.0 0.524 12.9
16 400 16 0.708 0.842 57.3 0.546 12.5
17 411,330 18 0.801 0.895 63.5 0.580 12.0
18 411,330 18 0.833 0.913 65.9 0.592 11.8
19 331 19 0.882 0.939 69.9 0.609 11.6
20 420 20 0.888 0.942 70.4 0.611 11.5
21 420 20 0.929 0.964 74.6 0.625 11.3
22 421 21 0.935 0.967 75.2 0.627 11.3
23 421 21 0.947 0.973 76.7 0.631 11.2
24 421 21 0.952 0.976 77.4 0.633 11.2

- Luego hallaremos el factor de estructura (F) , como la celda unidad es simple entonces

f = F, también hallamos el factor de multiplicidad de la tabla 9.9 y factor de polarización lorentz de la tabla
9.10.
𝒉𝟐 + 𝒌𝟐 𝐬𝐢𝐧 𝜽 Factor Polarización-
Línea hkl + 𝒍𝟐 𝐬𝐢𝐧 𝜽𝟐 𝐬𝐢𝐧 𝜽 𝜽 𝝀 f 𝑭𝟐 P Lorentz INTENSIDAD(𝟏𝟎𝟓 )
1 100 1 0.055 0.235 13.6 0.152 23.6 558.9 6 33.33 1.12
2 110 2 0.084 0.289 16.8 0.187 22.1 489.9 12 21.18 1.25
3 111 3 0.118 0.343 20.1 0.223 20.7 427.8 8 14.28 0.49
4 200 4 0.197 0.444 26.4 0.288 18.3 334.4 6 7.711 0.15
5 211 6 0.271 0.521 31.4 0.338 16.8 280.8 24 5.218 0.35
6 211 6 0.281 0.530 32.0 0.344 16.6 275.5 24 5.006 0.33
7 7 0.306 0.553 33.6 0.359 0 0 - - 0
8 300,221 9 0.398 0.631 39.1 0.409 15.0 225.3 6 24 3.375 0.05 0.18
9 300,221 9 0.403 0.635 39.4 0.412 15.0 223.6 6 24 3.333 0.04 0.18
10 310 10 0.448 0.669 42.0 0.434 14.5 209.9 24 3.038 0.15
11 222 12 0.545 0.738 47.6 0.479 13.7 186.5 8 2.742 0.04
12 320 13 0.578 0.760 49.5 0.493 13.4 179.9 24 2.728 0.12
13 320 13 0.579 0.761 49.6 0.493 13.4 179.6 24 2.729 0.12
14 321 14 0.635 0.797 52.8 0.517 13.0 169.3 48 2.795 0.23
15 321 14 0.654 0.809 54.0 0.524 12.9 166.1 48 2.848 0.23
16 400 16 0.708 0.842 57.3 0.546 12.5 157.4 6 3.067 0.03
17 411,330 18 0.801 0.895 63.5 0.580 12.0 143.9 24 12 3.812 0.13 0.07
18 411,330 18 0.833 0.913 65.9 0.592 11.8 139.7 24 12 4.245 0.14 0.07
19 331 19 0.882 0.939 69.9 0.609 11.6 133.5 24 5.224 0.17
20 420 20 0.888 0.942 70.4 0.611 11.5 132.8 24 5.376 0.17
21 420 20 0.929 0.964 74.6 0.625 11.3 127.8 24 7.041 0.22
22 421 21 0.935 0.967 75.2 0.627 11.3 127.2 48 7.354 0.45
23 421 21 0.947 0.973 76.7 0.631 11.2 125.8 48 8.259 0.50
24 421 21 0.952 0.976 77.4 0.633 11.2 125.2 48 8.754 0.53
Ahora por regla 3 simples: 1.25x105 → 10

Línea INTENSIDAD(𝟏𝟎𝟓 ) Intensidad Calculada Intensidad Observada CONSISTENCIA


1 1.12 9 5 INCONSISTENTE
2 1.25 10 2 INCONSISTENTE
3 0.49 4 10 INCONSISTENTE
4 0.15 1 2 CONSISTENTE
5 0.35 3 5 INCONSISTENTE
6 0.33 3 3 CONSISTENTE
7 0 0 6 INCONSISTENTE
8 0.05 0.18 0 1 4 INCONSISTENTE INCONSISTENTE
9 0.04 0.18 0 1 1 CONSISTENTE CONSISTENTE
10 0.15 1 1 CONSISTENTE
11 0.04 0 4 INCONSISTENTE
12 0.12 1 1 CONSISTENTE
13 0.12 1 1 CONSISTENTE
14 0.23 2 1 CONSISTENTE
15 0.23 2 7 INCONSISTENTE
16 0.03 0 1 CONSISTENTE
17 0.13 0.07 1 1 5 INCONSISTENTE INCONSISTENTE
18 0.14 0.07 1 1 1 CONSISTENTE CONSISTENTE
19 0.17 0 5 INCONSISTENTE
20 0.17 0 2 CONSISTENTE
21 0.22 0 1 CONSISTENTE
22 0.45 0 1 INCONSISTENTE
23 0.50 0 2 INCONSISTENTE
24 0.53 0 1 INCONSISTENTE

- En la línea 7 el FACTOR DE ESCTRUCTURA (F) es igual a cero , F = 0 -> No existe h k l en el fotograma.

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