Escolar Documentos
Profissional Documentos
Cultura Documentos
Synthesis
Synthesis of ceramic powders and nanoparticles,
sintering and grain growth mechanisms
Synthesis of Ceramic Powders
• In conventional solid-state method, high temperature and heating for prolonged time
makes successful the particles coarse.
• However, in many cases, the chemical routes generally involve complex techniques
when compared to the conventional solid-state methods
Conventional Ceramic Synthesis Route
Direct reaction between solids wont react at room temperature High Temp. are required to react
DST-SERB project
Wet-Chemical (Nano) Methods
Sol-Gel Synthesis
General schematic of the co-precipitation method
Wet-Chemical (Nano) Methods
1:1
Synthesis of NaFe(SO4)2, a cathode material for Na ion batteries by Wet-Chemical
route
DST-SERB project
1. Mechanical attrition
(Ball milling)
2. Lithography
1. Sol-gel
2. Chemical vapor
deposition (CVD)
TOP-down approach-Ball milling
Chemical Vapour deposition (CVD)
RF Plasma Synthesis