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Manufacturing Letters 16 (2018) 36–39

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Manufacturing Letters
journal homepage: www.elsevier.com/locate/mfglet

Effect of process parameters on tribological performance of 316L


stainless steel parts fabricated by selective laser melting
Hua Li a, Maziar Ramezani a,⇑, Ming Li b, Chao Ma c, Jyhwen Wang c
a
Department of Mechanical Engineering, Auckland University of Technology, Auckland 1010, New Zealand
b
Department of Industrial and Systems Engineering, Texas A&M University, College Station, TX 77845, USA
c
Department of Engineering Technology and Industrial Distribution, Texas A&M University, College Station, TX 77845, USA

a r t i c l e i n f o a b s t r a c t

Article history: Selective laser melting (SLM) is an additive manufacturing technique based on metallic powders that are
Received 14 December 2017 melted by the energy of laser with a layer build-up technique. This paper investigates the effect of process
Received in revised form 3 April 2018 parameters on tribological performance of 316L stainless steel samples made by SLM. Rectangular sam-
Accepted 21 April 2018
ples were produced using SLM at different laser powers and along different build-up directions. Sliding
Available online 23 April 2018
wear tests were conducted under two different normal loads at a constant frequency of 4 Hz in ambient
temperature. A scanning electron microscope was used for observing the microstructures and wear
Keywords:
tracks. The results showed that lower laser powers resulted in samples with lower hardness and densities
Build-up direction
Laser power
and lack of fusion at melt pools boundaries. However, the effects of laser power and build-up direction on
Selective laser melting coefficient of friction (COF) and wear rate are not significant. At higher contact pressures, wear rate was
Sliding wear higher, but COF was not affected remarkably. The findings suggest that further study of process param-
eters, material properties and performance can advance tribological applications of SLM parts.
Ó 2018 Society of Manufacturing Engineers (SME). Published by Elsevier Ltd. All rights reserved.

1. Introduction SLM [4]. It was also reported that laser power is one of the most
influential process parameters; and with decrease in the laser
Selective laser melting (SLM) is one of the most popular metal power, the tensile properties deteriorate due to the increase of
additive manufacturing (AM) technologies, which builds a part porosity [5]. Some authors illustrated that with optimized param-
by selectively melting powdered feedstock layer by layer [1]. With eters, SLM process is capable of producing highly dense (98–99.5%
many advantages, such as the high flexibility of product’s shape, of theoretical density) parts [6–8].
short process time, and various materials availability, SLM has A positive linear correlation between volume percentage of
been a very attractive technique. Due to its distinctive processing porosity and wear rate was found by Sun et al. [9] for SLMed sam-
philosophy, the quality of production is strongly related to SLM ples. However, more studies on processing parameter are required
processing parameters (e.g. laser power, build-up direction, scan to deal with reducing porosity. It has been shown by Gu et al. [1]
speed, and hatch distance). that insufficient densification and coarsened grains which caused
Various studies have been conducted on the effects of process- by unoptimized scanning speed limit the hardness of SLMed pure
ing parameters on SLMed parts; however, little work has been Ti parts. By adjusting linear energy densities, Gu et al. [1] found
done in the field of tribological properties. Tribology plays an that wear rate and COF followed similar trend with hardness per-
important role in engineering and characterising the tribological formance. Nevertheless, to the best of the author’s knowledge,
performance of materials is crucial [2]. Previous studies indicated there are still no related studies focusing on inherent relationship
that processing parameters such as laser power, point distance or between processing parameters and wear behaviour of SS 316L
scan speed have strong effects on density of parts produced by material and a systematic approach to investigate the effect of
SLM and the presence of porosity leads to a decrease in mechanical SLM process parameters on tribological behaviour is still missing.
strength [3]. SEM images showed large-sized irregular-shaped The objective of this study is therefore to investigate the sliding
pores were distributed in microstructure of components made by wear behaviours of SS 316L parts fabricated by SLM with different
laser powers and building orientations.

⇑ Corresponding author.
E-mail address: maziar.ramezani@aut.ac.nz (M. Ramezani).

https://doi.org/10.1016/j.mfglet.2018.04.003
2213-8463/Ó 2018 Society of Manufacturing Engineers (SME). Published by Elsevier Ltd. All rights reserved.
H. Li et al. / Manufacturing Letters 16 (2018) 36–39 37

2. Material and methods measure the surface roughness of the samples before and after
grinding and polishing.
A commercial SLM machine (Renishaw AM400) equipped with The samples were mechanically ground and polished and ultra-
an inert gas and vacuum system was used to produce the samples sonically cleaned before wear tests. It is worth noting that the
with 316L stainless steel powder (Renishaw 316L-0407) with a grinding direction in all samples was along the sliding direction.
particle size of 15–45 mm. The machine uses a fibre laser with a Sliding wear tests were conducted under dry contact condition
wavelength of 1070 nm, whose beam diameter at the focal point and at ambient temperature using a linear reciprocating ball on
is 70 mm. Test samples were made by four different laser powers plate tribometer. SS 316L plates were fixed on the tribometer,
of 100 W, 150 W, 200 W and 300 W and three different build-up while the upper ball slides over the samples. A wear distance of
directions. A hatch distance of 110 mm and a layer thickness of 1000 m and a sliding stroke of 10 mm were used for all tests. The
50 mm were used for producing the samples with an exposure time upper balls were made of E-52100 hardened steel with 58 HRC
of 80 ms. and 10 mm in diameter. The roughness of the ball, Ra was 0.04
The densities of the samples were measured before the sliding mm. Two different normal loads of 10 N and 20 N were used for
wear tests using Archimedes’ principles. The dimensions of the the sliding wear tests at a constant frequency of 4 Hz. These two
samples were approximately 40  15  5 mm3. Hardness of the loads result in Hertzian contact stresses of 534 MPa and 672
samples were also measured by a Rockwell micro-hardness tester MPa, respectively. COF versus time were recorded during each test
based on ASTM E-18 standard and the mean values were calculated and the mass loss were measured after each test. Wear rates were
through five measurements. A stylus profilometer was used to then calculated by dividing the wear volume by sliding distance.

Table 1
Surface roughness, hardness and density of test samples.

Power Built-up Hardness after grinding Surface roughness before grinding Surface roughness after grinding Average Density Porosity
(W) direction (Rockwell C) Ra (mm) Ra (mm) (kg/m3) (%)
100 1 14.4 24.4 0.17 6558 17.5
150 1 17.6 15.4 0.10 7345 7.6
200 1 23.8 7.5 0.05 7638 3.9
200 2 22.3 7.9 0.05 7661 3.6
200 3 20.8 8.2 0.05 7753 2.5
300 1 24.8 6.7 0.05 7669 3.5

(a) (b)

(c) (d)

Fig. 1. Porosity produced by different laser powers: (a) 100 W, (b) 150 W, (c) 200 W, and (d) 300 W.
38 H. Li et al. / Manufacturing Letters 16 (2018) 36–39

All tests were repeated three times and the average values and part can be produced by 300 W laser power. Lack of fusion occurs
standard deviations were calculated. due to insufficient power supplied to a region of powder. It can also
be seen in Table 1 that porosity increases significantly at lower
3. Results and discussion laser powers.
Fig. 2 shows the effect of laser power, normal load and build-up
Table 1 shows the surface roughness, hardness, density and direction on COF and wear rate. As can be seen in Fig. 2(a) and (b),
porosity of samples made by different laser powers and with dif- an increase in normal load results in an increase in wear rate, how-
ferent built-up directions. The porosity was estimated based on ever the effect of normal load on COF is not significant. This trend
the measured density, p ¼ 1  q=qth , where p is the porosity, q is can be seen for all samples made by different laser powers. As
the measured density, and qth is the theoretical density of the demonstrated in Table 1, the hardness indeed increases with
material (7950 kg/m3). Hardness test results showed that it higher laser power. The wear performance, however, does not
increases by the increasing laser power, and hardness values for improve with increased hardness. It can be seen in Fig. 2 that sam-
200 W and 300 W laser powers are almost the same. SLM compo- ples made by lower laser powers (100 W and 150 W) show wear
nents had rough surface finish with the root mean square value Ra resistance similar to the samples made by highest laser power
of samples ranging between 6.7 and 24.4 mm. This is far from real (300 W). This is mainly due to their porous structure, where part
engineering applications and therefore, coarse grinding and polish- of the debris produced from the wear test can be pressed into
ing were used to finish the contact surfaces of all specimens. The the pores in the wear track. The pores produced at lower laser
root mean square values Ra of samples after grinding and polishing powers actually attract the wear debris. The debris is buried into
are presented in Table 1. Samples made by lower laser powers have the pores and welded to the base material due to high contact pres-
higher surface roughness. The samples made by 300 W laser power sure, which will increase the hardness during sliding wear tests
have the hardest and finest surfaces as well as relatively higher and improve the wear resistance of the samples. The observation
density compared with other samples. The effect of build-up direc- of wear tracks in Fig. 3 for samples made with different laser pow-
tion on surface roughness, hardness and density is not remarkable. ers showed they all have similar morphology and no pore could be
Porosity is a common defect in SLM products that negatively found in the wear track, even for originally porous samples made
affects their mechanical properties. Fig. 1 shows the porosity of at lower laser powers.
samples made by different laser powers taken by scanning electron Different build-up directions as well as the sliding direction are
microscope (SEM). As illustrated in the figure, pores can be illustrated in Fig. 2(c). The sliding direction in all wear tests were
decreased by increasing the laser power and a nearly fully dense along the longest side of the specimen. Fig. 2(c) and (d) show the

Fig. 2. (a and b) Effect of laser power on COF and wear volume (Build-up direction 1, 4 Hz frequency), (c and d) Effect of build-up direction on COF and wear volume (200 W
laser power, 4 Hz frequency).
H. Li et al. / Manufacturing Letters 16 (2018) 36–39 39

(a) (b)

(c) (d)

Fig. 3. Wear track for samples produced by different laser powers: (a) 100 W, (b) 150 W, (c) 200 W, and (d) 300 W. (4 Hz frequency, 20 N normal load, build-up direction 1).

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