PDP TATASteel 5TPDCO2 - Rev1 PDF

CUSTOMER LICENSOR
PROCESS DESIGN PACKAGE

FOR 5 TPD CO2 RECOVERY
PLANT
Design and Engineering Package
For
5 TPD CO2 Capture Plant
Submitted To
TATA Steel Limited

P.O. Bistupur, Jamshedpur, Jharkhand, India - 831001
By
CARBONCAPTURE TECHNOLOGIES PRIVATE LIMITED

First Floor, Jivan Silk Mills Road, Opp MTNL Telephone Exchange
Sakinaka, Mumbai - 400072
This document is a property of Carbon Clean Solutions Limited and it cannot be reproduced or communicated to any third party
without prior written consent of Carbon Clean Solutions Limited.
CUSTOMER LICENSOR
PLANT
TABLE OF CONTENTS
1. Design Basis
2. Process Description
3. Process Flow diagram
4. Heat & Material Balance
5. Fluid Classification
6. Piping & Instrumentation Diagrams
7. Control and Operating Philosophy
8. Instrumentation Summary and I/Os list
9. Equipment List
10. Process Equipment Datasheets
11. Electrical Load List
12. Utilities, Chemicals and Effluent Summary
13. HSE Procedure, Solvent and Waste Handling Procedure
Annexure – I: Solvent MSDS
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DESIGN BASIS PROJECT

5 TPD CO2 RECOVERY
PLANT
DOC. NO. TSL-DB-100

1. INTRODUCTION
Tata steel produces LD slag and part of it is converted to products used in building roads, fly ash bricks
etc. and the balance is disposed as waste. Tata steel intends to utilize this LD slag waste by carbonization
of slag to reduce the disposal costs and to produce value products. For slag carbonation, TATA steel
intends to use the CO2 in the stack emissions or any other gas source available within the plant.
After diligent study of the Gas network with the Customer, its determined to extract the feed gas for the
CO2 recovery from the BF + LD gas mixture network. As per TATA Steel, the BF gas coming from the
G-Blast Furnace is mixed with the LD gas in 90-10% proportion before sending it to Coke plant. CCSL
performed the BF+LD gas mixture analysis to design the pre-treatment & CO2 recovery plant sections.
The feed gas composition is given below.
2. FEED GAS COMPOSITION
Temperature C 35-40
Pressure bara 1.0
CO 18.6
O2 1.85
Composition CO2 20.5
(mol%) N2 45.4
H2 6.64
H 2O 7.01
CH4 30.6
SO2 < 100.0
Composition Acid Mist < 0.2
(ppmv) NO/NO2/NOx < 1.0
PM (mg/Nm3) 12.1
NH3 < 1.0
Flow rate kg/h & Nm3/h 840 & 650
0 16.10.18 Issued for Engineering SL GK ARK

Rev. No. Date Description Prepared Checked Approved
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5 TPD CO2 RECOVERY
PLANT
DOC. NO. TSL-DB-100

3. Utilities to be supplied by TATA Steel at Battery Limits

Steam
Minimum 3.0
Supply pressure (barg)
Maximum 4.5
Supply temperature (0C) Saturated
Process Water
Minimum 3.0
Supply pressure (barg) Normal 4
Maximum 4.5
Minimum 24
Supply temperature (0C) Normal 28
Maximum 30
Water quality
pH TH TSS Conductivity Total Fe
8.4- <10 ppm (max) as CaCO3 20 ppm (max) 0-2000 µS/cm 1 ppm (max)
89
8.68 4 7 285 0.88
DM Water
Supply pressure (barg) Minimum
(Water is stored in overhead Normal
tank and supplied as required) Maximum 2.8 kg/cm2
Minimum 24
Maximum 35
Instrument Air
Minimum 4.0
Supply pressure (barg) Normal 4.5
Maximum 5
Minimum
Maximum
Back up for Instrument Air

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5 TPD CO2 RECOVERY
PLANT
DOC. NO. TSL-DB-100

4. CHEMICALS
CDRMax®
CCSL proprietary solvent CDRMax® shall be used for capture of CO2. A storage tank for storing
solvent inventory in the plant is considered. The makeup shall be done directly from the Solvent
barrels.
SCRUBBING AGENT
The Sodium Bicarbonate scrubbing solutions shall be used for removing SO2 & NO2 from fuel gas.
Sodium Hydroxide is required for the operation of fuel gas pre-treatment and thermal reclaimer.
5. POWER SUPPLY
Power HV Power LV Lightning Emergency
Underground cable lines
Aboveground cable lines
Rated voltage V 220/440 220/440 220/440 220/440
Related frequency Hz 50 50 50
Available power kVA
Earthing Grid: Available (Power supply has to be arranged as per the specification.)
- IT
6. END PRODUCT (CO2 conditions at the battery limits)

Minimum 0.4
CO2 pressure (barg)
Maximum 0.8
Minimum 35
0
CO2 temperature ( C) Normal 40
Maximum 50
CO2 purity, mol% dry basis Minimum > 99
CO2 flow rate, MTPD Minimum 5.0
7. PLANT LOCATION AND LOCAL CONDITIONS

Location Jamshedpur, Jharkhand, India
Minimum 10
Ambient temperature, (0C)
Normal 30

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5 TPD CO2 RECOVERY
PLANT
DOC. NO. TSL-DB-100

Maximum 45
Minimum 0.998
Atmospheric pressure (bar) Normal 1.01
Maximum 1.015
Minimum 20
Relative humidity Normal 45
Maximum 90
Wind Max. 25 km/hr (in last 10 years); Avg: 15 km/hr
Rainfall Max : 600 mm (last 10 years)
Jamshedpur lie in Zone II. The maximum intensity
Seismic data
expected in these areas would be around MSK VI.
Soil conditions Stable (please mention any specific property)
8. SHE REQUIREMENTS
Safety (Lightning/Earthing/CO
Will be considered and whole plant is leak proof
monitoring/ Others)
HSE procedures during installation PSSR (PRE-STARTUP SAFETY REVIEW) will be
and commissioning conducted
9. OPERATIONAL PHILOSOPHY
Existing DCS CCS will provide communication ports at the battery limits and give the
or not specifications required for the DCS setup which is in Customer scope.
Unit numbering The general numbering philosophy of CCSL will be used.
10. MISCELLANEOUS
Transportation limits No Restriction
Restrictions on column
No restriction
height
Plot area available 24 x 6 meters
CCSL will provide the specifications for the civil supports for the
Civil work
skid.
LD gas: Lower-14.8, Upper-71.5
Explosive limits of BF gas: Lower-35, Upper-73.5
gases, % The gas being used for the CO2 recovery consists of 90% BF gas
and 10% LD gas

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5 TPD CO2 RECOVERY
PLANT
DOC. NO. TSL-DB-100

11. BATTERY LIMITS AND CONDITIONS
Following shall be battery limit temperature & pressure at battery limit.
S. No. Description P, bar g T,°C Location

1 Fuel Gas 0.05-0.07 35 – 50 Battery Limit
2 Product CO2 0.5 35 – 40 Battery Limit
3 LP/MP Steam 3* Saturated Battery Limit
4 Steam Condensate 4 ~130 Battery Limit
5 Raw Water 2.5 Ambient Battery Limit
6 DM Water 4 Ambient Battery Limit
7 Depleted Fuel Gas 0-0.01 40 - 45 Battery Limit
*LP steam pressure.

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PROCESS 5 TPD CO2 RECOVERY
DESCRIPTION PROJECT PLANT
DOC. NO. TSL-PD-200

INTRODUCTION
This document describes the technology & process proposed for recovery of CO2 from the fuel gas
of Blast furnace after enrichment with LD gas at TATA Steel Limited. This document shall be read
in conjunction with Process flow diagram bearing document No. TSL-PFD-201.
PROCESS OVERVIEW
2.1 PRE-TREATMENT SECTION
Currently the fuel gas from the Blast Furnace is sent to Coke plant after mixing with LD gas in 90%-
10% proportion respectively. Fuel gas for CO2 recovery plant shall be tapped from the gas network
going to the Coke plant downstream of LD gas enrichment. A new damper shall be provided on fuel
gas duct line. The fuel gas composition is given in Design Basis document below for design of CO2
Recovery Plant. (Ref document TSL-DB-101).
Blower BL-101 is an induced draft fan provided at the battery limit to compensate the pressure drop
in the CO2 recovery plant.
The fuel gas will be sent to SOx/NO2 Scrubbing Column T-101 to reduce the concentration of SO2
to below 1 ppmv by circulating scrubbing solution. Scrubbing Solution is pumped from SOx
Scrubbing Column T-101 sump and discharged to Scrubbing Solution Circulation Cooler E-101 and
Scrubbing Solution Filtration Package Z-101 via Scrubbing Solution Circulation Pump P-101 A/B.
Scrubbing Solution Circulation Cooler E-101 takes the heat taken up by Scrubbing Solution in
SOx/NO2 Scrubbing Column T-101 and cools the solution to 40 C using cooling water. The bleed is
taken from Scrubbing Solution Circulation Pump P-101 A/B discharge based on conductivity of
circulating scrubbing solution. pH of circulation solution is controlled by dosing of Scrubbing
Solution via Scrubbing Solution Dosing Pump P-111 from Scrubbing Solution Tank TK-102. Solid
Scrubbing agent is added in tank to prepare scrubbing solution of required concentration. Caustic
Dosing Package Z-103 is provided as backup in case of eventualities.

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DOC. NO. TSL-PD-200

2.2 CARBON DIOXIDE RECOVERY SECTION
The fuel gas is now fed to the bottom of Absorber Column T-102 where the fuel gas contacts the
CDRMax® solvent in counter current direction. The lean solvent (containing a little amount of CO2)
is fed from the top of the absorption section and reacts selectively with the CO2 in the fuel gas.
Absorber Column T-102 consists of two structured packed bed sections to enable efficient mass and
heat transfer between the gas and liquid phases for the absorption of CO2. The Absorber Column T-
102 consists an inter-stage cooling section to remove the exothermic heat of reaction generated
during the absorption of CO2. The inter-stage cooling section contains Inter-Stage Pump P-102 for
withdrawal of liquid from the column. This flow is adjusted to maintain the temperature profile in
the absorber and avoid any bulge in the temperature in the bed. The liquid is fed to the top of the
bottom packing section after being cooled to 40 °C by cooling water in Inter-Stage Cooler E-102. 80
- 90 % of the inlet CO2 will be absorbed in the carbon capture plant to get 5 TPD of CO2.
The fuel gas with residual CO2 will then enter the Water Wash Column T-103 at around 65 - 70 °C.
Two structured packed bed sections are provided in the Water Wash Column T-103 to recover the
solvent from the depleted fuel gas leaving the absorber and to cool the depleted fuel gas (to maintain
the water balance). The fuel gas is washed and cooled with a circulating loop of water to recover
any entrained solvent. Both packings in the Water Wash Column are of structured type and with a
pump around system. The water in the lower water wash (water wash 2) is circulated with Water
Wash Circulation Pump-2 P-108 through water cooled Water Wash Circulation Cooler-2 E-108. The
objective of the lower water wash (water wash 2) is to recover the solvent vapor so that the upper
water wash (water wash 1) will be circulating wash water with lower solvent concentration. The fuel
gas is further cooled in the upper water wash packing to 40 °C. The water in the upper water wash
(water wash 1) is circulated with Water Wash Circulation Pump-1 P-107 through water cooled
Water Wash Circulation Cooler-1 E-107. The fuel gas temperature is maintained very close to the
fuel gas inlet temperature to the absorber column to minimize the water make-up. As the fuel gas
cools in each water wash section condensation occurs. In the upper water wash (water wash 1) the
condensate will overflow through a downpipe into the lower water wash (water wash 2). The
condensation and overflow from water wash section 2 will be transferred to Absorber Column T-

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DOC. NO. TSL-PD-200

102 using WW condensate pump P-109.The treated fuel gas temperature is controlled by controlling
the temperature of the wash water in the top water wash section.
The solvent flow from Absorber Column T-102, which is rich in CO2, is called rich solvent. The
rich solvent flow is regulated by a flow control valve located at Rich Solvent Pump P-103 A/B
discharge. The rich solvent is pumped by Rich Solvent Pump P-103 A/B through Lean Rich
exchanger E-103 and heated to about 105-110 °C by the lean solvent on the other side of the heat
exchanger. The lean solvent comes from the Stripper Reboiler E-105 and is around 120 °C. The rich
solvent is then fed to the top of Stripper Column T-104. Stripper Column is a packed column with
two structured packing sections and is connected to a re-boiler where the rich solvent is heated
further to maintain the reboiler temperature to strip the CO2. Heat is supplied to Stripper Reboiler E-
105 using LP steam.
Stripper Column T-104 produces overhead vapor, at about 1.8 to 2 bara and about 80-100 °C and is
cooled to about 40 °C in Stripper Condenser E-104. The CO2 stream and condensate are sent to the
Stripper Reflux Drum V-101. The condensate which has been collected is sent back to the stripper
as reflux, or alternatively this can be sent to the Absorber sump. The stripper top pressure is
controlled at 1.8 to 2 bara through a pressure control valve at the condenser outlet line of CO2
stream.
Lean solvent at approximately 120 °C leaves the bottom of the Stripper Reboiler E-105, through
Lean Solvent Pump P-106 A/B. A spill back line controls the level in the Stripper Reboiler sump E-
105. The lean solvent exchanges heat with rich solvent in Lean Rich Exchanger E-103 as described
earlier. The lean solvent is further cooled in Lean Solvent Cooler E-106 to about 38-42 °C by
controlling the cooling water flow. The cooled lean solvent is then sent to the top of absorption
section of Absorber Column T-102. The water balance in the solvent circulation loop is monitored
by the level in the absorber sump. The decrease in level is made up by either decreasing the
temperature of fuel gas at the water wash exit or increasing the temperature of the fuel gas at the
inlet to the absorber by about 1 °C. A DM water line is considered to maintain the level if the level
drops significantly in the Absorber column sump.

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DOC. NO. TSL-PD-200

2.3 SOLVENT TREATMENT UNIT
The solvent treatment section consists of two parts – the filtration section & the thermal reclaiming
section. These two can be operated independently.
The Filtration Section consists of an activated carbon filter with a duplex of mesh / cartridge filters
(< 5-micron pore size) at the inlet and outlet. The activated carbon filter is meant to remove the high
molecular weight degradation products formed by the solvent. A bleed (about 0.15 m3/ hour) from
the lean solvent line at the Lean Solvent Pump P-106 A/B outlet is taken to the Filtration section.
The filtration package shall be provided with differential pressure measurements with alarms and
this shall be reported to the DCS. When the differential pressure across the filter increases and
reaches the value specified by the filter vendor, the filter shall be by-passed and cleaned. After
cleaning, the filter shall be brought back online. The activated carbon shall be replaced based on the
vendor’s recommendations. Liquid sampling points are provided upstream and downstream of the
filtration section to measure its performance.
In case of a decrease in the CO2 production or a change in the solvent colour, the Heat stable salts
(HSS) content in the solvent shall be measured. The thermal reclaimer system shall be operated to
remove HSS and other contaminants from the solvent if the concentrations are more than 2 wt.%.
This is a vendor package and the operating manual from the vendor should be referred to. A bleed
(about 0.05 m3/ hour) from the lean solvent line at the Lean Solvent Pump P-106 A/B outlet is taken
to the Reclaiming section and, after treatment, the treated solvent is fed back to the Absorber
Column T-102 sump. The thermal reclaimer shall contain a reboiler and condenser and is operated
under vacuum conditions with the temperature ranging from 160 – 180 °C. The solvent is vaporized
in the reboiler using a thermic fluid heater or MP Steam and HSS will remain in the residue. The
vapors from the reboiler are sent to condenser. Both vapor and liquid from the condenser are routed
to the absorber column bottom. The residue will be mixed with DM water before withdrawal and
will be disposed of as hazardous waste.
2.4 SOLVENT STORAGE SECTION

The initial fill of solvent shall be stored in Solvent Storage Tank TK-101. The solvent shall be
loaded into the Absorber and Stripper via Solvent Transfer Pump P-110. Subsequently, during the

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DOC. NO. TSL-PD-200

plant shutdown / maintenance, the solvent shall be pumped back to Solvent Storage Tank TK-101
via Rich Solvent Pump P-103 A/B.
2.5 UTILITIES
Low Pressure steam is required for solvent regeneration in the Stripper Reboiler E-105. A Kettle-
type Reboiler E-105 is used to heat the solvent to liberate CO2 from the solvent inside the stripper.
The steam shall be supplied at the battery limits of the CO2 plant. The steam condensate from
Stripper Reboiler E-105 is collected in Steam Condensate Drum V-102 and pumped back to battery
limit via Steam Condensate Pump P-105.
The cooling water and DM water requirement for the CO2 capture unit shall be supplied at the
battery limit.
Electrical Power shall be supplied at the battery limit for running pumps, blowers and Cooling
Tower etc.

M
AI
M
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CUSTOMER:
PROJECT 5 TPD CO2 RECOVERY PLANT
LICENSOR: MATERIAL BALANCE DOC. NO. TSL‐HMB‐200

CARBON CLEAN
SOLUTIONS LIMITED REV. NO. 0
Stream Number ‐ 1 2 3 4 5 6 7 8 9
SOx/NO2 Column
Fuel Gas Fuel Gas to SOx/NO2 Column Circulation Water
Circulation Water to Fuel Gas to Interstage Draw Draw off Liquid to Draw off Liquid
Stream Description ‐ Inlet to SOx/NO2 Scrubbing Circulation Water Inlet to SOx/NO2
Scrubbing Solution Absorber from Absorber Interstage Cooler return to Absorber
Blower Column Outlet Column
Cooler
SOx/NO2 Scrubbing Scrubbing Solution Scrubbing Solution SOx/NO2
From BL Blower Absorber Interstage Pump Interstage Cooler
Column Circulation Pump Circulation Cooler Scrubbing Column
‐
SOx/NO2 Scrubbing Scrubbing Solution Scrubbing Solution SOx/NO2 Scrubbing
To Blower Absorber Interstage Pump Interstage Cooler Absorber
‐ Column Circulation Pump Circulation Cooler Column
Water kmol/hr 2.033 2.033 195.219 195.202 195.171 1.941 53.553 53.553 53.553
Carbon Dioxide kmol/hr 5.945 5.945 0.018 0.018 0.018 5.945 4.670 4.670 4.670
Solvent kmol/hr 0.000 0.000 0.000 0.000 0.000 0.000 7.057 7.057 7.057
Hydrogen kmol/hr 1.926 1.926 0.000 0.000 0.000 1.926 0.000 0.000 0.000
Carbon Monoxide kmol/hr 5.394 5.394 0.001 0.001 0.001 5.394 0.000 0.000 0.000
Nitrogen kmol/hr 13.166 13.166 0.001 0.001 0.001 13.166 0.000 0.000 0.000
Oxygen kmol/hr 0.536 0.536 0.000 0.000 0.000 0.536 0.000 0.000 0.000
Mass Flow kg/hr 839.21 839.21 3517.70 3517.40 3516.84 837.55 1923.53 1923.53 1923.53
Volume Flow cum/hr 753.9 696.6 3.5 3.5 3.5 676.9 1.7 1.7 1.7
** Total Flow kmol/hr 29.00 29.000 195.24 195.22 195.19 28.91 65.28 65.28 65.28
Pressure bara 1.00 1.13 1.07 2.10 1.10 1.110 1.03 2.20 1.20
Temperature Celsius 40.00 53.77 40.33 40.33 40.00 40.00 52.96 52.96 40.00
Frac Vapor ‐ 1.00 1.00 0.00 0.00 0.00 1.00 0.00 0.00 0.00
Liquid Fraction ‐ 0.00 0.00 1.00 1.00 1.00 0.00 1.00 1.00 1.00
Molec Wt ‐ 28.94 28.94 18.02 18.02 18.02 28.97 29.47 29.47 29.47
Density kg/cum 1.11 1.2 991.6 991.6 991.75 1.24 1108.4 1108.4 1118.6
Viscosity cP 0.02 0.02 0.65 0.65 0.66 0.02 2.92 2.93 4.70
Thermal Conductivity W/m‐K 0.02 0.02 0.62 0.62 0.62 0.02 0.38 0.37 0.37
Heat Capacity kJ/kg‐K 1.08 1.09 4.18 4.18 4.18 1.08 2.61 2.85 2.85
Surface Tension N/m ‐ ‐ 0.07 0.07 0.07 ‐ 0.06 0.06 0.06

REV. NO. DATE DESCRIPTION PREPARED CHECKED APPROVED
CUSTOMER:
LICENSOR:
CARBON CLEAN
MATERIAL BALANCE DOC. NO. TSL‐HMB‐200
SOLUTIONS LIMITED 0
REV. NO.
Stream Number ‐ 10 11 12 ‐ Vapor 12 ‐ Liquid 13 14 ‐ Vapor 14 ‐ Liquid 15 16 17
Condensed
Acid Gas to Condensed Liquid to
Stream Description ‐ Rich Solvent Rich Solvent Rich Solvent to Stripper Acid Gas to Reflux Drum Liquid to Acid Gas to BL
Condenser Stripper
Reflux Pump
Rich Solvent
From Absorber LR Exchanger Stripper Condenser Reflux Drum Reflux Drum Reflux Pump
Pump
‐
Rich Solvent
To LR Exchanger Stripper Condenser Reflux Drum Reflux Pump BL Stripper
‐ Pump
Water kmol/hr 66 66 0 66 4 0 3 3 0 3
Carbon Dioxide kmol/hr 6.8 6.8 1.1 5.8 4.8 4.8 0.0 0.0 4.8 0.0
Solvent kmol/hr 8.82 8.82 0.00 8.82 0.01 0.00 0.01 0.01 0.00 0.01
Hydrogen kmol/hr 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Carbon Monoxide kmol/hr 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Nitrogen kmol/hr 0 0 0 0 0 0 0 0 0 0
Oxygen kmol/hr 0 0 0 0 0 0 0 0 0 0
Mass Flow kg/hr 2431 2431 54 2376 275 213 62 62 213 62
Volume Flow cum/hr 2.1 2.1 11.6 2.2 127.1 63.9 0.1 0.1 63.9 0.1
** Total Flow kmol/hr 81.63 81.63 1.48 80.15 8.32 4.95 3.36 3.36 4.95 3.36
Pressure bara 1.04 5.00 4.00 4.00 2.00 2.00 2.00 2.00 2.00 4.00
Temperature Celsius 43.70 43.77 107.00 107.00 97.80 40.00 40.00 40.00 40.00 40.00
Frac Vapor ‐ 0.00 0.00 1.00 0.00 1.00 1.00 0.00 0.00 1.00 0.00
Liquid Fraction ‐ 1.00 1.00 0.00 1.00 0.00 0.00 1.00 1.00 0.00 1.00
Molec Wt ‐ 29.78 29.78 36.72 29.65 33.04 43.04 18.32 18.32 43.04 18.32
Density kg/cum 1135.8 1135.7 4.7 1059.9 2.16 3.34 1000.6 1000.6 3.34 1000.6
Viscosity cP 4.15 4.14 0.02 0.74 0.02 0.02 0.69 0.69 0.02 0.69
Thermal Conductivity W/m‐K 0.37 0.37 0.02 0.38 0.02 0.02 0.62 0.62 0.02 0.62
Heat Capacity kJ/kg‐K 2.69 2.69 1.08 2.85 1.16 0.88 4.11 4.11 0.88 4.11
Surface Tension N/m 0.06 0.06 0.05 0.06 0.06 0.06

CUSTOMER:
PROJECT: 5 TPD CO2 RECOVERY PLANT
LICENSOR:
CARBON CLEAN
MATERIAL BALANCE DOC NO: TSL‐HMB‐200
SOLUTIONS LIMITED REV NO: 0
Stream Number ‐ 18 19 20 21 22 23
Lean Solvent
Lean Solvent From Lean Solvent to LR to Lean Depleted Fuel Gas to Water Circulation Water from
Stream Description ‐ Lean Solvent to Absorber
Stripper Exchanger Solvent Wash Column Water Wash Column
Cooler
From Stripper Lean Solvent Pump LR Exchanger Lean Solvent Cooler Absorber Water Wash Column

‐
Lean Solvent
To Lean Solvent Pump LR Exchanger Absorber Water Wash Column WW Circulation Pump 2
‐ Cooler
Water kmol/hr 66 66 66 66 7 104
Carbon Dioxide kmol/hr 2.1 2.1 2.1 2.1 1.2 0.3
Solvent kmol/hr 8.82 8.82 8.82 8.82 0.02 0.57
Hydrogen kmol/hr 0.00 0.00 0.00 0.00 1.93 0.00
Carbon Monoxide kmol/hr 0.00 0.00 0.00 0.00 5.39 0.00
Nitrogen kmol/hr 0 0 0 0 13 0
Oxygen kmol/hr 0 0 0 0 1 0
Mass Flow kg/hr 2217 2217 2217 2215 721 1942
Volume Flow cum/hr 2.3 2.3 2.1 2.1 766.3 1.97
** Total Flow kmol/hr 76.68 76.68 76.68 76.55 29.25 105.11
Pressure bara 2.03 3.20 2.20 1.20 1.07 1.02
Temperature Celsius 122.44 122.44 51.66 40.00 64.71 64.72
Frac Vapor ‐ 0.00 0.00 0.00 0.00 1.00 0.00
Liquid Fraction ‐ 1.00 1.00 1.00 1.00 0.00 1.00
Molec Wt ‐ 28.92 28.92 28.92 28.94 24.65 18.48
Density kg/cum 976.9 976.9 1038.6 1047.4 0.9 988.5
Viscosity cP 0.56 0.56 3.12 4.81 0.02 0.47
Thermal Conductivity W/m‐K 0.38 0.38 0.37 0.37 0.03 0.63
Heat Capacity kJ/kg‐K 3.32 3.32 3.19 3.18 1.26 4.12
Surface Tension N/m 0.05 0.05 0.06 0.06 ‐ 0.06

CUSTOMER:

CARBON CLEAN
Stream Number ‐ 24 25 26 27 28 29 30 31
Circulation Water Circulation Water
Circulation Water Circulation Water Circulation Water WW Condensate to
to WW to WW Depleted Fuel WW Condensate to
Stream Description ‐ return to WW from WW Column return to WW WW Condensate
Circulation Circulation Gas to BL Absorber
Column Section 2 Section 1 Bottom Column Section 1 Pump
Cooler 2 Cooler 1
WW Circulation WW Circulation Water Wash WW Circulation WW Circulation Water Wash Water Wash
From Water Wash Column
Pump 2 Cooler 2 Column Pump 1 Cooler 1 Column Condensate Pump
‐
WW Circulation Water Wash WW Circulation WW Circulation Water Wash Water Wash
To BL Absorber
‐ Cooler 2 Column Pump 1 Cooler 1 Column Condensate Pump
Water kmol/hr 104 104 95 95 95 2 6 6
Carbon Dioxide kmol/hr 0.3 0.3 0.0 0.0 0.0 1.2 0.0 0.0
Solvent kmol/hr 0.57 0.57 0.02 0.02 0.02 0.00 0.02 0.02
Hydrogen kmol/hr 0.00 0.00 0.00 0.00 0.00 1.93 0.00 0.00
Carbon Monoxide kmol/hr 0.00 0.00 0.00 0.00 0.00 5.39 0.00 0.00
Nitrogen kmol/hr 0 0 0 0 0 13 0 0
Oxygen kmol/hr 0 0 0 0 0 1 0 0
Mass Flow kg/hr 1942 1942 1721 1721 1721 623 102 102
Volume Flow cum/hr 1.97 1.95 1.7 1.74 1.73 592.0 0.1 0.1
** Total Flow kmol/hr 105 105 95.46 95.46 95.51 23.91 5.54 5.539
Pressure bara 2.22 1.22 1.02 2.21 1.21 1.05 1.02 4.000
Temperature Celsius 64.72 45.00 51.19 51.19 39.00 39.85 60.12 60.12
Frac Vapor ‐ 0.00 0.00 0.00 0.00 0.00 1.00 0.00 0.00
Liquid Fraction ‐ 1.00 1.00 1.00 1.00 1.00 0.00 1.00 1.00
Molec Wt ‐ 18.48 18.48 18.03 18.03 18.03 26.06 18.33 18.33
Density kg/cum 988.5 997.1 988.4 988.4 992.8 1.1 988.6 988.61
Viscosity cP 0.47 0.66 0.54 0.54 0.67 0.02 0.49 0.49
Thermal Conductivity W/m‐K 0.63 0.61 0.64 0.64 0.62 0.03 0.64 0.64
Heat Capacity kJ/kg‐K 4.12 4.12 4.18 4.18 4.18 1.15 4.14 4.14
Surface Tension N/m 0.06 0.06 0.06 0.06 0.06 ‐ 0.06 0.06

CUSTOMER:

CARBON CLEAN
Stream Number ‐ 32 33 34 35 36 37 38 39 40
Steam to Condensate from
Stream Description ‐ CW Supply CW Supply CW Return CW Supply CW Return CW Supply CW Return
Reboiler Reboiler
Scrubbing Solution
From BL Reboiler BL BL BL Interstage Cooler BL Lean Solvent Cooler
‐ Circulation Cooler
Scrubbing Solution Interstage
To Reboiler BL CW Users BL BL Lean Solvent Cooler BL
Circulation Cooler Cooler
‐
Water kmol/hr 14.7 14.7 1009.3 73 73 118 118 137 137
Carbon Dioxide kmol/hr 0 0 0 0 0 0 0 0 0
Solvent kmol/hr 0 0 0 0 0 0 0 0 0
Hydrogen kmol/hr 0 0 0 0 0 0 0 0 0
Carbon Monoxide kmol/hr 0 0 0 0 0 0 0 0 0
Nitrogen kmol/hr 0 0 0 0 0 0 0 0 0
Oxygen kmol/hr 0 0 0.00 0 0 0 0 0 0
Mass Flow kg/hr 265 265 18152.00 1319 1319 2123 2123 2461 2461
Volume Flow cum/hr 123 11.7 18.2 1.326 1.3 2 2 2.5 1.4
** Total Flow kmol/hr 14.7 14.7 1009 73 73 118 118 137 137
Pressure bara 4.00 3.95 6.50 5.00 4.50 5.00 4.50 5.00 4.50
Temperature Celsius 143.60 143.60 30.00 30.00 38.00 30.00 38.00 30.00 38.00
Frac Vapor ‐ 1.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Liquid Fraction ‐ 0.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00
Molec Wt ‐ 18.00 18.00 18.00 18.00 18.00 18.00 18.00 18.00 18.00
Density kg/cum 2.16 923.0 995.0 995.0 992.70 995.00 992.7 995.0 992.7
Viscosity cP 0.01 0.19 0.81 0.81 0.69 0.81 0.69 0.81 0.69
Thermal Conductivity W/m‐K 0.03 0.68 0.61 0.61 0.62 0.61 0.62 0.61 0.62
Heat Capacity kJ/kg‐K 2.34 4.30 4.18 4.18 4.18 4.18 4.18 4.18 4.18
Surface Tension N/m ‐ 0.05 0.07 0.070 0.070 0.07 0.07 0.07 0.07

REV. NO. DATE DESCRIPTION PREPARER CHECKER APPROVER
CUSTOMER:

CARBON CLEAN
SOLUTIONS LIMITED 0
REV.NO.
Stream Number ‐ 41 42 43 44 45 46 47
Stream Description ‐ CW Supply CW Return CW Supply CW Return CW Supply CW Return CW Return
WW Circulation WW Circulation Stripper

From BL BL BL CW Users
‐ Cooler 1 Cooler 2 Condenser
WW
WW Circulation Stripper
To BL Circulation BL BL Cooling Tower
Cooler 1 Condenser
‐ Cooler 2
Water kmol/hr 146 146 263 263 273 273 1009
Carbon Dioxide kmol/hr 0 0 0 0 0 0 0
Solvent kmol/hr 0 0 0 0 0 0 0
Hydrogen kmol/hr 0 0 0 0 0 0 0
Carbon Monoxide kmol/hr 0 0 0 0 0 0 0
Nitrogen kmol/hr 0 0 0 0 0 0 0
Oxygen kmol/hr 0 0 0 0 0 0 0
Mass Flow kg/hr 2620 2620 4725 4725 4904 4904 18152
Volume Flow cum/hr 2.6 3 4.7 5 5 5 18
** Total Flow kmol/hr 146 146 263 263 273 273 1009
Pressure bara 5.00 4.50 5.00 4.50 5.00 4.50 4.00
Temperature Celsius 30.00 38.00 30.00 38.00 30.00 38.00 38.00
Frac Vapor ‐ 0.00 0.00 0.00 0.00 0.00 0.00 0.00
Liquid Fraction ‐ 1.00 1.00 1.00 1.00 1.00 1.00 1.00
Molec Wt ‐ 18.00 18.00 18.00 18.00 18.00 18.00 18.00
Density kg/cum 995.0 992.70 995.0 992.70 995.0 992.70 992.7
Viscosity cP 0.81 0.69 0.81 0.69 0.81 0.69 0.69
Thermal Conductivity W/m‐K 0.61 0.62 0.61 0.62 0.61 0.62 0.62
Heat Capacity kJ/kg‐K 4.18 4.18 4.18 4.18 4.18 4.18 4.18
Surface Tension N/m 0.07 0.07 0.07 0.07 0.07 0.07 0.07

REV. NO. DATE DESCRIPTION PREPARER CHECKER APPROVER
CUSTOMER
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LICENSOR
1 of 1
FLUID 5TPD CO2 RECOVERY
CLASSIFICATION PROJECT PLANT
DOC. NO. TSL-FC-800

S. No Fluid Name Fluid Code Remarks
A PROCESS
1 Fuel Gas FG
2 Rich Solvent RS
3 Lean Solvent LS
4 CO2 Vapour CO2
5 Process Vapour VA
6 Solvent Solution SS
7 Scrubbing Solution SAS
8 Wash Water WW
9 Reflux Condensate RC
B UTILITIES
1 Cooling water Supply CWS
2 Cooling water Return CWR
3 DeMineralized Water DM
4 LP Steam LPS
5 LP Steam condensate LPC
6 Plant Air PA
7 Nitrogen N
8 Process Water PW
9 Instrument Air IA
10 MP Steam MPS

M
M
M M
S2
S1
M S2
S1
S1
M M
S2
S1
M M
M
M
S1
S2
S2
S1
S1
S1
M M M
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LICENSOR
CONTROL AND 1 of 11
OPERATING PROJECT
5 TPD CO2 RECOVERY
PLANT
PHILOSOPHY TSL-COP-301
DOC. NO.
INTRODUCTION
This document describes the control and operating philosophy proposed for recovery of CO2 from
the fuel gas of the TATA STEEL from blast furnace. This document shall be read in conjunction
with Process flow diagram bearing document No. TSL-PFD-201 and Piping and Instrumentation
Diagrams bearing document no. TSL-PID-300/301/302/303/304/305/306/307/308/309.
PROCESS CONTROL DESCRIPTION

Currently the fuel gas from the Blast Furnace is sent to Coke plant after mixing with LD gas in 90%-
10% proportion respectively. Fuel gas for CO2 recovery plant shall be tapped from the gas network
going to the Coke plant downstream of LD gas enrichment. A new damper shall be provided on fuel
gas duct line.
2.1 PRE-TREATMENT SECTION

BL-101: Blower
Temperature and pressure measurements are provided for the fuel gas upstream and downstream of
the Blower BL-101. A High and Low Temperature & Pressure Alarm in the DCS are provided
upstream of Blower BL-101. Damper is provided in the Blower suction which will be closed as the
Blower stops.
The Blower BL-101 provided with a Variable Speed Drive (VSD) and draws the required quantity
of fuel gas into the CO2 plant by measuring the fuel gas at inlet of Absorber Column T-102.
T-101: SOx/NO2 Scrubbing Column

The fuel gas at around 40 C is contacted with recirculating loop of scrubbing solution for removal of
SOx & NO2. The SOx & NO2 content in the fuel gas is reduced to less than 1 ppmv using scrubbing
solution. Scrubbing Solution Circulation Pump P-101 A/B takes the suction from SOx/NO2
Scrubbing Column sump and pump it to top of the column via Scrubbing Solution Circulation
Cooler E-101 and Scrubbing Solution Filtration Package Z-101. SOx & NO2 in fuel gas will react
with scrubbing agent to form sulfate, sulfite and nitrate salts and increase the conductivity of

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CONTROL AND 2 of 11
OPERATING PROJECT
5 TPD CO2 RECOVERY
PLANT
DOC. NO.
solution. To maintain the conductivity of scrubbing solution the bleed rate at Scrubbing Solution
Circulation Pump P-101 A/B discharge shall be increased. Level in the SOx/NO2 Scrubbing
Column Sump shall be maintained by addition of DM water via level control valve. Due to bleed
and DM water addition pH of scrubbing solution will decrease, which shall be maintained by
addition of scrubbing solution makeup from Scrubbing Solution Tank TK-102 via Scrubbing
Solution Dosing Pump P-111. Caustic Solution Dosing Package Z-103 is provided to manually add
caustic solution as backup for maintaining the pH of the scrubbing solution.
Pressure Differential transmitters with a high alarm in the DCS are provided across the SOx/NO2
Scrubbing Column and Demister to observe the performance of packing and for troubleshooting.
Flow transmitter with high and low alarm is provided to measure circulating scrubbing solution flow
rate.
E-101: Scrubbing Solution Circulation Cooler
The temperature of the Scrubbing Solution at the Scrubbing Solution Circulation Cooler E-101
outlet shall be measured and controlled by a temperature control valve on cooling water return line.
A High Temperature Alarm is provided in the DCS.
Z-101: Scrubbing Solution Filtration Package
It is consisting of two no’s of filters, out of which, one filter will be on standby. The filters are
intended to remove suspended solids (the suspended particulate matter from fuel gas). Differential
pressure (DP) across the filters shall be measured and a High/Low alarm is provided in the DCS.
When the DP across the operating filter reaches the value specified by the vendor the filter shall be
switched over to the standby filter manually and immediate cleaning or replacement of the cartridge
shall be carried out for the exhausted filter.
2.2 ABSORBER COLUMN SECTION

T-102: Absorber Column
The inlet fuel gas temperature, pressure, flow rate and composition shall be measured upstream of
Absorber Column T-102. The fuel gas analyzer shall measure CO2, O2, SO2 and NO2 concentrations
at the absorber inlet. High & Low Flow rate Alarm, Low CO2 alarm, High SO2 & High NO2 alarms
are provided in the DCS. This composition analyzer shall be provided with another channel to

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CONTROL AND 3 of 11
OPERATING PROJECT
5 TPD CO2 RECOVERY
PLANT
DOC. NO.
measure the gas composition at the water wash column (T-103) column outlet. Manual/Automatic
control shall be provided to switch between channels. Sampling points are also provided to sample
and measure the fuel gas composition at the absorber column inlet and water wash column outlet for
cross-checking online analyzer measurements. Gas sampling points at the absorber column inlet and
outlet shall be provided to collect the iso-kinetic samples for measurement of emissions.
A Pressure Differential transmitter with a high alarm in the DCS is provided across each Packing
section and demisters to observe the performance and for troubleshooting.
The level transmitter in the Absorber Column T-102 is provided and any reduction in level (due to
water imbalance in the plant) is controlled by adjusting the DM water makeup to Absorber Column
T-102 sump. The temperature of the fuel gas leaving the Water Wash Column T-103 can be adjusted
to be close to absorber inlet gas temp to minimize the DM water makeup.
If the level in the Absorber Column T-102 increases, it means moisture in the fuel gas is
accumulating in the system. Hence the temperature of the fuel gas at the inlet of the absorber shall
be reduced by 2 to 3 C more than the Water Wash Column T-103 outlet gas temp or the outlet of
the Water Wash Column T-103 shall be increased by 2 to 3 °C more than the fuel gas absorber inlet
temperature in order to reduce water accumulation in the system. The temperature of gas leaving the
Water Wash Column T-103 shall not be more than 45 °C.
Pressure and Temperature Transmitters with high alarms shall be provided on the fuel gas duct at
the outlet of Absorber Column T-102. A flow transmitter is provided for measuring the inlet lean
solvent flow to the Absorber Column T-102.
A Liquid Sampling point is provided at the Rich Solvent Pump P-103 A/B discharge for taking
samples of rich solvent for measuring pH, density and CO2 loading once a day. Safety precautions
should be taken while taking samples and ensure that the plant has reached stable condition.
E-102: Interstage Cooler

Absorption of CO2 with the solvent solution is exothermic reaction. This means that the temperature
of the liquid in the absorption section increases. To remove this heat and maintain the temperature
profile in the absorption section to maximize the absorption, an Interstage cooling system is
provided. The withdrawal for the Interstage cooling section shall be maintained between 60 and 80

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CONTROL AND 4 of 11
OPERATING PROJECT
5 TPD CO2 RECOVERY
PLANT
DOC. NO.
% of the lean solvent flow by using flow controller and a flow control valve at downstream of the
Interstage Cooler E-102.
The temperature of the solvent solution from the Interstage cooler E-102 is controlled between 40
and 45 °C by adjusting the cooling water flow to the coolers. The pressure drop across the Interstage
Cooler E-102 shall be measured using a Pressure Differential Transmitter provided with high alarm.
A provision is provided for sending part of the rich solution from the Interstage Cooler E-102
downstream to the lean solvent line going to the top of the Absorber Column T-102. This is to
maintain the temperature profile in the top packing of the absorption section.
A Liquid Sampling Point is provided at the discharge of the Interstage Cooler E-102 for taking
samples for troubleshooting.
2.3 WATER WASH SECTION

T-103: Water Wash Column
Fuel gas from Absorber Column is sent to Water Wash Column to prevent the solvent emissions
along with gas. The CO2 analyzer shall be provided with another channel to measure the CO2
composition at the Water Wash column outlet.
A Pressure Differential transmitter with a high alarm in the DCS is provided across each Packing
section and demisters to observe the performance and for troubleshooting. The level transmitter in
the Water Wash Column T-103 is provided and level is controlled by adjusting the Water Wash
Condensate to Absorber Column T-102 sump.
One temperature transmitter in each packing section in the Water Wash Column are provided.
Pressure and Temperature Transmitters with high and low alarms shall be provided on the fuel gas
duct at the outlet of Water Wash Column T-103. A flow transmitter is provided for measuring the
circulating water flow to each section of the Water Wash Column T-103. A DM water connection is
provided at each section for initial filling of DM water in the Water Wash Column T-103.
E-108: Water Wash Circulation Cooler-2
The fuel gas to the Water wash Column will be at about 50– 70 °C. To condense the water and
recover the solvent, the fuel gas is cooled with a circulating water loop. The wash water circulation
rate is measured and controlled by a flow transmitter with a flow control valve at downstream of the

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CONTROL AND 5 of 11
OPERATING PROJECT
5 TPD CO2 RECOVERY
PLANT
DOC. NO.
Water Wash Circulation Cooler-2 E-108. The outlet temperature of the wash water in Water Wash
Circulation Cooler-2 E-108 shall be controlled using a temperature controller and adjusting the
cooling water flow. The wash water outlet temperature shall be set between 45 and 50 °C. The
bottom water wash is to recover as much of the solvent as possible so that the top water wash
section will be circulating wash water with lower solvent concentration to minimize the solvent loss.
The pressure drops across the Water Wash Circulation Cooler-2 E-108 shall be measured using a
Pressure Differential Transmitter provided with a high alarm.
E-107: Water Wash Circulation Cooler-1
The wash water circulation rate is measured and controlled by a flow transmitter with a flow control
valve. The outlet temperature of the wash water in Water Wash Circulation Cooler-1 E-107 shall be
controlled using a temperature controller and adjusting the cooling water flow. The wash water
outlet temperature shall be set to less than 40 °C to ensure fuel gas outlet temperature below 40 °C
or less depending on the inlet FG temperature. A temperature difference of 1 to 2 °C shall be
maintained between the inlet and outlet FG temperature to ensure no dilution of the solvent and
minimize the water makeup. The pressure drops across the Water Wash Circulation Cooler-1 E-107
shall be measured using a Pressure Differential Transmitter provided with a high alarm.
2.4 SOLVENT COOLING SECTION

E-103: Lean Rich Exchanger
E-106: Lean Solvent Cooler
The rich solvent from Absorber Column T-102 sump is pumped by Rich Solvent Pump P-103 A/B
to Stripper column after getting heated up in Lean Rich Exchanger E-103. The solvent circulation
rate in the plant is controlled using a flow control valve at the discharge of Rich Solvent Pump P-
103 A/B.
The temperature of the lean solvent at the outlet of the Lean Solvent Cooler E-106 is controlled by
the temperature controller and adjusting the cooling water flow through a control valve in the
cooling water return line from the cooler. The temperature set point shall be about 40°C. The
pressure drop across the coolers shall be measured using a Pressure Differential Transmitter
provided with a high alarm.

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CONTROL AND 6 of 11
OPERATING PROJECT
5 TPD CO2 RECOVERY
PLANT
DOC. NO.
Sampling points are provided downstream of the Lean Solvent Cooler E-106 to measure pH,
density, CO2 loading & moisture content of lean solvent. Samples of lean & rich solvent shall be
taken at the same time once a day for analysis, ensure that the plant has reached stable condition.
2.5 STRIPPER SECTION

T-104: Stripper Column
E-104: Stripper Condenser
V-101: Stripper Reflux Drum
E-105: Stripper Reboiler
V-102: Steam Condensate Drum
The stripper top pressure is maintained at 0.8 to 1 barg using a pressure controller and a pressure
control valve in the CO2 line at the stripper reflux drum V-101 outlet. A PSV set at about 1.5 barg is
provided at the CO2 battery limit to avoid damage to the solvent due to very high temperature.
The temperature of the outgoing vapor from the Stripper Reboiler E-105 is controlled at about 115 –
120 °C using a temperature controller and temperature control valve which adjusts the steam flow to
the Stripper Reboiler to achieve the required CO2 production.
The temperature of the stripper overhead CO2 vapor after the Stripper Condenser E-104 shall be
maintained at about 40 °C. This temperature is controlled by temperature controller and temperature
control valve in the cooling water return line from Stripper Condenser E-104.
Differential Pressure Transmitters with High Alarms are provided for the bottom packing, the top
packing and the demister of the stripper. Temperature transmitters are also provided at the top
packing, bottom packing, Stripper Reboiler inlet, Stripper Reboiler Vapor outlet line, Stripper
Condenser inlet and the CO2 product line. High Temperature Alarms are provided for the Stripper
Reboiler Vapor outlet line and the CO2 product line. A Level Transmitter is provided to check the
level in the Stripper Column T-104 Sump.
The level in the Stripper Reflux Drum V-101 is controlled using a level controller and a level
control valve at the Stripper Reflux Pump P-104 discharge. A provision is made to send the reflux
condensate to the stripper top and also to the absorber column sump.

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OPERATING PROJECT
5 TPD CO2 RECOVERY
PLANT
DOC. NO.
In case solvent carryover is observed downstream of the CO2 plant, the stripper reflux can be sent to
the sump of Absorber Column T-102 instead of Stripper Column T-104.
The level in the Stripper Reboiler E-105 (weir side) is maintained using a level controller and level
control valve on the Lean Solvent Pump P-106 A/B recirculation line.
Pressure, Temperature and Flow Transmitters are provided on the incoming steam supply to the
Stripper Reboiler E-105. Steam Condensate Drum V-102 is provided with a Level Control Valve on
the Steam Condensate Pump P-105 discharge line.
2.6 SOLVENT STORAGE SECTION

TK-101: Solvent Storage Tank
The Solvent Storage Tank TK-101 shall be used for storing first solvent fill / makeup solvent and is
also used for storing the solvent when the plant is taken for maintenance.
Solvent shall be loaded from the Tanker/ Barrel to the Solvent Storage Tank TK-101 using Solvent
Transfer Pump P-110 through the pump recirculation line. During shut down for maintenance, the
entire solvent inventory shall be sent to this tank using Rich Solvent Pump P-103 A/B.
A Level Transmitter is provided for level measurement. Pressure and Temperature Transmitters are
also provided for the tank.
2.7 COOLING WATER NETWORK

The cooling water supply line is provided with a flow transmitter to measure the cooling water
circulation requirement. Temperature Transmitters with high & low alarms are provided on cooling
water supply and return line.
2.8 DEMINERALIZED (DM) WATER NETWORK

DM Water shall be used for following:
• Initial fill of the SOx/NO2 Scrubbing Column T-101 and Water Wash Column T-103.
During normal operation,the level in the SOx/NO2 Scrubbing Column is maintained by

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PLANT
DOC. NO.
addition of DM water. As there is water added along with the scrubbing solution additional
DM water requirement would be very small.
• Maintaining water balance in the CO2 plant.
2.9 SOLVENT TREATMENT SECTION

Z-102: Solvent Treatment Package
The solvent treatment section consists of two parts – the filtration section & the thermal reclaiming
section. These two can be operated independently.
The Filtration Section consists of an activated carbon filter with a duplex of mesh / cartridge filters
(< 5-micron pore size) at the inlet and outlet. The activated carbon filter is meant to remove the high
molecular weight degradation products formed by the solvent. A bleed (about 0.15 m3/ hour) from
the lean solvent line at the Lean Solvent Pump P-106 A/B outlet is taken to the Filtration section.
The filtration package shall be provided with differential pressure measurements with alarms and
this shall be reported to the DCS. When the differential pressure across the filter increases and
reaches the value specified by the filter vendor, the filter shall be by-passed and cleaned. After
cleaning, the filter shall be brought back online. The activated carbon shall be replaced based on the
vendor’s recommendations. Liquid sampling points are provided upstream and downstream of the
filtration section to measure its performance.
In case of a decrease in the CO2 production or a change in the solvent colour, the Heat stable salts
(HSS) content in the solvent shall be measured. The thermal reclaimer system shall be operated to
remove HSS and other contaminants from the solvent if the concentrations are more than 2 wt.%.
This is a vendor package and the operating manual from the vendor should be referred to. A bleed
(about 0.05 m3/ hour) from the lean solvent line at the Lean Solvent Pump P-106 A/B outlet is taken
to the Reclaiming section and, after treatment, the treated solvent is fed back to the Absorber
Column T-102 sump. The thermal reclaimer shall contain a reboiler and condenser and is operated
under vacuum conditions with the temperature ranging from 160 – 180 °C. The solvent is vaporized
in the reboiler (0.6 to 0.8 bara) using a thermic fluid heater or MP Steam and HSS will remain in the
residue. Caustic solution is added to the residue to regenerate the active amine. The vapors from the
reboiler are sent to condenser. Both vapor and liquid from the condenser are routed to the absorber

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PLANT
DOC. NO.
column bottom. The residue will be mixed with DM water before withdrawal and will be disposed
of as hazardous waste.
CAUSE AND EFFECT DIAGRAM

The following interlocks will be made available in the unit.
No. Interlock No. Caused by Description of Cause Effect
1 I-101 TAHH-1102 High High Fuel Gas Trip Blower BL-101

Temperature at SOx/NOx Close Damper at Fuel gas
Scrubbing Column outlet battery limit
2 I-102 AAHH- High High SO2 concentration at Trip Blower BL-101
1101 Absorber Inlet Close Damper at Fuel gas
battery limit
3 I-103 LALL-1102 Low Low Level in SOx/NOx Trip Scrubbing Solution
Scrubbing Column T-101 Sump Circulation Pump P-101 A/B
4 I-104 LALL-1104 Low Low Level in Scrubbing Trip Scrubbing Solution
Solution Tank TK-102 Dosing Pump P-111
5 I-201 LALL-2101 Low Low Level in Absorber Trip Rich Solvent Pump P-
Column T-102 Sump 103 A/B
6 I-202 FALL-2101 Low Low Flow of Lean Solvent Trip Interstage Pump P-102
to Absorber T-102
7 I-401 LALL-4105 Low Low Level in Stripper Trip Lean Solvent Pump P-
Reboiler E-105 sump 106 A/B
8 I-402 LALL-4103 Low Low Level in Stripper Trip Stripper Reflux Pump
Reflux Drum V-101 P-104
9 I-403 LALL-4107 Low Low Level in Steam Trip Steam Condensate
Condensate Drum V-102 Pump P-105
STARTUP, SHUTDOWN PROCEDURE:

4.1 Startup Sequence.
1. After successful hydro test, pre-commissioning, water run, and all checks/inspections performed
the following steps shall be followed for starting the plant.
2. The CDRMax® Solution shall be unloaded into Solvent Storage Tank (TK-101) from the Tanker
for first fill using Solvent Transfer Pump P-110.
3. Start the instrumentation air, DM water and cooling water to plant.

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DOC. NO.
4. DM water shall be added to SOx/NO2 Scrubbing Column T-101 until level reaches 100% in
Column. After the level reaches 100%, start the Scrubbing Solution Circulation Pump P-101
A/B.
5. Fill the Water Wash Column T-103, Water wash section top & bottom collectors and suction
lines of pumps P-107 & P-108 with DM water till a level is observed in the column sump. Start
the pumps P-107 & P-108 and keep it in circulation mode. Drain the additional water in column
sump.
6. Load the solvent to the Absorber Column through Solvent Transfer Pump P-110. Once the level
reaches 100%, start the rich solvent pump P-103 to send the solvent to the Stripper Column T-
104 & Stripper Reboiler E-105 through lean rich exchanger E-103.
7. Once enough level is reached in the Stripper Reboiler E-105, start the Lean Solvent Pump P-106
to send the solvent back to Absorber Column T-102 via Lean& Rich exchanger E-103 and Lean
Solvent Cooler E-106.
8. Start interstage pump P-102 and start circulating the solvent in the loops.
9. Change all the level and flow controllers to auto-mode once all the levels and flows are normal.
10. Keep the liquid circulation for about 30 min to ensure all levels and flows are maintained.
11. Start the steam flow to the reboiler with 2 C increase in temperature per min till it reaches about
100 C.
12. Start BL-101 and adjust the control valve/ near the gas network to get about required fuel gas
into the system.
13. Adjust the LP Steam supply to Reboiler to get the required CO2 production & set PCV-4106 in
CO2 Product line to 1 barg to obtain desired CO2 Production. Start the Stripper Reflux Pump
once enough level is reached in Stripper Reflux Drum V-101
4.2 Normal Shutdown Sequence:
1. Shutoff the steam supply to Reboiler E-105 by taking Stripper Reboiler temperature controller to
manual mode and closing the control valve.
2. Trip the blower to stop fuel gas inlet to SOx/NO2 Scrubbing Column/ Absorber Column.
3. Stop DM Water supply to SOx/NO2 Scrubbing Column.

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DOC. NO.
4. Stop Scrubbing Solution Circulation Pumps. If SOx/NO2 Scrubbing Column requires

maintenance, drain the liquid otherwise retain it in Column.
5. Maintain the circulation of CDRMax® Solvent in plant until the rich solvent temperature reaches
below 40 C.
6. After rich solvent temperature reaches below 40 C, divert rich solvent discharge from Rich
Solvent Pump P-103A/B to Solvent Storage Tank TK-101 instead of Stripper Column T-104.
7. Open the valve connecting drain of Reboiler to Lean Solvent Pump Suction. Keep the Reboiler
Level Control Valve in Manual mode & set the opening to 0%.
8. Once the Reboiler is entirely emptied of CDRMax® Solution, stop Lean Solvent Pump P-106
A/B and Interstage pumps P-102.
9. Stop the Stripper Reflux pump P-104 once the solution Stripper Reflux drum V-101 is emptied.
10. Once the Absorber is emptied, stop Rich Solvent Pump P-103 A/B.
11. Start draining the DM water from Water Wash circulation Pumps 1 & 2 suction lines and stop it
once collectors are emptied.
12. Stop Cooling Water Supply.
13. Plant is now under shutdown.
4.3 Emergency Shutdown Sequence:

1. Shutoff the steam supply to Reboiler E-105 by taking Stripper Reboiler temperature controller to
manual mode and closing the control valve.
2. The ID fan BL-101 shall be tripped
3. Stop all pumps.
4. The DM water and Cooling Water shall be stopped
The detailed operating procedures along with startup and shutdown procedures will be provided in
the operating manual during Detail Engineering.

LICENSOR
CUSTOMER INSTRUMENTATION SUMMARY

PROJECT NAME 5TPD CO2 RECOVERY PLANT
DOC. NO. TSL-IS-302
INSTRUMENTATION SUMMARY

This document is a property of Carbon Clean Solutions Limited and it cannot be reproduced or communicated to any third party without prior written consent of Carbon
Clean Solutions Limited.
LICENSOR
CUSTOMER INSTRUMENTATION SUMMARY PROJECT NAME

5TPD SKID MOUNTED PLANT
DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
TAG NO SERVICE COMPONENTS TYPE UNIT REMARKS
NO HH H L LL MIN. MAX COUNT
TSL-PID-301: P&ID FOR PRETREATMENT SECTION

Fuel Gas to Absorber Column T-
AIT-1101A CO2 Analyzer Y 0 40 vol % 1
102 Online Analyzer. IR AIT-1101B SO2 Analyzer Y 0 500 ppmv 1
type/Electrochemical sensors. Two AIT-1101C O2 Analyzer Y 0 21 vol% 1
1 AIT-1101
channels, Manual Swichover to
measure the WW outlet AIT-1101D NO2 Analyzer Y 0 50 ppmv 1
composition
Bleed from Scrubbing Solution
2 AIT-1102 AIT-1102 Conductivity Analyzer Y Y 0 1,00,000 µS/cm2 1
Circulation Pump P-101 discharge
Scrubbing Solution to SOx/NO2
3 AIT-1103 AIT-1103 pH Analyzer Y Y 0 12 - 1
Scrubbing Column T-101
4 FIT-1101 FIT-1101 Ultrasonic Flow Transmitter Y Y 0 2000 Nm3/hr 1
102
Scrubbing Solution Circulation
5 FIT-1102 FIT-1102 Magnetic Flow Transmitter Y Y 0 7 m3/hr 1
Pump P-101A/B discharge
Bleed from Scrubbing Solution
Circulation Pump P-113 discharge
SOx/NO2 Scrubbing Column T-101
7 LI-1101 LI-1101 Level Indicator 0.1 4 m 0
Sump
8 LIT-1102 LIT-1102 Diaph. Seal Diff. Level Transmitter Y Y 0.1 4 m 2
Sump
9 LIT-1104 Scrubbing Solution Tank TK-102 LIT-1104 Diaph. Seal Diff. Level Transmitter Y Y 0.1 4 m 2
10 PIT-1111 Fuel Gas at battery limit PIT-1111 Diaph. Seal Pressure Transmitter Y Y 0 1000 mmWC 1
11 PIT-1113 Blower BL-101 Discharge PIT-1113 Diaph. Seal Pressure Transmitter Y Y 0 2000 mmWC 1
12 PI-1106 Blower BL-101 Discharge PI-1106 Diaph. Seal Pressure Indicator 0 2000 mmWC 0
13 PDIT-1101 PDIT-1101 Diaph. Seal Diff. Pressure Transmitter Y 0 1000 mmWC 1
Packing
Demister
Fuel Gas at Absorber Column T-
15 PIT-1103 PIT-1103 Diaph. Seal Pressure Transmitter Y Y 0 2000 mmWC 1
102 inlet
16 PI-1104 PI-1104 Diaph. Seal Pressure Indicator 0 2 barg 0
Pump P-101A/B suction
Pump P-101A/B discharge
18 PDIT-1108 PDIT-1108 Diaph. Seal Diff. Pressure Transmitter Y Y 0 2 bar 1
Cooler E-101
Scrubbing Solution Filtration
Package Z-101
Scrubbing Solution Dosing Pump P-
111 suction
This document is a property of Carbon Clean Solutions Limited and it cannot be reproduced or communicated to any third party without prior written consent of
Carbon Clean Solutions Limited. Page 1 of 20
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
Scrubbing Solution Dosing Pump P-
111 discharge
22 PIT-1115 Scrubbing Solution Tank TK-102 PIT-1115 Diaph. Seal Pressure Indicator -100 200 mmWC 1
23 TIT-1107 Fuel Gas at battery limit TIT-1107 Temperature Transmitter Y Y 0 120 °C 1
Fuel Gas at Blower BL-101
24 TIT-1108 TIT-1108 Temperature Transmitter Y Y 0 120 °C 1
discharge
SOx NO2 Scrubbing Column T-101
25 TIT-1101 TIT-1101 Temperature Transmitter 0 120 °C 1
Packing
102
Scrubbing Solution at Scrubbing
27 TI-1103 Solution Circulation Cooler E-101 TI-1103 Temperature Indicator 0 120 °C 0
inlet
Scrubbing Solution at Scrubbing
28 TIT-1104 Solution Circulation Cooler E-101 TIT-1104 Temperature Transmitter Y 0 75 °C 1
outlet
Cooling Water at Scrubbing
29 TI-1105 Solution Circulation Cooler E-101 TI-1105 Temperature Indicator 0 70 °C 0
outlet
Scrubbing Solution Tank TK-102
30 TIT-1106 TIT-1106 Temperature Transmitter Y 0 75 °C 1
outlet
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
TSL-PID-302: P&ID FOR ABSORPTION COLUMN SECTION
Lean Solvent to Absorber Column T-
1 FIT-2101 FIT-2101 Magnetic Flow Transmitter Y Y Y 0 5 m3/hr 1
102
3
2 FIT-2102 Interstage Pump P-102 discharge FIT-2102 Magnetic Flow Transmitter Y Y 0 5 m /hr 1
3 LIT-2101 Absorber Column T-102 Sump LIT-2101 Diaph. Seal Diff. Level Transmitter Y Y Y 0 3 m 2
4 LI-2102 Absorber Column T-102 Sump LI-2102 Level Indicator 0 3 m 0
Absorber Column T-102 Bottom
Packing
Absorber Column T-102 Top
Packing
7 PDIT-2103 Absorber Column T-102 Demister PDIT-2103 Diaph. Seal Diff. Pressure Transmitter Y 0 1000 mmWC 1
Fuel Gas from Absorber Column T-
8 PIT-2103 PIT-2103 Diaph. Seal Pressure Transmitter Y Y 0 100 mmWC 1
102 to Water wash Column
T-102 Interstage Pump P-102
suction
T-102 Interstage Pumps P-102
discharge
11 PDIT-2108 Interstage Cooler E-102 PDIT-2108 Diaph. Seal Diff. Pressure Transmitter Y Y 0 2000 mmWc 1
Absorber Column T-102 Above
Bottom Packing
Absorber Column T-102 Top
Packing
Absorber Column T-102 Fuel gas
14 TIT-2104 temperature to Water Wash Column TIT-2104 Temperature Transmitter Y Y 0 80 °C 1
T-103
Solvent inlet to Insterstage Cooler E-
15 TI-2105 TI-2105 Temperature Indicator 0 80 °C 0
102
Solvent outlet from Insterstage
Cooler E-102
Cooling water outlet from
Insterstage Cooler E-102
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
TSL-PID-303: P&ID FOR SOLVENT COOLING SECTION
Rich Solvent from Absorber
Column T-102
Rich Solvent Pump P-103A/B
suction
Rich Solvent Pump P-103A/B
discharge
Rich Solvent across Lean Rich
Exchanger E-105
Rich Solvent at Lean Rich
5 PIT-3106 PIT-3106 Diaph. Seal Pressure Transmitter Y Y 0 10 barg 1
Exchanger E-103 outlet
Lean Solvent across Lean Rich
Exchanger E-103
Lean Solvent across Lean Solvent
Cooler E-106
Lean Solvent at Lean Solvent
Cooler E-106 outlet
Rich Solvent outlet from Absorber
Column T-102
Rich Solvent outlet from Lean Rich
Exchanger E-103
Lean Solvent inlet to Lean Rich
Exchanger E-103
Lean Solvent outlet from Lean Rich
Exchanger E-103
Lean Solvent outlet from Lean
Solvent Cooler E-106
Cooling Water outlet from Lean
Lean Solvent outlet from Lean
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
TSL-PID-304: P&ID FOR STRIPPING SECTION
with Totalizer
1 FIT-4101 Steam to Reboiler E-105 FIT-4101 Orifice Flow Transmitter Y Y 0 500 kg/h 2
function
with Totalizer
2 FIT-4102 CO2 at battery limits FIT-4102 Coriolis Mass Flow Transmitter Y Y 0 500 kg/h 2
function
3 LIT-4101 Stripper Column T-104 Sump LIT-4101 Diaph. Seal Diff. Level Transmitter Y Y 0 2 m 1
5 LIT-4103 Stripper Reflux Drum V-101 LIT-4103 Diaph. Seal Diff. Level Transmitter Y Y Y 0 2 m 2
6 LI-4104 Stripper Reboiler E-105 LI-4104 Level Indicator 0 1.5 m 0
7 LIT-4105 Stripper Reboiler E-105 LIT-4105 Diaph. Seal Diff. Level Transmitter Y Y Y 0 1.5 m 2
9 LIT-4107 Steam Condensate Drum V-102 LIT-4107 Diaph. Seal Diff. Level Transmitter Y Y Y 0 2 m 2
10 PIT-4101 Stripper Column T-104 sump PIT-4101 Diaph. Seal Pressure Transmitter 0 2 barg 1
Stripper Column T-104 Bottom
Packing
Stripper Column T-104 Top
Packing
13 PDIT-4104 Stripper Column T-104 Demister PDIT-4104 Diaph. Seal Diff. Pressure Transmitter Y 0 2000 mmWC 1
14 PIT-4105 Stripper Column T-104 PIT-4105 Diaph. Seal Pressure Transmitter Y 0 2 barg 2
15 PIT-4106 Stripper Column T-104 PIT-4106 Diaph. Seal Pressure Transmitter Y Y 0 2 barg 1
Stripper Reflux Drum V-101
Demister
CO2 at Stripper Reflux Drum V-
17 PIT-4108 PIT-4108 Diaph. Seal Pressure Transmitter 0 2 barg 1
101 outlet
18 PIT-4109 CO2 Battery Limit Pressure PIT-4109 Diaph. Seal Pressure Transmitter Y 0 2 barg 1
Stripper Reflux Pump P-104
suction
discharge
21 PI-4114 Stripper Reboiler E-105 Shell Side PI-4114 Diaph. Seal Pressure Indicator 0 3 barg 0
Solvent & CO2 vapors from
Stripper Reboiler E-105 outlet
Lean Solvent Pump P-106A/B
suction
Lean Solvent Pump P-106A/B
discharge
25 PIT-4120 LP Steam battery limit PIT-4120 Diaph. Seal Pressure Transmitter Y 0 5 barg 1
LP Steam at Stripper Reboiler E-
26 PIT-4121 PIT-4121 Diaph. Seal Pressure Transmitter Y 0 5 barg 1
105 inlet
27 PI-4122 Steam Condensate Drum V-102 PI-4122 Diaph. Seal Pressure Indicator 0 10 barg 0
Steam Condensate Pump P-105
suction
Steam Condensate Drum P-105
discharge
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
30 TIT-4101 Stripper Column T-104 sump TIT-4101 Temperature Transmitter Y 0 150 °C 1
Stripper Column T-104 Bottom
Packing
Stripper Column T-103 Top
Packing
33 TIT-4104 Stripper top to Condensor E-104 TIT-4104 Temperature Transmitter Y Y 0 150 °C 1
CO2 Vapor outlet from Stripper
Condensor E-104
Cooling Water outlet from Stripper
Condensor E-104
36 TIT-4107 CO2 vapor at Battery Limits TIT-4107 Temperature Transmitter Y Y 0 80 °C 1
discharge
Solvent inlet to Stripper Reboiler E-
105
Solvent inlet to Stripper Reboiler E-
39 TI-4110 TI-4110 Temperature Transmitter 0 150 °C 0
105
Vapor outlet from Stripper Reboiler
E-105
LP Steam inlet to Stripper Reboiler
E-105
Steam Condensate Drum V-102
outlet
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
TSL-PID-305: P&ID FOR SOLVENT STORAGE SECTION
1 LIT-5101 Solvent Storage Tank TK-101 LIT-5101 Diaph. Seal Diff. Level Transmitter Y Y 0 3 m 1
Solvent Transfer Pump P-110
suction
Solvent Transfer Pump P-110
discharge
4 PI-5104 Solvent Storage Tank TK-101 PI-5104 Diaph. Seal Pressure Indicator 0 10 barg 0
5 TIT-5101 Solvent Storage Tank TK-101 TIT-5101 Temperature Transmitter Y Y 0 70 °C 1
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
TSL-PID-306: P&ID FOR COOLING WATER NETWORK
Cooling Water Supply at Battery
1 FIT-6101 FIT-6101 Orifice Flow Transmitter Y Y 0 300 m3/hr 1
Limits
Cooling Water Supply at Battery
Limits
Cooling Water Return at Battery
Limits
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
TSL-PID-307: P&ID FOR DM WATER NETWORK
1 PIT-7101 DM Water at battery limits PIT-7101 Pressure Transmitter 0 5 barg 1
2 TIT-7101 DM Water at battery limits TIT-7101 Temperature Transmitter Y Y 0 60 °C 1
TSL-PID-308: P&ID FOR WATER WASH SECTION
1 AIT-8101 Depleted Fuel Gas at Battery Limit AIT-8101 CO2 Analyzer 0 10 vol % 1
Water Wash Circulation Cooler-2 3
2 FIT-8102 FIT-8102 Magnetic Flow Transmitter Y Y 0 5 m /hr 1
discharge
Water Wash Circulation Cooler-1
discharge
4 LIT-8102 Water Wash Column T-103 Sump LIT-8102 Diaph. Seal Diff. Level Transmitter Y Y Y 0 2 m 2
5 LI-8101 Water Wash Column T-103 Sump LI-8101 Level Indicator 0 2 m 0
Water Wash Column T-103 Bottom
Packing
Water Wash Column T-103 Top
Packing
Water Wash Column T-103
Demister
Water Wash Circulation Pump-2 P-
108 suction
108 discharge
107 suction
107 discharge
13 PIT-8104 Depleted Fuel Gas at Battery Limit PIT-8104 Pressure Transmitter Y Y 0 1000 mmWc 1
Water Wash Condensate Pump P-
109 suction
Water Wash Condensate Pump P-
109 discharge
Water Wash Circulation Cooler-2 E-
108
Water Wash Circulation Cooler-1 E-
107
18 TIT-8102 Water Wash Column T-103 Sump TIT-8102 Temperature Transmitter 0 80 °C 1
Water Wash Column T-103 Bottom
Packing
Water Wash Column T-103 Top
Packing
21 TIT-8105 Depleted Fuel Gas at Battery Limit TIT-8105 Temperature Transmitter Y Y 0 80 °C 1
Water wash inlet to Water Wash
Circulation Cooler-2 E-108
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
Water wash inlet to Water Wash
23 TI-8111 TI-8111 Temperature Transmitter Y Y 0 80 °C 0
Circulation Cooler-1 E-107
Cooling water outlet from Water
Wash Circulation Cooler-2 E-108
Water wash outlet from Water
Water wash outlet from Water
Cooling water outlet from Water
LICENSOR

DOC. NO. TSL-IS-302

S. Alarm RANGE I/O
I/O COUNT
Sub-Total 108
Control Valves x 18 (4 Nos Each) 72
Pumps x 14 28
Blower x 1 2
Solvent Treatment Package 4
Total 214
Margin @ 20 % 43
Total I/O Count with margin 257
LICENSOR
DOC. NO. TSL-IS-302
S. Non- Corrosive/ Differential Design P, Line Size,
TAG NO SERVICE P&ID No. Fail Safe Design T, °C REMARKS
NO Corrosive Pressure, bar barg mm
LIST OF CONTROL VALVES

1 ACV-1102 Scrubbing Solution Bleed TSL-PID-301 Fail Close Non-Corrosive 0.8 8.8 75 25
2 LCV-1102 DM Water TSL-PID-301 Fail Close Non-Corrosive 0.8 5 75 25
3 ACV-1103 Scrubbing Solution TSL-PID-301 Fail Close Non-Corrosive 0.8 8.8 75 25
4 TCV-1104 Cooling Water TSL-PID-301 Fail Open Non-Corrosive 0.8 7.8 65 25
5 LCV-2101 DM Water TSL-PID-302 Fail Close Non-Corrosive 0.8 5 65 25
6 FCV-2102 Interstage Solvent TSL-PID-302 Fail Open Corrosive 0.8 6.8 75 40
8 FCV-3101 Rich Solvent TSL-PID-303 Fail Open Corrosive 0.8 8.5 75 40
10 LCV-4103 Stripper Reflux TSL-PID-304 Fail Open Corrosive 0.8 9.2 150 25
11 LCV-4105 Lean Solvent TSL-PID-304 Fail Close Corrosive 0.8 10 150 40
12 LCV-4107 Steam Condensate TSL-PID-304 Fail Open Non-Corrosive 0.8 10 180 25 IBR Certified
14 PCV-4106 Product CO2 TSL-PID-304 Fail Close Corrosive 0.2 3.5 65 50
15 TCV-4111 LP Steam TSL-PID-304 Fail Close Non-Corrosive 0.2 4.5 180 80 IBR Certified
Carbon Clean Solutions Limited.
LICENSOR

DOC. NO. TSL-IS-302
LIST OF PRESSURE SAFETY VALVES
1 PSV-4102 CO2 + Solvent +Water TSL-PID-304 High High Stripper Pressure Non- Fire 1.4 65 1 Reliving Rate: 400 kg/hr
Carbon Clean Solutions Limited.
CUSTOMER PROJECT 5 TPD CO2 RECOVERY PLANT
EQUIPMENT LIST
DOC. NO. TSL-EL-400
LICENSOR
REV. NO. 0 PAGE 1 of 4

INTRODUCTION
This document specifies list of equipment’s along with their basic information for the proposed CDRMax Technology for capture of CO2 from the fuel gas of the TATA Steel plant in Jamshedpur, Jharkhand. This document
shall be read in conjunction with Process flow diagram bearing document No. TSL-PFD-201.
COLUMNS
Medium Remarks
Internal Pressure, barg Temperature, °C Packing MOC
S. Equipment Height,
Tag No. Type Capacity Diameter Height, Packing Type
No. Name m
,m Operating Design Operating Design m Column Packing
1 T-101 SOx/ NO2 Packed 1x100% 0.4 11.0 Atm 0.4 & 40-50 70 5mx1 Intalox Ultra High SS304L SS304L Fuel Gas, Note 1
Scrubbing Column HV Performance/ Scrubbing
Column Equivalent Solution
2 T-102 Absorber Packed 1x100% 0.4 19.0 Atm 0.4 & 40-80 110 6mx2 Mellapak Plus 252Y/ SS304L SS304L Fuel Gas, Note 1
Column Column HV Flexipac 250Y HC Solvent
3 T-103 Water Wash Packed 1x100% 0.35 14.0 Atm 0.4 & 40-70 110 3mx2 Mellapak Plus 252Y/ SS304L SS304L Fuel Gas, Note 1
Column Column HV Flexipac 250Y HC Circulating
Water
3 T-104 Stripper Packed 1x100% 0.3 15 1 3.5 & 80-120 160 4mx2 Mellapak Plus 252Y/ SS304L SS304L CO2, Solvent Note 1
Column Column FV Flexipac 2Y HC Solution
PUMPS
S. Tag No. Equipment Name Type Capacity Each Unit Differential Discharge Design Temperature, °C MOC Medium Estimated Remarks
C: Continuous
I: Intermittent
No. Rated Flow Pressure, Pressure, Pressure absorbed
Operation
Rate, bar barg barg Power
m3/hr Operating Design Casing Impeller Requirement
per pump
(kW)
1 P-101 A/B Scrubbing Solution Centrifugal 2 x 100 % 4.3 4.3 4.8 6 40 70 SS304 SS304 Circulating 0.67 C
Circulation Pump Scrubbing Solution
2 P-102 Interstage Pump Centrifugal 1 x 100 % 2.1 2.7 4 5 55 85 SS304 SS304 Solvent 0.21 C
3 P-103 A/B Rich Solvent Pump Centrifugal 2 x 100 % 2.6 5.8 6.2 8.3 44 75 SS304 SS304 Solvent 0.56 C
4 P-104 Stripper Reflux Centrifugal 1 x 100 % 0.1 3.5 4.8 8.3 40 160 SS304 SS304 Reflux condensate 0.01 C
Pump
5 P-105 Steam Condensate Centrifugal 1 x 100 % 0.6 3.3 6.6 9.7 140 160 SS304 SS304 Steam Condensate 0.07 C
Pump
6 P-106 A/B Lean Solvent Pump Centrifugal 2 x 100 % 2.8 4.4 5.9 9.7 123 160 SS304 SS304 Solvent 0.44 C
7 P-107 Water Wash Centrifugal 1 x 100 % 2.15 2.7 3.7 4.8 53 85 SS304 SS304 Wash Water 0.22 C
Circulation Pump -1

This document is a property of Carbon Clean Solutions Limited and it cannot be reproduced or communicated to any third party without prior written consent of Carbon Clean Solutions Limited.
EQUIPMENT LIST
DOC. NO. TSL-EL-400
LICENSOR

S. Tag No. Equipment Name Type Capacity Each Unit Differential Discharge Design Temperature, °C MOC Medium Estimated Remarks
C: Continuous
I: Intermittent
No. Rated Flow Pressure, Pressure, Pressure absorbed
Operation
Rate, bar barg barg Power
m3/hr Operating Design Casing Impeller Requirement
per pump
(kW)
8 P-108 Water Wash Centrifugal 1 x 100 % 2.35 3.2 3.5 4.7 65 95 SS304 SS304 Wash Water 0.29 C
Circulation Pump -2
9 P-109 WW Condensate Centrifugal 1 x 100 % 0.13 2 2.4 3.4 65 95 SS304 SS304 Wash Water 0.01 C
Pump
10 P-110 Solvent Transfer Centrifugal 1 x 100 % 1.2 1.7 1.8 2.5 40 70 SS304 SS304 Solvent Solution 0.08 I
Pump
11 P-111 Scrubbing Solution Centrifugal 1 x 100 % 0.12 3.3 3.8 4.5 40 70 SS304 SS304 Scrubbing Solution 0.015 C
Dosing Pump
BLOWER
S. Tag No. Equipment Type Capacity Each Unit Differential Discharge Design Temperature, °C MOC Medium Estimated Operation Remarks
No. Name Rated Flow Pressure, Pressure, Pressure Power C: Continuous
Rate, bar barg barg Operating Design Casing Impeller Requirement I: Intermittent
NCMH per blower,
kW
1 BL-101 ID Fan Centrifugal 1 x 100 % 715 0.1305 0.1305 0.5 40 75 SS304 SS304 Fuel Gas 3.85 C
HEAT EXCHANGERS
S. Tag No. Equipment Name Type Capacity Design Heat Surface Pressure, bar g Temperature, °C MOC Medium Remarks
No. Duty, MJ/hr Area, m2 Inlet Outlet Design Inlet Outlet Design
1 E-101 Scrubbing Solution Plate Heat 1 x 100% 55 VTA Hot Side 4.8 3.8 6 43 40 70 SS304 Scrubbing Solution
Circulation Cooler Exchanger Cold Side 4 3.5 7.0 30 38 65 Cooling Water
2 E-102 Interstage Cooler Plate Heat 1 x 100% 81.7 VTA Hot Side 4 3 5 53 40 85 SS304 Solvent
Exchanger Cold Side 4 3.5 7.0 30 38 65 Cooling Water
3 E-103 Lean Rich Exchanger Plate Heat 1 x 100% 663 VTA Hot Side 6 5 10 122.2 48 160 SS304 Solvent
Exchanger Cold Side 6.2 5.2 8.3 44 110 120 Solvent
4 E-104 Stripper Condenser Shell & 1 x 100% 248 17 Shell 1 0.9 3.5/FV 101.8 40 160 SS304 CO2 Vapor Note 1
Tube Tube 4 3.5 7.0 30 38 65 Cooling Water
5 E-105 Stripper Reboiler Kettle type 1 x 100% 720 17.5 Shell 1.1 1 3.5/FV 121 122.4 150 SS304 Solvent Note 1
Tube 3 2.9 4.5/FV 140 140 160 LP Steam

EQUIPMENT LIST
DOC. NO. TSL-EL-400
LICENSOR

S. Tag No. Equipment Name Type Capacity Design Heat Surface Pressure, bar g Temperature, °C MOC Medium Remarks
No. Duty, MJ/hr Area, m2 Inlet Outlet Design Inlet Outlet Design
6 E-106 Lean Solvent Cooler Plate Heat 1 x 100% 98.8 VTA Hot Side 5 4 10 51.5 40 120 SS304 Solvent
Exchanger Cold Side 4 3.5 7.0 30 38 65 SS304 Cooling Water
7 E-107 Water Wash Circulation Plate Heat 1 x 100% 105.1 VTA Hot Side 3.7 2.7 5.0 51.5 39 85 SS304 Wash Water
Cooler-1 Exchanger Cold Side 4 3.5 7.0 30 38 65 Cooling Water
8 E-108 Water Wash Circulation Plate Heat 1 x 100% 190 VTA Hot Side 3.5 2.5 5.0 64.8 45 95 SS304 Wash Water
Cooler-2 Exchanger Cold Side 4 3.5 7.0 30 38 65 Cooling Water
TANKS
S. Tag No. Equipment Name Type Capacity Operating Internal Height, Operating Operating Design Design MOC Medium Remarks
No. Volume, m3 Diameter, m Pressure, Temperature, Pressure, bar Temperature,
m bar g °C g °C
1 TK-101 Solvent Storage Vertical 1 x 100% 1.9 1.3 2.6 Atm 40 0.08 65 SS304L Solvent
Tank
2 TK-102 Scrubbing Vertical 1 x 100% 0.28 0.6 1.0 Atm 40 0.08 65 SS304L Solvent
Solution Tank
VESSELS
S. Tag No. Equipment Name Type Capacity Internal Height, Operating Operating Design Design MOC Medium Remarks
No. Diameter, m Pressure, Temperature, Pressure, Temperature,
m bar g °C bar g °C
1 V-101 Stripper Reflux Drum Vertical 1 x 100% 0.3 2.6 1 40 3.5/FV 160 SS304L CO2, Note 1
Solvent
2 V-102 Steam Condensate Drum Vertical 1 x 100% 0.3 2.65 3 140 4.5/FV 180 CS + Steam , Note 1
3mm CA condensate

EQUIPMENT LIST
DOC. NO. TSL-EL-400
LICENSOR

PACKAGES
S. Tag No. Equipment Name Capacity Details Design Design MOC Estimated Remarks
No. Pressure, Temperature, absorbed Power
bar g °C Requirement, kW
1 Z-101 Scrubbing Solution Filtration 1 x 100% Cartridge Type Filters (2 x 100 %) 6 70 SS304L -
Package Each Filter Flow rate: 4.3 m3/hr
2 Z-102 Solvent Treatment Package 1 x 100% Thermal Reclaimer: 0.05 m3/hr 10/FV 250 SS304/SS316 3 (Intermittent) Note 1
3 Z-103 Caustic Solution Dosing Package 1 x 100% 200 litres tank of SS304 and a 200 litres/hr pump
NOTES
1. FV- Full Vacuum, HV – Half Vacuum
2. VTA: Vendor to advise

CUSTOMER
PAGE
PROCESS DATA SHEET LICENSOR
1 of 1
BLOWER PROJECT
5 TPD CO2 RECOVERY
PLANT
(BL-101) TSL-PDS-BL-101
DOC. NO.

Tag No. BL-101 Description Blower
Capacity 1 x 100 % Type of Fan Centrifugal
Fluid Conditions
Fluid Fuel gas
Operating Temperature 40 °C
Viscosity at operating temperature 0.02 cP at 40 C
Density at operating temperature 1.13 kg/m3 at 40 C
Molecular Weight 28.94
Presence of solid components No
Each Fan Flow rate Normal 650 Nm3/hr
Maximum 715 Nm3/hr
Minimum 600 Nm3/hr
Suction Pressure 0.0 bar g
Discharge Pressure 0.1305 bar g
Differential Pressure 0.1305 bar
Design Temperature 75 °C
Operation Continuous
Mechanical Data
Material of Construction
Casing SS304
Impeller SS304
Shaft SS304
Design Code ISO 12759
Noise Level <85 dB(A) at 1 meter distance
Motor Details
Power Supply 6.6 kV / 50 Hz , 3 phase
Standard IS 325; IS 12615/IEC 60034
Type Industrial
VSD Required (Yes/No) Yes
Estimated Absorbed Power for each fan 3.85 kW
NOTES
1.

CUSTOMER
PROCESS DATA SHEET PAGE
LICENSOR
1 of 1
SCRUBBING SOLUTION 5 TPD CO2 RECOVERY
CIRCULATION COOLER PROJECT PLANT
(E-101) DOC. NO. TSL-PDS-E-101

Tag No. E-101 No. of Unit 1 Description Scrubbing Solution Circulation Cooler
Performance of Each Unit
Fluid Conditions Hot Side Cold Side
Fluid Scrubbing Solution Cooling Water
In Out In Out
Operating Temperature 43 40 30 38 °C
Operating Pressure 4.8 3.8 4 3.5 bar g
Liquid Properties
Normal Flow Rate 3517 3517 1316 1316 kg/hr
Density 991 992 995.5 992.4 kg/m3
Viscosity 0.621 0.658 0.781 0.653 cP
Specific Heat 4.18 4.179 4.179 4.178 kJ/kg °C
Thermal Conductivity 0.622 0.619 0.617 0.629 W/mK
Vapor Properties
Normal Flow Rate kg/hr
Density kg/m3
Viscosity cP
Specific Heat kJ/kg °C
Thermal Conductivity W/mK
Design Heat Duty 55100 kJ/hr
Allowable Pressure Drop @ Design Cond. 1 0.5 bar
Heating/Cooling Curve Data Attached No No
Over Capacity Factors
Flow 25 %
Duty 25 %
Design Pressure 6 7 bar g
Design Temperature 70 65 °C
Heat Transfer Plates SS304
Frame SS304
Gaskets EPDM – Peroxide Cured
Design Code ASME Section VIII
NOTES
1 Design heat duty is inclusive of overcapacity factor

CUSTOMER PROCESS DATA SHEET PAGE
LICENSOR
1 of 1
INTERSTAGE 5 TPD CO2 RECOVERY
COOLER PROJECT PLANT

Tag No. E-102 No. of Unit 1 Description Interstage Cooler
Fluid Solvent Solution Cooling Water
In Out In Out
Operating Temperature 53 40 30 38 °C
Operating Pressure 4 3 4 3.5 bar g
Liquid Properties
Density 1108 1118 995.5 992.4 kg/m3
Viscosity 2.928 4.695 0.781 0.653 cP
Vapor Properties
Density kg/m3
Viscosity cP
Allowable Pressure Drop @ Design Cond. 0.8 0.5 bar
Flow 15 %
Duty 15 %
Frame SS304
NOTES
1 Design heat duty is inclusive of overcapacity factor

LICENSOR
1 of 3
LEAN RICH 5 TPD CO2 RECOVERY
EXCHANGER PROJECT PLANT

Tag No. E-103 No. of Unit 1 Description Lean Rich Exchanger
Fluid Lean Solvent Rich Solvent
In Out In Out
Operating Temperature 122.5 48 44 110 °C
Operating Pressure 6.0 5.0 6.2 5.2 bar g
Liquid Properties
Design Flow Rate 2570 2570 2785 2737 kg/hr
Density 1106 1024.5 1106 1030 kg/m3
Viscosity 0.451 2.224 4.14 0.74 cP
Vapor Properties
Design Flow Rate 48 kg/hr
Density 4.52 kg/m3
Viscosity 0.0175 cP
Specific Heat 1.11 kJ/kg °C
Thermal Conductivity 0.024 W/mK
Allowable Pressure Drop @ Design Cond. 1 1 bar
Heating/Cooling Curve Data Attached No Yes
Flow 25 %
Duty 25 %
Design Pressure 10 8.3 bar g
Frame SS304
NOTES
1 Design flow rate and Design heat duty are inclusive of overcapacity factors

CUSTOMER PROCESS DATA SHEET LICENSOR PAGE
2 of 3
LEAN RICH EXCHANGER
(E-103) PROJECT 5 TPD CO2 RECOVERY PLANT
DOC. NO. TSL-PDS-E-103

Segment 0 1 2 3 4 5 6 7 8 9 10
Duty MJ/hr 66.3 66.3 66.3 66.3 66.3 66.3 66.3 66.3 66.3 66.3
Cumulative Duty MJ/hr 66.3 132.6 198.9 265.2 331.5 397.8 464.1 530.4 596.7 663.0
Overall Stream-Rich Solvent

Temperature Celsius 43.90 51.91 59.90 67.88 75.84 83.77 91.66 97.64 102.15 106.31 110.12
Pressure barg 4.00 3.90 3.80 3.70 3.60 3.50 3.40 3.30 3.20 3.10 3.00
Molecular Weight 26.25 26.25 26.25 26.25 26.25 26.25 26.25 26.25 26.25 26.25 26.25
Molar Flow kmol/hr 106.09 106.09 106.09 106.09 106.09 106.09 106.09 106.09 106.09 106.09 106.09
Mass Flow kg/hr 2785 2785 2785 2785 2785 2785 2785 2785 2785 2785 2785
Density kg/cum 1106.00 1100.37 1094.49 1088.36 1081.98 1075.38 1067.42 623.12 349.24 230.01 163.86
Vapor Phase
Phase Fraction - - - - - - 0.00 0.00 0.01 0.01 0.02
Molecular Weight - - - - - - 37.51 38.86 37.84 36.71 35.50
Molar Flow kmol/hr - - - - - - 0.00 0.26 0.73 1.25 1.83
Mass flow kg/hr - - - - - - 0.00 10.104 27.62 45.89 64.97
Enthalpy kJ/kg - - - - - - 61.45 67.02 73.18 79.46 85.85
Heat Capacity kJ/kg-k - - - - - - 1.01 1.02 1.05 1.08 1.11
Density kg/cum - - - - - - 5.51 5.50 5.17 4.84 4.52
Viscosity cP - - - - - - 0.02 0.02 0.02 0.02 0.02
Thermal Conductivity W/m-K - - - - - - 0.02 0.02 0.02 0.02 0.02

This document is a property of Carbon Clean Solutions Limited and it cannot be reproduced or communicated to any third party without prior written consent of Carbon Clean Solutions
Limited.
CUSTOMER PROCESS DATA SHEET LICENSOR PAGE
3 of 3
LEAN RICH EXCHANGER
(E-103) PROJECT 5 TPD CO2 RECOVERY PLANT
DOC. NO. TSL-PDS-E-103

Aqueous Phase
Phase Fraction 1.00 1.00 0.99 0.99 0.98
Molecular Weight 26.25 26.22 26.17 26.13 26.09
Molar Flow kmol/hr 106.09 105.83 105.36 104.84 104.26
Mass Flow kg/hr 2784.86 2774.86 2757.27 2739.47 2720.14
Heat Capacity kJ/kg-K 3.04 3.08 3.12 3.15 3.19
Density kg/cum 1068.55 1059.94 1050.45 1041.35 1032.75
Viscosity cP 0.75 0.67 0.62 0.58 0.54
Thermal Conductivity W/m-K 0.44 0.44 0.44 0.44 0.44
Surface Tension N/m 0.05 0.05 0.05 0.05 0.05

Limited.
PAGE
CUSTOMER PROCESS DATA SHEET LICENSOR 2 OF 2
STRIPPER CONDENSOR PROJECT 5 TPD CO2 RECOVERY PLANT
90°
270° 90°
180°
01. ALL DIMENSIONS ARE IN mm UNLESS OTHERWISE SPECIFIED.
TO BE PROVIDED DURING DETAIL ENGINEERING.
THIS DOCUMENT IS A PROPERTY OF CARBONCAPTURE TECHNOLOGIES PRIVATE LIMITED AND IT CANNOT BE REPRODUCED OR COMMUNICATE TO ANY THIRD PARTY WITHOUT PRIOR WRITTEN CONSENT OF CARBONCAPTURE TECHNOLOGIES PRIVATE LIMITED.
LICENSOR
1 of 1
STRIPPER 5 TPD CO2 RECOVERY
CONDENSOR PROJECT PLANT

Tag No. E-104 No. of Unit 1 Description Stripper Condenser
Fluid CO2 + Vapors Cooling Water
In Out In Out
Liquid Properties
Design Flow Rate 94.34 7406 7406 kg/hr
Density 999 995.5 992.4 kg/m3
Viscosity 0.685 0.781 0.653 cP
Specific Heat 4.124 4.179 4.178 kJ/kg °C
Thermal Conductivity 0.618 0.617 0.629 W/mK
Vapor Properties
Design Flow Rate 317.84 223.5 kg/hr
Density 1.987 3.338 kg/m3
Viscosity 0.016 0.0155 cP
Specific Heat 1.231 0.884 kJ/kg °C
Thermal Conductivity 0.0236 0.0177 W/mK
Flow 40 %
Duty 40 %
Design Pressure 3.5/FV 7 bar g
No. of passes per shell 1 1
Fouling Resistance 0.0002 0.0004 m2K/W
Mechanical Details
Shell per unit 1 Type BEM – Horizontal Series 1 Parallel 1
Surface per unit 190/187 m2 (Gross/Eff) Surface per shell 190/187 m2 (Gross/Eff)
Tube No. 180 Thickness 2.413 mm Tube Type Plain
Tube OD 12.7 mm Length 2438 mm Pitch ratio 1.25 Tube pattern 30°
Shell ID 350 mm Kettle ID - Shell OD - Total Length
Baffle type Perpendicular Orientation NTIW Seg Cut 24% Spacing 400 mm Inlet 968 mm
Pairs seal strips 0 Passlane Seal Rod no 0 Impingement plate Circular Plate Cross passes 5
Material of Constructions
Shell SS304L Tube SS304L Tube sheet SS304L
Channel SS304L Channel Cover SS304L Baffles SS304L
NOTES
1. Design duty and Design Flow are inclusive of overcapacity factors

PAGE
CUSTOMER PROCESS DATA SHEET LICENSOR 2 OF 2
STRIPPER REBOILER PROJECT 5 TPD CO2 RECOVERY PLANT
CUSTOMER
PAGE
1 of 3
STRIPPER REBOILER PROJECT

5 TPD CO2 RECOVERY
PLANT
(E-105) TSL-PDS-E-105
DOC. NO.

Tag No. E-105 No. of Unit 1 Description Stripper Reboiler
Fluid Conditions Shell Side Tube Side
Fluid Lean Solvent Steam
In Out In Out
Operating Temperature 121 122.4 140 140 °C
Operating Pressure 1.11 1.08 3.0 2.9 bar g
Liquid Properties
Design Flow Rate 2895 2569 338 kg/hr
Density 969.5 963.4 927.66 kg/m3
Viscosity 0.427 0.45 0.19 cP
Specific Heat 3.6 3.57 4.28 kJ/kg °C
Thermal Conductivity 0.468 0.446 0.685 W/mK
Vapor Properties
Design Flow Rate 326 338 kg/hr
Specific Heat 1.882 2.303 kJ/kg °C
Thermal Conductivity 0.026 0.03 W/mK
Allowable Pressure Drop @ Design Cond. 0.03 0.1 bar
Heating/Cooling Curve Data Attached No
Flow 25 %
Duty 25 %
Design Pressure 3.5/FV 4.5/FV bar g
No. of passes per shell 1 2
Fouling Resistance 0.0004 0.0002 m2K/W
Design Code ASME Section VIII, TEMA R
Mechanical Details
Shell per unit 1 Type BKU – Horizontal Series 1 Paralle 1
l
Surface per unit 17.72/17.49 m2 (Gross/Eff) Surface per shell 17.72/17.49 m2 (Gross/Eff)
Tube No. 70 Thickness 2.413 mm Tube Type Plain
Tube OD 25.4 mm Length 3048 mm Pitch 31.750 mm Tube pattern 90°
Shell ID 400 mm Kettle ID 600 mm Shell OD Total Length mm
Baffle type Cross Orientation Support Cut -- Spacing 1002.66 mm Inlet --
Pairs seal strips 0 Passlane Seal Rod no 0 Impingement plate Circular Crosspasses 1
Material of Constructions
Shell SS304L Tube SS304L Tubesheet SS304L
Channel SS304L Channel Cover SS304L Baffles SS304L
NOTES
1. Design duty and Design flow are inclusive of overcapacity factors

CUSTOMER
PAGE
2 of 3

5 TPD CO2 RECOVERY
PLANT
(E-105) TSL-PDS-E-105
DOC. NO.

Segment 0 1 2 3 4 5 6 7 8 9 10
Duty MJ/hr 72.03 72.03 72.03 72.03 72.03 72.03 72.03 72.03 72.03 72.03
Cumulative Duty MJ/hr 72.0 144.1 216.1 288.1 360.2 432.2 504.2 576.3 648.3 720.3
Overall Stream
Temperature Celsius 121.00 120.81 121.07 121.29 121.48 121.66 121.83 121.98 122.12 122.26 122.40
Pressure barg 1.00 1.01 1.01 1.01 1.02 1.02 1.02 1.02 1.03 1.03 1.03
Mass flow kg/h 2895.14 2895.14 2895.14 2895.14 2895.14 2895.14 2895.14 2895.14 2895.14 2895.14 2895.14
Density kg/cum 969.41 94.55 50.95 34.72 26.28 21.12 17.64 15.14 13.26 11.79 10.61
Vapor Phase
Phase Fraction 0.01 0.03 0.04 0.06 0.07 0.09 0.10 0.11 0.13 0.14
Molecular Weight 19.82 19.68 19.58 19.50 19.43 19.37 19.33 19.29 19.25 19.23
Molar Flow kmol/hr 1.72 3.35 5.01 6.69 8.37 10.08 11.79 13.50 15.22 16.95
Mass flow kg/h 34.1 66.0 98.1 130.4 162.7 195.2 227.8 260.3 293.0 325.8
Heat Capacity kJ/kg-K 1.82 1.83 1.84 1.85 1.86 1.86 1.87 1.87 1.88 1.88
Density kg/cum 1.23 1.22 1.22 1.21 1.21 1.21 1.21 1.21 1.21 1.21
Viscosity cP 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01
Thermal Conductivity W/m-K 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03 0.03

Limited.
CUSTOMER
PAGE
3 of 3

5 TPD CO2 RECOVERY
PLANT
(E-105) TSL-PDS-E-105
DOC. NO.

Aqueous Phase
Phase Fraction 1.00 0.99 0.97 0.96 0.94 0.93 0.91 0.90 0.89 0.87 0.86
Mass flow kg/h 2895.14 2861.09 2829.18 2797.06 2764.79 2732.46 2699.97 2667.38 2634.81 2602.13 2569.35
HeatCapacity kJ/kg-K 3.60 3.60 3.60 3.60 3.59 3.59 3.59 3.58 3.58 3.57 3.57
Density kg/cum 969.41 968.50 967.47 966.63 965.93 965.34 964.83 964.39 964.01 963.68 963.38
Viscosity cP 0.43 0.43 0.43 0.43 0.44 0.44 0.44 0.44 0.44 0.45 0.45
Thermal Conductivity W/m-K 0.47 0.47 0.46 0.46 0.46 0.46 0.46 0.45 0.45 0.45 0.45
Surface Tension N/m 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05 0.05

Limited.
LICENSOR
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LEAN SOLVENT 5 TPD CO2 RECOVERY
COOLER PROJECT PLANT

Tag No. E-106 No. of Unit 1 Description Lean Solvent Cooler
Fluid Lean Solvent Cooling Water
In Out In Out
Liquid Properties
Density 1039 1047.5 995.5 992.4 kg/m3
Viscosity 3.128 4.811 0.781 0.653 cP
Vapor Properties
Density kg/m3
Viscosity cP
Heat Duty 98800 kJ/hr
Flow 20 %
Duty 20 %
Frame SS304
NOTES
1 Design duty is inclusive of overcapacity factor

LICENSOR
1 of 1
WATER WASH 5 TPD CO2 RECOVERY
CIRCULATION PROJECT PLANT
COOLER-1 (E-107) DOC. NO. TSL-PDS-E-107

Tag No. E-107 No. of Unit 1 Description Water Wash Circulation Cooler-1
Fluid Wash Water Cooling Water
In Out In Out
Liquid Properties
Normal Flow Rate 1721.5 1721.5 2619 2619 kg/hr
Density 988.5 993 995.5 992.4 kg/m3
Viscosity 0.537 0.673 0.781 0.653 cP
Vapor Properties
Density kg/m3
Viscosity cP
Flow 20 %
Duty 20 %
Frame SS304
NOTES
1 Design duty is inclusive of overcapacity factor

LICENSOR
1 of 1
COOLER-2 (E-108) DOC. NO. TSL-PDS-E-108

Tag No. E-108 No. of Unit 1 Description Water Wash Circulation Cooler-2
Fluid Wash Water Cooling Water
In Out In Out
Liquid Properties
Density 988.4 997 995 992.4 kg/m3
Viscosity 0.466 0.657 0.781 0.653 cP
Vapor Properties
Density kg/m3
Viscosity cP
Flow 20 %
Duty 20 %
Frame SS304
NOTES
1 Design duty is inclusive of overcapacity factors

CUSTOMER
LICENSOR
1 of 1
CIRCULATION PUMP PROJECT PLANT
(P-101A/B) DOC. NO. TSL-PDS-P-101

Tag No. P-101 A/B Description Scrubbing Solution Circulation Pump
Capacity 2 x 100 % Type of Pump Centrifugal
Fluid Conditions
Fluid Scrubbing Solution
Pumping Temperature 40 °C
Viscosity at pumping temperature 0.594 cP
Density at pumping temperature 990 kg/m3
Vapor Pressure at pumping temperature 0.07 bar
Presence of corrosive components No
Solids in suspension No
Each Pump Flow rate Normal 3.5 m3/hr
Maximum 4.3 m3/hr
Minimum 3.0 m3/hr
NPSH Available1 14 m
Maximum Suction Pressure 0.1 bar g
Mechanical Data
Casing CS
Impeller SS304
Shaft SS304
Packing/Mechanical Seal Mechanical Seal
Motor Details
Power Supply 415 V / 50 Hz , 3 phase
Type Industrial
VSD Requirement (Yes/No) No
Estimated Absorbed Power for each pump 0.67 kW
NOTES
1. Shall be updated during detail engineering on the equipment layout.

CUSTOMER
PAGE
1 of 1
INTERSTAGE PUMP PROJECT

5 TPD CO2 RECOVERY
PLANT
(P-102) TSL-PDS-P-102
DOC. NO.

Tag No. P-102 Description Interstage Pump
Fluid Conditions
Fluid Solvent Solution
Presence of corrosive components Yes – CO2, O2, Dissolved Organic Salts
Maximum 2.1 m3/hr
Minimum 1.0 m3/hr
NPSH Available1 17.5 m
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Packing/Mechanical Seal Double Mechanical Seal
Design Code ISO 13709/API 610
Motor Details
Type Industrial
NOTES
2. All non-metallic components and elastomers in contact with process fluid shall be of materials which have
proven resistance to degradation with MEA.

CUSTOMER
PAGE
1 of 1
RICH SOLVENT 5 TPD CO2 RECOVERY
PUMP PROJECT PLANT
(P-103 A/B) DOC. NO. TSL-PDS-P-103

Tag No. P-103 A/B Description Rich Solvent Pump
Fluid Conditions
Maximum 2.6 m3/hr
Minimum 1.6 m3/hr
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Motor Details
Type Industrial
NOTES

CUSTOMER
PAGE
1 of 1
STRIPPER REFLUX 5 TPD CO2 RECOVERY
PROJECT
PUMP PLANT
(P-104) DOC. NO. TSL-PDS-P-104

Tag No. P-104 Description Stripper Reflux Pump
Fluid Conditions
Fluid Stripper Reflux Condensate
Presence of corrosive components Yes – Solvent Solution, CO2, O2,H2O
Maximum 0.1 m3/hr
Minimum 0.04 m3/hr
NPSH Available3 22 M
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Motor Details
Type Industrial
NOTES

LICENSOR
1 of 1
STEAM 5 TPD CO2 RECOVERY
CONDENSATE PUMP PROJECT PLANT

Tag No. P-105 Description Steam Condensate Pump
Fluid Conditions
Fluid Steam Condensate
Maximum 0.6 m3/hr
Minimum 0.23 m3/hr
Discharge Pressure1 6.6 bar g
Differential Pressure1 3.3 bar
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Motor Details
Type Industrial
NOTES
1. Shall be updated during detail engineering on the equipment layout and destination point details.

LICENSOR
1 of 1
LEAN SOLVENT 5 TPD CO2 RECOVERY
PUMP PROJECT PLANT
(P-106 A/B) DOC. NO. TSL-PDS-P-106

Tag No. P-106 A/B Description Lean Solvent Pump
Capacity 2 x 100% Type of Pump Centrifugal
Fluid Conditions
Maximum 2.8 m3/hr
Minimum 1.8 m3/hr
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Motor Details
Type Industrial
NOTES

LICENSOR
1 of 1
WATER WASH PROJECT 5 TPD CO2 RECOVERY
CIRCULATION PLANT
PUMP-1 (P-107) DOC. NO. TSL-PDS-P-107

Tag No. P -107 Description Water Wash Circulation Pump 1
Fluid Conditions
Fluid Wash Water
Maximum 2.15 m3/hr
Minimum 1.0 m3/hr
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Motor Details
Type Industrial
NOTES

LICENSOR
1 of 1
PUMP-2 (P-108) DOC. NO. TSL-PDS-P-108

Tag No. P-108 Description Water Wash Circulation Pump 2
Fluid Conditions
Fluid Wash Water
Maximum 2.35 m3/hr
Minimum 1.0 m3/hr
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Noise Level <85 dB(A) at 1 meter distance ( Note- 3)
Motor Details
Type Industrial
NOTES

LICENSOR
1 of 1
CONDENSATE PUMP PROJECT PLANT

Tag No. P-109 Description Water Wash Condensate Pump
Fluid Conditions
Fluid Wash Water
Maximum 0.13 m3/hr
Minimum 0.08 m3/hr
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Noise Level <85 dB(A) at 1 meter distance ( Note- 3)
Motor Details
Type Industrial
NOTES

CUSTOMER
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1 of 1
SOLVENT TRANSFER 5 TPD CO2 RECOVERY
PUMP PROJECT PLANT

Tag No. P-110 Description Solvent Transfer Pump
Fluid Conditions
Viscosity at pumping temperature 14 cP
Presence of corrosive components Solvent Solution
Each Pump Flow rate Normal -- m3/hr
Maximum 1.2 m3/hr
Minimum -- m3/hr
Operation Intermittent (Note- 3)
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Motor Details
Type Industrial
NOTES
3. Normal operation- Operated for few minutes for transferring solvent to the plant.
Startup - Continuous operation for about 2 hrs to load solvent from storage tank

CUSTOMER
LICENSOR
1 of 1
DOSING PUMP PROJECT PLANT

Tag No. P-111 Description Scrubbing Solution Dosing Pump
Fluid Conditions
Maximum 0.12 m3/hr
Minimum 0.06 m3/hr
NPSH Available1 9 m
Mechanical Data
Casing SS304
Impeller SS304
Shaft SS304
Motor Details
Type Industrial
NOTES

LICENSOR
1 of 2
SOx/NO2 SCRUBBING 5 TPD CO2 RECOVERY
COLUMN PROJECT PLANT
(T-101) DOC. NO. TSL-PDS-T-101

Tag No. T-101 Description SOx/NO2 Scrubbing Column
No. of Units 1
Fluid Conditions
Fluid Fuel Gas & Scrubbing Solution
Pressure – Operating / Design Atm / 0.4 & Half Vacuum barg
Temperature – Operating / Design 40-50/70 °C
Turndown/Overdesign 50/ 110 %
Packing Data for Each Unit
Bottom Top Bottom Top
Location from Bottom 1st
Packing Height 5000 mm
Packing Type Intalox Ultra high performance
Vapor Data
Mass flow rate 840 840 kg/hr
Liquid Data
Mass flow rate 3520 3520 kg/hr
Density 992 992 kg/m3
Surface Tension 0.0695 0.0695 N/m
Mechanical Data
Internal Diameter 400 mm
Height (Tangent – Tangent) 11000 mm
Shell SS304L
Internals SS304L
Insulation Required No
Vortex Breaker Required Yes
Demister Details
Demister Required Yes
Type Knit mesh Brownian demister based on customer approval
Liquid Droplet Size & Separation Efficiency >5 micron @ 99 % Removal
Allowable Pressure Drop across Column 15 mbar
Design Code ASME Section VIII, Div. 1
Nozzle Details
Mark NB No. Description Mark NB No. Description
FG1 150 1 Fuel Gas in DP1 25 1 DPIT
FG2 150 1 Fuel Gas out DP2 25 1 DPIT
L1 40 1 Liquid inlet DP3 25 1 DPIT
L2 40 1 Liquid outlet DP4 25 1 DPIT
DM 15 1 DM Water LT1 25 1 Level Transmitter
H1 100 1 Handhole LT2 25 1 Level Transmitter
H2 100 1 Handhole LG1 25 1 Level Gauge
LG2 25 1 Level Gauge TT1 25 1 Temperature Transmitter

LICENSOR
2 of 2
SOx/NO2 SCRUBBING 5 TPD CO2 RECOVERY

SG1 50 2 Sight Glass
NOTES
1

CUSTOMER PAGE
3 OF 3
SOX/NO2 SCRUBBING COLUMN PROJECT 5 TPD CO2 RECOVERY PLANT
01. LADDER AND INTERMEDIATE LANDINGS WILL BE DECIDED DURING DETAIL ENGINEERING.
02. NOZZLES FOR SKIRT SUPPORT WILL BE DECIDED DURING DETAIL ENGINEERING.
03. ELEVATION OF HANDHOLE WILL BE DECIDED DURING DETAIL ENGINEERING.
04. NOZZLE ORIENTATION WILL BE DECIDED DURING DETAIL ENGINEERING.
CUSTOMER
PAGE
1 of 2
ABSORBER COLUMN PROJECT

5 TPD CO2 RECOVERY
PLANT
(T-102) TSL-PDS-T-102
DOC. NO.

Tag No. T-102 Description Absorber Column
No. of Units 1
Fluid Conditions
Fluid Fuel Gas & Solvent Solution
Pressure – Operating / Design Atm / 0.4 & Half Vacuum bar g
Temperature – Operating / Design 40-80 / 110 °C
Turndown/Overdesign 50 / 110 %
Location from Bottom 1st 2nd
Packing Height 6000 6000 mm
Packing Type Mellapak Plus 252Y/ Mellapak Plus 252Y/
Flexipac 250Y H C Flexipac 250Y H C
Vapor Data
Mass flow rate 842 814 816.5 740.5 kg/hr
Density 1.14 1.1 1.062 0.891 kg/m3
Viscosity 0.018 0.018 0.0174 0.017 cP
Liquid Data
Mass flow rate 2442 2432.5 2416.5 2404 kg/hr
Density 1135 1114 1108 1021 kg/m3
Viscosity 4.065 3.534 2.893 1.083 cP
Surface Tension 0.0613 0.0608 0.06 0.058 N/m
Mechanical Data
Shell SS304L
Internals SS304L
Demister Details
Demister Required Yes ( 1 nos.)
Type Knit mesh
Nozzle Details
FG1 150 1 Fuel Gas in DM 25 1 DM Water
FG2 150 1 Fuel Gas out R 25 1 Reflux inlet
S1 50 1 Rich Solvent outlet LT1 25 1 Level Transmitter
S2 40 1 Lean Solvent inlet LT2 25 1 Level Transmitter
S3 50 1 Interstage outlet LG1 25 1 Level Gauge
S4 40 1 Interstage inlet LG2 25 1 Level Gauge

CUSTOMER
PAGE
2 of 2
ABSORBER COLUMN PROJECT

5 TPD CO2 RECOVERY
PLANT
(T-102) TSL-PDS-T-102
DOC. NO.

S5 40 1 Makeup Solvent inlet TT1 25 1 Temperature Transmitter
S6 40 1 Treated Solvent Inlet TT2 25 1 Temperature Transmitter
S7 40 1 Solvent Vapor Line WW1 40 1 Water wash condensate
DP1 25 1 DPIT SG1 50 2 Sight Glass
DP4 25 1 DPIT H1 100 1 Handhole
NOTES
1. Solvent is non-flammable.

CUSTOMER PAGE
3 OF 3
ABSORBER COLUMN PROJECT 5 TPD CO2 RECOVERY PLANT
(T -102) DOC. NO. TSL-PDS-T-102
FG2
2:1 SEMI ELLIPSOIDAL

DISHED END (TYP.)
DP6
DP5
SG3 SG3
S2
H3
DP4
TT2
DP3
S3
SG2 SG2
DP2 H2
S4
TT1
WW1
DP1
SG1 SG1
FG1
S7
S5 S6
H1 DM
LG2
LT2 R
LT1
LG1
S1 01. LADDER AND INTERMEDIATE LANDINGS WILL BE DECIDED DURING DETAIL ENGINEERING.
LICENSOR
1 of 2
WATERWASH 5 TPD CO2 RECOVERY

Tag No. T-103 Description Water Wash Column
No. of Units 1
Fluid Conditions
Fluid Fuel Gas & Solvent Solution
Pressure – Operating / Design Atm / 0.4 & Half Vacuum bar g
Turndown/Overdesign 50 / 110 %
Flexipac 250Y H C Flexipac 250Y H C
Vapor Data
Mass flow rate 738.5 669.5 665 627 kg/hr
Density 0.883 0.951 0.945 1.009 kg/m3
Viscosity 0.0172 0.0173 0.01736 0.01745 cP
Liquid Data
Mass flow rate 2018 1969.5 1764 1725 kg/hr
Density 988 994 987.5 992.5 kg/m3
Viscosity 0.453 0.578 0.517 0.669 cP
Mechanical Data
Shell SS304L
Internals SS304L
Demister Details
Demister Required Yes ( 1 nos.)
Type Knit mesh
Nozzle Details
FG1 150 1 Fuel Gas in from Absorber DM1 25 1 DM Water
FG2 150 1 Fuel Gas out LT1 25 1 Level Transmitter
L1 40 1 WW column top packing liquid L4 40 1 WW column bottom packing
inlet liquid inlet
L3 40 1 WW column top packing liquid L5 40 1 WW column bottom packing
outlet liquid outlet

LICENSOR
2 of 2
WATERWASH 5 TPD CO2 RECOVERY

LT2 25 1 Level Transmitter LG2 25 1 Level Gauge
L2 25 1 Water Wash condensate LG1 25 1 Level Gauge
DM2 25 1 DM Water TT1 25 1 Temperature Transmitter
DP1 25 1 DPIT TT2 25 1 Temperature Transmitter
SG2 50 2 Sight Glass
NOTES

CUSTOMER PAGE
3 OF 3
WATER WASH COLUMN PROJECT 5 TPD CO2 RECOVERY PLANT
CUSTOMER
PAGE
1 of 2
STRIPPER COLUMN PROJECT

5 TPD CO2 RECOVERY
PLANT
(T-104) TSL-PDS-T-104
DOC. NO.

Tag No. T-104 Description Stripper Column
No. of Units 1
Fluid Conditions
Fluid CO2 Vapor & Solvent Solution
Pressure – Operating / Design 1 / 3.5 & Full Vacuum bar g
Turndown/Overdesign 50/ 110 %
Flexipac 2Y HC Flexipac 2Y HC
Vapor Data
Mass flow rate 252 227.5 223.5 189.7 kg/hr
Density 1.269 1.593 1.65 2.16 kg/m3
Viscosity 0.014 0.015 0.015 0.016 cP
Liquid Data
Mass flow rate 2484 2460 2457 2422 kg/hr
Density 990 1023 1023 1059 kg/m3
Viscosity 0.533 0.624 0.643 0.867 cP
Mechanical Data
Shell SS304L
Internals SS304L
Insulation Required Yes Hot Insulation
Demister Details
Type Knit mesh – High Efficiency
Nozzle Details
S1 50 1 Rich Solvent inlet DP3 25 1 DPIT
S2 25 1 Lean Solvent to Reboiler DP4 25 1 DPIT
S3 25 1 Reflux inlet DP5 25 1 DPIT
V1 80 1 Vapor from Reboiler DP6 25 1 DPIT
V2 80 1 Vapor to Condensor SG1 50 2 Sight Glass
LT1 25 1 Level Transmitter SG2 50 2 Sight Glass
LT2 25 1 Level Transmitter SG3 50 2 Sight Glass

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STRIPPER COLUMN PROJECT

5 TPD CO2 RECOVERY
PLANT
(T-104) TSL-PDS-T-104
DOC. NO.

PT1 25 1 Pressure Transmitter TT1 25 1 Temperature Transmitter
H1 100 1 Handhole H3 100 1 Handhole
H2 100 1 Handhole
NOTES
1. Solvent is nonflammable.

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STRIPPER COLUMN PROJECT 5 TPD CO2 RECOVERY PLANT
NOTES:
LICENSOR
1 of 1
SOLVENT STORAGE 5 TPD CO2 RECOVERY
TANK PROJECT PLANT
(TK-101) DOC. NO. TSL-PDS-TK-101

Tag No. TK-101 Description Solvent Storage Tank
Capacity 1 x 100 % Type Vertical Storage Tank
Details of each unit
Fluid Conditions
Volume – Operating / Actual 1.9/1.5 m3
Pressure – Operating / Design Atm/0.08 bar g
Temperature – Operating / Design 40/65 °C
Density at Operating P&T 1040 kg/m3
Blanketing Required No Blanketing Gas
Mechanical Data
Internal Diameter 1300 (Note-3) mm
Height 2600 (Note-3) mm
Shell CS + 3mm CA
Bottom CS + 3mm CA
Roof CS + 3mm CA
Breather Valve/PVRV Required Yes
Design Code ASME Sec. VIII, Div. 1
Nozzle Details
S1 50 1 Rich Solvent inlet H1 100 1 Handhole
S2 40 1 Recirculation line PVRV HOLD 1 PVRV
S3 50 1 Solvent Outlet LT1 25 1 Level Transmitter
D 25 1 Drain LT2 25 1 Level Transmitter
DM 25 1 DM Water PT1 25 1 Pressure Transmitter
TT1 25 1 Temperature Transmitter
NOTES
2. Size of PVRV shall be calculated during Detailed Engineering.
3. Optimization of Height & Diameter to be done during FEED/Detailed Engineering to minimize cost.

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SOLVENT STORAGE TANK PROJECT 5 TPD CO2 RECOVERY PLANT
0°
65°
290°
270° 90°
105°
135°
180°
LICENSOR
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SCRUBBING 5 TPD CO2 RECOVERY
SOLUTION TANK PROJECT PLANT

Tag No. TK-102 Description Scrubbing Solution Tank
Capacity 1 x 100 % Type Vertical Storage Tank
Fluid Conditions
Fluid Scrubbing Agent
Volume – Operating / Design 0.28/0.3 m3
Pressure – Operating / Design Atm/0.08 bar g
Blanketing Required No Blanketing Gas
Mechanical Data
Internal Diameter 600 (Note -1) mm
Height 1000 (Note-1) mm
Shell SS304
Bottom SS304
Roof SS304
Breather Valve/PVRV Required No
Nozzle Details
S1 50 1 Solid Scrubbing Agent TT1 25 1 Temperature Transmitter
S2 40 1 Scrubbing Solution Outlet LT1 25 1 Level Transmitter
DM 25 1 DM Water LT2 25 1 Level Transmitter
V1 25 1 Vent PT1 25 1 Pressure Transmitter
D 25 1 Drain H1 100 1 Handhole (Shell)
NOTES
1. Optimization of Height & Diameter to be done during FEED/Detailed Engineering to minimize cost.

PAGE
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SCRUBBING SOLUTION TANK PROJECT 5 TPD CO2 RECOVERY PLANT
LICENSOR
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STRIPPER REFLUX 5 TPD CO2 RECOVERY
DRUM PROJECT PLANT
(V-101) DOC. NO. TSL-PDS-V-101

Tag No. V-101 Description Stripper Reflux Drum
Capacity 1 x 100 % Type Vertical Drum
Fluid Conditions
Fluid CO2 + Solvent
Pressure – Operating/ Design 1/3.5 and Full Vacuum bar g
Temperature – Operating/ Design 40/160 °C
Mechanical Data
Height 2600 mm
Shell SS304L
Internals SS304L
Is Inlet Baffle Deflector Required Yes
Design Code ASME Section VIII, Div.1
Demister Details
Type Knit mesh
Nozzle Details
V1 50 1 CO2 inlet DP2 25 1 DPIT
V2 50 1 CO2 outlet LT1 25 1 Level Transmitter
V3 25 1 Vent LT2 25 1 Level Transmitter
L1 25 1 Reflux inlet H1 100 1 Handhole (Shell)
L2 25 1 Reflux outlet D 25 1 Drain
DP1 25 1 DPIT
NOTES
1. Solvent is nonflammable.

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CUSTOMER PROCESS DATA SHEET LICENSOR
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STRIPPER REFLUX DRUM PROJECT 5 TPD CO2 RECOVERY PLANT
(V -101) DOC. NO. TSL-PDS-V-101
LICENSOR
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STEAM 5 TPD CO2 RECOVERY
CONDENSATE DRUM PROJECT PLANT
(V-102) DOC. NO. TSL-PDS-V-102

Tag No. V-102 Description Steam Condensate Drum
Capacity 1 x100 % Type Vertical Drum
Fluid Conditions
Fluid Steam Condensate
Pressure – Operating/ Design 3/4.5 and FV bar g
Temperature – Operating/ Design 140/180 °C
Mechanical Data
Height 2650 mm
Shell CS + 3mm CA
Internals CS + 3mm CA
Insulation Required Hot Insulation
Is Inlet Baffle Deflector Required Yes
Design Code ASME Section VIII, Div.1, IBR Certified
Demister Details
Demister Required No
Type NA
Liquid Droplet Size & Separation Efficiency NA
Nozzle Details
L1 40 1 Condensate inlet PT1 25 1 Pressure Transmitter
L2 25 1 Condensate outlet LT1 25 1 Level Transmitter
V1 25 1 Vapor Balance Line LT2 25 1 Level Transmitter
V2 25 1 Vent Line LG1 25 1 Level Gauge
D 25 1 Drain LG2 25 1 Level Gauge
H1 100 1 Handhole (Shell)
NOTES
1.

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STEAM CONDENSATE DRUM PROJECT 5 TPD CO2 RECOVERY PLANT
(V -102) DOC. NO. TSL-PDS-V-102
THIS DOCUMENT IS A PROPERTY OF CARBON CLEAN SOLUTION LIMITED AND IT CANNOT BE REPRODUCED OR COMMUNICATE TO ANY THIRD PARTY WITHOUT PRIOR WRITTEN CONSENT OF CARBON CLEAN SOLUTION LIMITED.
CUSTOMER TECHNICAL PAGE
SPECIFICATIONS LICENSOR
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SCRUBBING SOLUTION PROJECT

5 TPD CO2 RECOVERY
PLANT
FILTRATION PACKAGE
TSL-TS-Z-101
(Z-101) DOC. NO.

Tag No. Z-101 Description Scrubbing Solution Filtration Package
Equipment Capacity 2 x 100% Location Outside with no Roof
Fluid Conditions
Flow Rate – Operating / Design 3.6/4.0 m3/hr
Pressure – Operating / Design 5/7 bar g
Viscosity at Operating P&T 0.65 cP
Max Allowable Pressure Drop at design flow 1 bar
Type Cartridge Type
Size of suspended solids to be removed >2 micron
Removal Efficiency 99 %
Mechanical Data
Filter Casing SS304L
Vessel Internals SS304L
Filter Elements Vendor to advise
NOTES
1. pH of scrubbing solution will vary from 4-12

Page 1 of 1

ELECTRICAL
LICENSOR
LOAD LIST DOC. NO. TSL-ELL-600
S.No. Tag No. Equipment Name No. of Units in Absorbed Power for each unit, kW
simultaneous Continuous Intermittent
operation Normal Design Normal Design
1 P-101 A/B Scrubbing Solution Circulation pump 1 0.56 0.67 - -
2 P-102 Interstage Pump 1 0.18 0.21
3 P-103 A/B Rich Solvent Pump 1 0.45 0.56
4 P-104 Reflux Pump 1 0.01 0.01
5 P-105 Condensate Pump 1 0.03 0.07
6 P-106 A/B Lean Solvent Pump 1 0.37 0.44
7 P-107 WW Circulation Pump 1 1 0.18 0.22
8 P-108 WW Circulation Pump 2 1 0.24 0.29
9 P-109 WW Condensate Pump 1 0.01 0.01
10 P-110 Solvent Transfer Pump 1 - - 0.08 0.08
11 P-111 Scrubbing Solution Dosing Pump 1 0.015 0.015 - -
12 BL-101 Blower 1 - 3.85 - -
13 Z-103 Solvent Treatment Package 1 - - 0.5 0.55
Total Electrical Load 2.05 6.35 0.6 0.6

NOTES
1 The above power consumption is at motor loads and excludes lightning loads, control and automation loads.
2 Motor Efficiency to be confirmed by vendor during Detail Engineering

Rev. Date Description Prepared Checked Approved
This document is a property of Carbon Clean Solutions Limited and it cannot be reproduced or communicated to any third party without prior written consent of Carbon
Clean Solutions Limited.
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CHEMICALS & 5TPD CO2 RECOVERY
EFFLUENT PROJECT PLANT
SUMMARY DOC. NO. TSL-US-700

INTRODUCTION
This document specifies utility, chemicals requirement and summary of effluents from CO2
Recovery Plant.
UTILITY AND CHEMICALS SUMMARY
Sr. No. Utilities Unit Values
1 LP Steam kg/hr 300

2 Cooling Water m3/hr 25
3 DM Water kg/hr 4*
4 Power kW 6.5
5 CDRMax® Solvent kg/d 2.0
6 Scrubbing Agents kg/d 10.0
NOTES:
1. Intermittent addition in the SOx/NO2 removal package and Absorber sump for plant water
balance.
GASEOUS EFFLUENT
3.1 Depleted Fuel Gas
The concentrations of emissions in the depleted fuel gas will be as below
S.No. Components Concentrations
1 Flow Rate 630 kg/hr

(540 Nm3/hr)
2 Ammonia (NH3) <5 ppmv

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CHEMICALS & 5TPD CO2 RECOVERY
EFFLUENT PROJECT PLANT
SUMMARY DOC. NO. TSL-US-700

3 Solvent <1 ppmv
4 Frequency Continuous
LIQUID EFFLUENT
4.1 Liquid Bleed
The concentrations of bleed from SOx and NO2 Treatment Package will be as below
Sr.No. Components Concentrations
1 Flow rate** 5.0 kg/hr
2 pH 10-11
3 TDS 35000 ppmw
4 Frequency Continuous
** For normal operation 10 mg/Nm3 of SO2 is considered. For design case of 100 ppmv
of SO2 the bleed rate would be about 40 kg/hr and the scrubbing agent requirement
would be about 1.5 kg/hr
SOLID EFFLUENT
5.1 Reclaimer spent solvent waste
The expected reclaimer waste for 12 months period will be 100 kgs on dry basis. The reclaimer
waste is hazardous and shall be sent for incineration or deep well injection as outlined in the HSE
procedures document.

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HSE PROCEDURES PROJECT

5 TPD CO2 RECOVERY
PLANT
DOC. NO. TSL-HSE-900
HSE OVERVIEW
1.1 SOLVENT HANDLING
Carbon Clean Solutions Limited’s APBS-CDRMax® solvent is specifically engineered for CO2
recovery and must not be used for any other means of utilization. The solvent is slightly viscous and
highly alkaline liquid. It has a slight Ammonia odour and is colorless to slightly yellow in color. The
other properties related to the APBS-CDRMax® solvent can be referred to in the respective Safety
Data Sheet Sections (Auxiliary attachment) on Properties, Handling, First Aids, Personal
Protective Equipment (PPE) needed etc.
If the solvent to be handled onsite is in large quantities, adequate storage facilities and handling
equipment should be in place while loading-unloading of the solvent from the respective
containment and while in operation of the CO2 recovery plant.
The two main ways in which the solvent shall be dispatched to the customer is via:-
1. Chemical Barrels or IBC (Intermediate Bulk Containment)

2. Tanker trucks
The barrels will usually be of HDPE grade plastic with each barrel containing about 200kg of
APBS-CDRMax® solvent. The IBC’s will be of export grade quality and will be containing about
1000kg to 1500kg of APBS-CDRMax® solvent. The solvent, after the necessary Quality Checks
and Document verifications, ought to be handled as per the proposed methodology specified in the
relevant section in the CCS Operation Manual.
In the transportation mode via Tanker Trucks, the quantity of the solvent shall be varying from
10 Tons to 25 Tons. Necessary pumping precautions, Spillage control setup and PPE ought to be
provided to the operators while carrying out the pumping operation from both modes of
transportation.
It is strongly advised to permit only trained personnel for the solvent handling aspects, like the
loading-unloading operations of the APBS-CDRMax® Solvent and the Spill-Containment of the
solvent, so as to avoid injuries and accidents. The handling of the barrels and the tanker-truck should
0 02.11.2018 Issued for Information VG GK ARK

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5 TPD CO2 RECOVERY
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be in accordance to Standard Practices prescribed, considering the specificities mentioned on the

respective section specified in the CCS Operation Manual.
The possible causes for leakage/spillage of the solvent are listed below:
1. Sampling points
2. Piping rupture/wear-and-tear
3. Flanges
4. Heat Exchangers Joints
5. Pumps
6. Re-boiler Connections
7. Loading-Unloading of solvent
The main reason for the leaks is wear-and-tear of the material housing the solvent or solvent flow. In
addition, improper maintenance and the lack of punctuality in repairing faulty machinery can also
lead to leakages. Major reasons for spillage are improper handling of the barrels of solvent and not
following the standard operating procedure prescribed. In addition, improper sample collection may
also result in spillages.
1.2 SPILL CONTROL PROCEDURES
The on-site manager/spill coordinator will determine if the spill is “minor” or “major” before
evacuating the building or contacting any of the emergency contacts listed. The following criteria
shall be used:
• A “minor spill” is the scenario which usually presents little or no hazard to person/property and
is small enough to be safely contained and cleaned up using the Emergency Spill Kit (described
in the next section).
• A “major spill” is the scenario that cannot be contained safely with the materials on the site
(Emergency Spill Kit). It threatens safety to life, and/or threatens to enter the sewer system/soil
or travel beyond the boundaries of the premises to endanger the environment.

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The following steps should be followed in an attempt to clean up a spill or leak in a safe and secured
manner: -
1. Alert the right people regarding the spillage after it is determined that it is minor or major.
2. If the spillage is Minor,
a. Wear proper Personal Protective Equipment (PPE) contained in the Emergency Spill Kit.
b. Contain the spreading of the spillage by using material from the Emergency Spill Kit
c. Once spill is contained, apply absorbent material found within the spill kits to the entire
spilled area (DO NOT USE WATER)
d. Using a no-sparking shovel, ensure that all the liquid has been mixed with the absorbent
material.
e. Place the spent absorbent into a disposal bag and then into the Hazardous Waste
Containers.
f. Dispose the material in conformance with the MSDS sheet.
g. Ventilate and wash area when clean-up is complete. Do NOT wash into sewer/drainage
system.
3. If the spill is Major (and/or spillage cannot be contained),
a. Inform surrounding staff and building occupants.

b. Secure and control entrance to the area. Eliminate all ignition sources
c. Evacuate personnel and move upwind/high level areas.
d. Call the assigned Environment Cleaning Company to undertake cleaning activities
e. The spill control personnel ought to wear the appropriate PPE and follow the Instructions
and Standard Operating Procedures (SOP) prescribed.
f. In case of serious damage/injury to personnel, equipment or property, alert the Occupier
of the plant and the local Fire Dept.

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1.2.1 SPILL KIT DOCUMENTATION
The spill kits are only to be used by personnel who have had proper training under the supervision
of the Spill Coordinator or the Acting Spill Coordinator. Tri-Monthly inspection shall take place to
ensure sufficient supplies within the spill kits. After a spill, all used items ought to be promptly
replaced. The contents of the Emergency Spill Kit are listed below and shown in Figure 1 below:
Figure 1: Emergency Spill Kit Contents
1. Absorbent pads/pillows for use on floors or ground

2. Absorbent for use on liquids (bases)
3. 50 feet of absorbent socks for use as dam/dyke containment
4. Non-Sparking Shovels
5. Perforated Shovel (for removing the absorbent from the liquid)
6. PPE: Rubber gloves, Rubber boots, Heavy Duty goggles, Rubber Apron
7. 5L/10L Pail (bucket)
8. Refuse sacks (for holding the collected/accumulated hazardous waste)

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1.2.2 CONTAINMENT MECHANISMS
There are two options for spill containment:

1. Bund system: A bund system can be built around the storage systems present in the CO2
recovery system. It is advised to consider a bund system with at least 50% capacity of the
containment unit around which it is to be built. The major areas where the bund system can
be considered to be built are:
1. The Absorber column
2. The Stripper column
3. The Lean Solvent tank
4. The Make-up solvent tank
A picture of a Bund System is given in Figure 2 below. The interior walls of the bund need to
be made of material that is non-reactive and resistant with the solvent in case of a spillage
scenario.
Figure 2: A Bund System to Contain Liquid Spillage

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2. Sump System: A Sump system is similar to a bund system. The only difference is that the
containment structure is built below the ground level. It is advised to consider a bund
system with at least 50% capacity of the containment unit around which it is to be built.
Point to note is that the interior walls of the bund need to be repulsive, non-reactive and/or
resistive with the liquid that needs to be contained in case of a spillage scenario.
The major areas where the sump system can be considered are the same as those for a bund
system.
3. Barrel Storage:
For the fresh or used solvent barrel storage area, pallets having an in-built sump can be used
so that the operator in charge for decanting the solvent from the barrels need not worry
about the spillage onto the shop-floor. The spilled solvent can be re-used back in the system
as it does not get contaminated. Periodic cleaning of the pallets are needed to avoid
contamination in them. A picture of a pallet with built-in sump is given In Figure 3.
Figure 3: A Picture of a Pallet with Built-in Sump
1.3 EXPOSURE SCENARIOS
The CO2 recovery plant is designed as a Closed-Loop system of solvent circulation and hence there
is basically no active/continuous generation of waste either in the form of liquid/solid. APBS-
CDRMax® solvent has low vapour pressure and thus, the emanation of vapours from the solvent in
ambient conditions is very low.

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5 TPD CO2 RECOVERY
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Prolonged exposure to the leaked/spilled solvent in ambient conditions and at elevated process
conditions should be minimized and appropriate PPE as specified in the MSDS should be equipped
by the employees working onsite, as part of standard practice.
1.3.1 OPERATING CONDITIONS
The most common Operating conditions in the CO2 recovery plant are listed below during which
solvent exposure may occur:
1. Use in closed processes, Ambient operating conditions (temperature, pressure, flow-rate)

– No/Minimal exposure from routine operation
2. Use in closed processes at elevated operating conditions (temperature, pressure, flow-
rate) – No/Minimal exposure from routine operation
3. Sample collection
i. Ambient conditions
ii. Elevated conditions
4. Laboratory testing’s and Quality Checks
5. Leaks/Spills
i. Loading/Unloading Operation – Manual transfer/Mechanical transfer
ii. Sample collection
iii. Others – Wear-and-tear, Leakages
6. Maintenance Operations and Normal Shutdown
7. Emergency Shutdown
The Properties of Solvent are as follows:
Some of the physical properties of the solvent are listed below:
1. pH > 12
2. Vapour Pressure: 4.5 kPa (40 °C)
3. Ammoniacal Odour
4. Non-explosive, Non-Flammable, Non-Oxidizing
5. Solvent is stable under standard temperature and pressure

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5 TPD CO2 RECOVERY
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Some Important Toxicological and Ecological information are listed below:

1. Causes serious damage to eye (pH > 13). The eye must be washed repeatedly with
potable water
2. Ingestion: LD50 (rat) > 2000 mg/kg body weight
3. Skin contact: Non –Skin Irritant; Dermal acute toxicity estimate: 4452.3 mg/kg body
weight
4. May cause an allergic skin reaction on contact (depending on case-to-case basis)
1.3.2 PRECAUTIONS
The precautions to be taken in case of any contact with the solvent while handling are listed below:
1. Refer to Section 4: First Aid measures in the Material Safety Data Sheet (MSDS) for the
specific action needed on contact on the respective area mentioned.
2. Refer to Section 9 of the MSDS for the Personal Protective Equipment specifications
required to handle the solvent such as:
a. Hands (Gloves)
b. Feet (Industrial Boots)
c. Body (Apron)
d. Eyes (Chemical resistive Goggles)
e. Inhalation (Face Mask to cover the nose and mouth to avoid inhalation or full-
face mask)
1.3.3 SOLVENT HANDLING: BARREL TRANSFER, SAMPLING & TESTING
During all these activities, care must be taken that the PPE are worn by the employees in adherence
to the Standard Operating Procedures (SOP) during the whole operation. The Standard Operating
Procedure (SOP) for the solvent barrel transfer is as follows:
1. Check for any defects/damage/leaks either near the opening or along the side and bottom
of the barrels. If there is any damage or leaks, DO NOT use the barrel. Contact the
supplier.

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2. The decanting operation done with the help of mechanistic pumps ought to be done in
such a way that the opening of the barrel is towards the direction of the tilt of the barrel
holder in order to drain out the solvent efficiently and quicker thus reducing the exposure
to the operator.
3. If the decanting operation is done manually, it should be done under supervision of the
Shift In-charge with First-Aid and Emergency Spillage Kit available. The best way to
decant in this method will be to put the barrel on a set-up as shown in Figure 4a below.
Figure 4b shows various trolleys.
Figure 4a: Barrel Decanting with Spill Control Figure 4b: Trolleys for Solvent Barrel
4. The operators must be aware of the spill containment procedure to be followed in case it
happens. Refer to the Spill Containment section for detailed procedure to handle the
spillages.
5. The spillages from the tank can be contained by the means of provision of a bund system
around it to contain the spread and make it accumulate at one place which can be scooped
up later.
6. Once the barrel decantation activity is done, the operator can take the barrels to the drum
cleaning yard and clean the inside of the barrel thoroughly so that the barrels can be re-
used.
7. In the laboratory testing area, first aid-kit must be ready in stand-by and the necessary
precautionary measures and PPE should be worn by the personnel so as to avoid contact.

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1.3.4 PLANT OPERATIONS

In the CO2 recovery plant, there shall be provisions for sampling points for gas, liquid and solid
streams. Some of the areas of solvent exposure are:
1. Flue gas stream devoid of CO2 gas
2. CO2 gas stream
3. Filters and Activated Carbon Cartridges (sludge)
4. Sampling points for solvent (lean/rich solvent)
There is a low probability for an insignificant quantity of solvent to be present in the Flue gas outlet
stream and product CO2 line depending on the process operating conditions. The level is expected to
be a few parts per million and well below the level at which any long-term effect can occur. There
will be some solvent retained by the Filter media or Activated Carbon cartridges.
Hence, during maintenance or inspection of the filters and carbon cartridges and during Sampling of
solvent, the specified PPE needs to be worn by the personnel as specified in Section 9 of the MSDS.
1.4 WASTE HANDLING
The APBS-CDRMax® solvent being alkaline, should not be let into water-bodies and drain lines in
case of spills or leaks from the CO2 recovery plant or while loading or unloading. The solvent after
its use-life and the spilled/contaminated solvent ought to be disposed of as hazardous waste as per
applicable regulations.
There shall be solid sediments which shall be collected at the Filter mesh and also in the form of
sludge in the CO2 recovery plant, which shall also be handled and treated accordingly as Hazardous
waste. The necessary PPE ought to be utilized while handling the waste and the waste handling
procedure should be followed as per the local regulations in the area by trained personnel and/or
authorized waste treatment agency.

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1.4.1 SOURCES OF WASTE IN THE CO2 RECOVERY PLANT

There are 3 main sources in the CO2 Recovery plant where waste gets generated. They are:
1. Used Solvent
The solvent used in the CO2 Recovery plant will begin to lose it properties over a period of time
and it needs to be replaced with a fresh batch of solvent to keep the overall process running
efficiently. This will be due to the fact that the solvent begins to degrade under thermal and
oxidative conditions which are part of the process.
2. Sludge
The sludge gets generated from the Reclaimer system in the CO2 Recovery plant which is
primarily installed to clean-up the solvent which is contaminated with Heat Stable Salts (HSS).
The used solvent and the sludge in the Reclaimer system need to be removed and the cycle can
be repeated again. In addition, Particulate matters and other solid contaminants that do not get
filtered out in the filters decrease the efficiency of the absorber and stripper by plugging packings
and process piping. The solution is to provide filter cartridges with very small pore sizes.
3. Filters
The filters will be of Duplex-Mesh type and an addition of an Activated carbon filter will be
provided to filter out suspended solid particulates in the lean solvent stream. 10 micron is a
reasonable maximum and 5 micron a reasonable minimum for filter element porosity. In due
course of time the pores of these filters are blocked by solids present in the liquid. Thus, they
need to be cleaned by regeneration for re-use or replaced for further usage. The activated carbon
filter needs to be replaced once in every 6month/1year depending on the process condition
variability.
1.4.2 WASTE CLASSIFICATION AND WAYS TO STORE

The used solvent should be classified as hazardous waste and must be disposed of accordingly as
per rules and regulations applicable. As mentioned earlier, the used solvent and the sludge from the
Reclaimer system will be consisting of compounds that get generated as a result of oxidative and
thermal degradation cycles that take place as a part of the process. Following are the procedures
needed to follow for onsite storage of waste:

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1. Contents clearly marked on the tank.

2. All individual tanks or groups of tanks must be surrounded by a dike of greater capacity
than the largest tank (unless otherwise approved)
3. All new and replacement tanks are to be internally protected against corrosion.
4. Should have no openings in the dikes that provide a direct connection to any place
beyond the dike area. This includes rainwater line.
5. Should be of adequate size and minimize odors
6. Should have spill containment for loading and unloading areas
7. Spill containment on load lines or elevated load/unload ports to prevent spillage.
8. Constructed of a material compatible with stored substance (i.e. alkaline chemicals)
9. Designed and installed to withstand any stresses from the stored material
10. Coated with a corrosion resistant material if susceptible to corrosion
11. Corrosion protection for any associated subsurface fittings or piping
12. Equipped with high level alarms
13. If > 10000 liters and susceptible to corrosion a thickness test must be performed 20 years
after the date of manufacture and every 10 years after initial inspection. The tank must be
marked after each test to indicate the date, remaining life of the tank and the plate
thickness.
The filters should be drained of all the liquids prior to the transportation and disposal. This can be
accomplished with screened barrel containers. The liquid (solvent) must be separately disposed. To
reduce volume, drained filters can be crushed. Only non-pyrophoric filters are allowed in bag
containers and the bags are not designed/permitted to store and transport free liquids.
1.4.3 OPTIONS FOR DISPOSAL
APBS-CDRMax® solvent waste is a hazardous waste and it should be handled accordingly. The
best option currently available is off-site treatment and disposal by Government authorized Third
party Waste Handlers/Contractors. The Used solvent needs to be pumped into the original solvent
containers/barrels or onto the make-up chemical barrels. This will be marked as per applicable

CUSTOMER
PAGE
LICENSOR
13 of 13

5 TPD CO2 RECOVERY
PLANT
regulations and stored in the allocated space for hazardous waste. The recommended methodology
for the disposal of the hazardous waste is Incineration followed by Landfill (post Solvent
Reclamation process), by Authorized Waste Handling agencies.
1.4.4 FUTURE PROSPECTS

Other future prospects could be to incinerate the used-solvent in a coal-fired boiler or in a cement
kiln as use it as a resource. This will significantly reduce the cost of disposal. However, a
comprehensive analysis of the actual emissions from the used solvent needs to be done and the
approval for co-firing in either a coal-fired boiler/cement kiln needs to be taken from the respective
Pollution Control Board authorities keeping in mind the limit cap on the emissions. Further study
needs to be done on this aspect considering all relevant aspects.

CUSTOMER LICENSOR
PLANT
Annexure - I
Solvent Material Safety Data Sheet
SAFETY DATA SHEET – APBS-CDRmax
Version: 5.0 Date: 31st January 2018
ACCORDING TO EC-REGULATIONS 1907/2006 (REACH),

1272/2008 (CLP) & 2015/830
SECTION 1: IDENTIFICATION OF THE SUBSTANCE/MIXTURE AND OF THE COMPANY/UNDERTAKING

1.1 Product identifier
Product Name APBS - CDRmax
Product code(s) Not established.
1.2 Relevant identified uses of the substance or mixture
and uses advised against
Identified Use(s) CO2 CAPTURE SYSTEMS
Uses Advised Against None known.

1.3 Details of the supplier of the safety data sheet
Company Identification Carbon Clean Solutions Ltd.
47 Castle Street
Reading
Berkshire
RG1 7SR
United Kingdom
Telephone +91 981 989 1937 (or) +91 7700 90 2244

Fax Not available.
E-Mail (competent person) vigneswaran@carboncleansolutions.com
1.4 Emergency telephone number 0044(0)1235 239670 - National Emergency Response Center, UK
24 hours 7days per week
Languages spoken English, German, Swedish, Norwegian
SECTION 2: HAZARDS IDENTIFICATION

2.1 Classification of the substance or mixture
2.1.1 Regulation (EC) No. 1272/2008 (CLP) Skin Sens. 1; H317
Eye Dam. 1; H318
Repr. 2; H361
STOT RE. 1; H372
Aquatic Chronic 3; H412
2.2 Label elements According to Regulation (EC) No. 1272/2008 (CLP)

Product Name APBS - CDRmax
Hazard Pictogram(s)
Signal Word(s) DANGER
Hazard Statement(s) H317: May cause an allergic skin reaction.

H318: Causes serious eye damage.
H361: Suspected of damaging fertility or the unborn child.
H372: Causes damage to organs through prolonged or repeated exposure.
H412: Harmful to aquatic life with long lasting effects.
Precautionary Statement(s) P280: Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338: IF IN EYES: Rinse cautiously with water for several minutes.
Remove contact lenses, if present and easy to do. Continue rinsing.
P310: Immediately call a POISON CENTER/doctor.
Page: 1 of 8 Confidential Document


1272/2008 (CLP) & 2015/830
P302+P352: IF ON SKIN: Wash with plenty of water.

P332+P313: If skin irritation occurs: Get medical advice/attention.
P273: Avoid release to the environment.
2.3 Other hazards None known.
SECTION 3: COMPOSITION/INFORMATION ON INGREDIENTS

3.1 Substances Not applicable
3.2 Mixtures Substances in preparations / mixtures
The components and composition of APBS-CDRMax® is a confidential business information of Carbon Clean Solutions Limited, UK.
For full text of H phrases see section 16.
SECTION 4: FIRST AID MEASURES
4.1 Description of first aid measures

Inhalation IF INHALED: Remove person to fresh air and keep comfortable for breathing.
Maintain an open airway. Loosen tight clothing such as a collar, tie, belt or
waistband. Get medical advice/attention if you feel unwell.
Skin Contact IF ON SKIN (or hair): Remove/take off immediately all contaminated clothing.
Rinse skin with water/shower. After contact with skin, wash immediately with
plenty of water. If irritation (redness, rash, blistering) develops, get medical
attention. Wash contaminated clothing before reuse.
Eye Contact IF IN EYES: Flush eyes with water for at least 15 minutes while holding eyelids
open. Remove contact lenses, if present and easy to do. Continue rinsing. Get
medical attention immediately.
Ingestion IF SWALLOWED: rinse mouth. Do NOT induce vomiting. Drink 1-2 glasses of
water or milk. Get medical attention immediately.
4.2 Most important symptoms and effects, both acute Causes serious eye damage. May cause an allergic skin reaction. Suspected of
and delayed damaging fertility or the unborn child. Causes damage to organs through
prolonged or repeated exposure.
4.3 Indication of any immediate medical attention and Treat symptomatically. IF IN EYES: Obtain prompt consultation, preferably from
special treatment needed an ophthalmologist. Chemical eye burns may require extended irrigation.
SECTION 5: FIREFIGHTING MEASURES

5.1 Extinguishing media
Suitable Extinguishing media Product as supplied: Does not support combustion. Extinguish with carbon
dioxide, dry chemical, foam or waterspray. Alcohol resistant foams (ATC type)
are preferred.
Unsuitable extinguishing media General purpose synthetic foams (including AFFF) or protein foams may
function, but will be less effective. Direct water jet may spread the fire.
5.2 Special hazards arising from the substance or Combustion may cause toxic fumes. Hazardous decomposition product(s):
mixture Nitrogen oxides, Carbon monoxide, Carbon dioxide
5.3 Advice for fire-fighters Fire fighters should wear complete protective clothing including self-contained
breathing apparatus. Do not breathe fumes. Keep containers cool by spraying
with water if exposed to fire. Avoid run off to waterways and sewers.


1272/2008 (CLP) & 2015/830
SECTION 6: ACCIDENTAL RELEASE MEASURES

6.1 Personal precautions, protective equipment and Ensure adequate ventilation. Avoid contact with skin and eyes. Wear
emergency procedures appropriate personal protective equipment, avoid direct contact.
6.2 Environmental precautions Avoid release to the environment. Do not release undiluted and unneutralised to
the sewer. Spillages or uncontrolled discharges into watercourses must be
alerted to the Environment Agency or other appropriate regulatory body.
6.3 Methods and material for containment and cleaning Cover spills with inert absorbent material. Transfer to a lidded container for
up disposal or recovery. Dispose of waste according to applicable legislation. Flush
spill area with copious amounts of water. Ensure waste is collected and
contained.
6.4 Reference to other sections See Section: 8, 13
SECTION 7: HANDLING AND STORAGE

7.1 Precautions for safe handling Do not eat, drink or smoke when using this product. Wear appropriate personal
protective equipment, avoid direct contact. In case of inadequate ventilation
wear respiratory protection. Avoid skin and eye contact. Do not breathe vapour.
Take off contaminated clothing and wash it before reuse.
7.2 Conditions for safe storage, including any Do not store in unlabelled containers. Keep only in original container. Keep
incompatibilities container tightly closed and in a well-ventilated place. Keep from direct sunlight.
Opened containers should be carefully resealed and stored in an upright
position.
Storage temperature Store in a well-ventilated place. Keep cool.
Storage life Stable at ambient temperatures.
Incompatible materials Strong acids and alkali.oxidizing materials, Aluminium, Zinc, Brass, Copper,
copper alloy, metals, Halogenated hydrocarbons. Do not use sodium nitrite or
other nitrosating agents in formulations containing this product. Carcinogenic
nitrosamines may be formed.
7.3 Specific end use(s) See Section:1.2 and/or Exposure ScenarioWear appropriate personal protective
equipment, avoid direct contact.
SECTION 8: EXPOSURE CONTROLS/PERSONAL PROTECTION

8.1 Control parameters
8.1.1 Occupational Exposure Limits None assigned.
8.1.2 Biological limit value Not established.
8.1.3 PNECs and DNELs
COMPONENT 1 COMPONENT 2
Human Health (DNEL)
Short term Inhalation Not applicable Not applicable
Systemic effects Dermal Not applicable Not applicable
Workers
Long Term Inhalation 6.5 mg/m³ 10.6 mg/m³
Systemic effects Dermal 7.3 mg/kg bw/day 3.33 mg/kg bw/day
Inhalation 1.6 mg/m³ Not applicable
Consumer Dermal 37 mg/kg bw/day Not applicable
Oral 0.46 mg/kg bw/day Not applicable
Environmental Parameters (PNECs)
freshwater 0.188 mg/l 0.058 mg/l
marine water 0.019 mg/l 0.006 mg/l
freshwater sediment 0.71 mg/kg dry weight 215 mg/kg dry weight
marine sediment 0.071 mg/kg dry weight 21.5 mg/kg dry weight
Sewage Treatment Plant 10 mg/l 250 mg/l
Soil 0.03 mg/kg dry weight 1 mg/kg dry weight


1272/2008 (CLP) & 2015/830
8.2 Exposure controls Advanced (industrial) exposure controls assumed.

8.2.1 Appropriate engineering controls
Industrial use Outdoor use. Ensure adequate ventilation.
Use as laboratory reagent Indoor use. Provide a good standard of general ventilation (not less than 3 to 5
air changes per hour). Handle in a fume cupboard or under extract ventilation.
Efficiency of at least: 90%
8.2.2 Individual protection measures, such as personal Assumes a good basic standard of occupational hygiene is implemented.
protective equipment (PPE)
Eye/ face protection Use eye protection according to EN 166, designed to protect against liquid
splashes.
Skin protection Hand protection:

Wear impervious gloves (EN374). Efficiency of at least: 80%
Long Term Exposure:
Butyl rubber; Minimum thickness: 0.3 mm; breakthrough time: 480 minutes.
Short Term Exposure:
Nitrile rubber; Minimum thickness: 0.11 mm; breakthrough time: 30 minutes.
Body protection:
Wear impervious protective clothing, including boots, lab coat, apron or coveralls,
as appropriate, to prevent skin contact.
Respiratory protection Wear a respirator providing a minimum efficiency

PROC2 (Elevated) of (%): 95%. Recommended: Gas filtering
respirator (DIN EN 14387).
PROC3, PROC4, Wear a respirator providing a minimum efficiency
PROC8a, PROC8b, of (%): 90%. Recommended: Gas filtering
PROC15 respirator (DIN EN 14387).
In case of inadequate ventilation wear respiratory
protection. Wear a respirator providing a minimum
All other uses
efficiency of (%): 95% Recommended: Gas
filtering respirator (DIN EN 14387).
Thermal hazards Not applicable

8.2.3 Environmental Exposure Controls Avoid release to the environment.
SECTION 9: PHYSICAL AND CHEMICAL PROPERTIES

9.1 Information on basic physical and chemical properties (Substances in preparations / mixtures)
Appearance Viscous liquid; Colourless
Odour Ammonia odour.
Odour threshold Not determined.
pH > 13
Melting point/freezing point No data
Initial boiling point and boiling range 104 – 220 °C
Flash point Not applicable
Evaporation rate Not available.
Flammability (solid, gas) Not applicable (Liquid)
Upper/lower flammability or explosive limits Not applicable (Liquid)
Vapour pressure 4.5 kPa (40 °C)
Vapour density Not determined.
Relative density 1.04
Solubility(ies) Miscible with: Water
Partition coefficient: n-octanol/water Not established.
Auto-ignition temperature Not established.


1272/2008 (CLP) & 2015/830
Decomposition Temperature Not established.

Viscosity 7 cSt at 40 °C
Explosive properties Not explosive.
Oxidising properties Not oxidising.
9.2 Other information Not applicable
SECTION 10: STABILITY AND REACTIVITY

10.1 Stability and reactivity Stable under normal conditions.
10.2 Chemical stability Stable under normal conditions.
10.3 Possibility of hazardous reactions Hazardous polymerisation will not occur.
10.4 Conditions to avoid Keep from direct sunlight.
10.5 Incompatible materials Strong acids and alkali.oxidizing materials, Aluminium, Zinc, Brass, Copper,
copper alloy, metals, Halogenated hydrocarbons. Do not use sodium nitrite or
other nitrosating agents in formulations containing this product. Carcinogenic
nitrosamines may be formed.
10.6 Hazardous decomposition product(s) Combustion may cause toxic fumes. Hazardous decomposition product(s):
Nitrogen oxides, Carbon monoxide, Carbon dioxide
SECTION 11: TOXICOLOGICAL INFORMATION

11.1 Information on toxicological effects (Substances in Substance characteristics: All test data taken from existing ECHA
preparations / mixtures) registrations for the substances mentioned.
Acute toxicity - Ingestion Mixture - Based upon the available data, the classification criteria are not met.
LD50 (rat) >2000 mg/kg bw/day (OECD 423)
Component 1 Not classified. LD50 (rat) >2000 mg/kg bw/day (OECD 401)
Component 2 Acute Tox. 4; Harmful if swallowed. Harmonised Classification
Acute toxicity - Inhalation Mixture - Based upon the available data, the classification criteria are not met.
Component 1 Not classified. No data.
Component 2 Not classified. Technically not possible.
Acute toxicity - Skin Contact Mixture - Based upon the available data, the classification criteria are not met.
Acute Toxicity Estimate Mixture Calculation: 4452.3 mg/kg bw/day
Component 1 Not classified. LD50 (rat) >2000 mg/kg bw/day (OECD 402)
Component 2 Acute Tox. 4; Harmful in contact with skin. Harmonised Classification
Skin corrosion/irritation Mixture - Based upon the available data, the classification criteria are not met.
Mixture Test Result (OECD 439)
Component 1 Skin Irrit. 2; Causes skin irritation. Harmonised Classification
Component 2 Skin Corr. 1B; Causes severe skin burns. Harmonised Classification
Serious eye damage/irritation Mixture - Eye Dam. 1; Causes severe damage to eyes.
Component 1 Eye Irrit. 2; Causes serious eye irritation. Harmonised Classification
Component 2 Skin Corr. 1B; Causes severe eye damage. Harmonised Classification
Respiratory or skin sensitization Mixture - Skin Sens. 1; May cause an allergic skin reaction.
Component 1 Respiratory sensitization: Not classified. No data.
Skin Sensitisation: Negative Guinea pig (OECD 406)
Component 2 Respiratory sensitization: Not classified. No data.
Skin Sensitisation: Skin Sens. 1; May cause an allergic skin reaction.
Harmonised Classification
Germ cell mutagenicity Mixture - Based upon the available data, the classification criteria are not met.
Component 1 In vivo: Negative mouse (OECD 474)
In vitro: Negative Bacteria (OECD 471)
Component 2 In vivo: Negative mouse EPA report 560/6-83-001
In vitro: Negative Bacteria (OECD 471)
Carcinogenicity Mixture - Based upon the available data, the classification criteria are not met.
Reproductive toxicity Mixture – Repr. 2; Suspected of damaging fertility or the unborn child.
Component 1 Reproductive toxicity: Not classified. NOEL 60 mg/kg bw/day Oral (rat) OECD


1272/2008 (CLP) & 2015/830
416
Developmental Toxicity: Not classified. NOEL 300 mg/kg bw/day Dermal (rat)
OECD 414
Component 2 Reproductive toxicity: No effects observed. NOEL 8,000 ppm Oral (rat) OECD
422
Developmental Toxicity: Positive NOAEL 75 mg/kg bw/day Oral (rabbit) OECD
414
STOT - single exposure Mixture - Based upon the available data, the classification criteria are not met.
Component 2 Not classified. Technically not possible.
STOT - repeated exposure
Ingestion Mixture - Based upon the available data, the classification criteria are not met.
Component 1 Not classified. NOAEL > 100 ppm (Dog) OECD 452
Component 2 Not classified. NOAEL 2000 mg/l Oral (rat) OECD 422
Inhalation Mixture – STOT RE. 2; Causes damage to organs through prolonged or
repeated exposure.
Component 2 STOT RE. 1; Causes damage to organs through prolonged or repeated
exposure by inhalation. NOEC Systemic effects 53.5 mg/m³
Dermal Mixture - Based upon the available data, the classification criteria are not met.
Component 2 Not classified. NOEL > 1000 mg/kg bw/day (rat) OECD 410
Aspiration hazard Mixture - Based upon the available data, the classification criteria are not met.
11.2 Other information None
SECTION 12: ECOLOGICAL INFORMATION

12.1 Toxicity Aquatic Chronic 3; Harmful to aquatic life with long lasting effects.
Mixture Estimated LC50 (96 hour) > 10 < 100 mg/l (Fish)
Component 1 Aquatic Chronic 3; Harmful to aquatic life with long lasting effects. Harmonised
Classification
Component 2 Aquatic Chronic 3; Harmful to aquatic life with long lasting effects. Harmonised
Classification
12.2 Persistence and degradability Part of the components are biodegradable.
Component 1 Readily biodegradable.
Component 2 Not biodegradable.
12.3 Bioaccumulative potential The substance has low potential for bioaccumulation.
Component 1 Low bioaccumulation potential.
Component 2 Low bioaccumulation potential.
12.4 Mobility in soil The product is predicted to have moderate mobility in soil.
Component 1 The substance has high mobility in soil.
Component 2 The product is predicted to have low mobility in soil.
12.5 Results of PBT and vPvB assessment No data for the mixture as a whole. None of the substances in this product fulfil
the criteria for being regarded as a PBT or vPvB substance.
Component 1 Not classified as PBT or vPvB.
Component 2 Not classified as PBT or vPvB.
12.6 Other adverse effects None known
SECTION 13: DISPOSAL CONSIDERATIONS

13.1 Waste treatment methods Dispose of contents in accordance with local, state or national legislation.
Dispose of this material and its container as hazardous waste (2008/98/EEC).
13.2 Additional Information Do not release undiluted and unneutralised to the sewer. Residues which cannot
be recycled are disposed off as chemical waste.Dedicated recollection
infrastructure required for waste.
SECTION 14: TRANSPORT INFORMATION

Not classified according to the United Nations ‘Recommendations on the Transport of Dangerous Goods’.


1272/2008 (CLP) & 2015/830
ADR/RID IMDG IATA/ICAO

14.1 UN number None assigned. None assigned. None assigned.
14.2 UN proper shipping name None assigned. None assigned. None assigned.
14.3 Transport hazard class(es) None assigned. None assigned. None assigned.
14.4 Packing group None assigned. None assigned. None assigned.
14.5 Environmental hazards Not classified. Not classified. Not classified.
14.6 Special precautions for user See Section: 2
14.7 Transport in bulk according to Annex II of MARPOL Not applicable. Not applicable. Not applicable.
73/78 and the IBC Code
14.8 Additional Information None.
SECTION 15: REGULATORY INFORMATION

15.1 Safety, health and environmental
regulations/legislation specific for the substance or
mixture
15.1.1 EU regulations The surfactants contained in this preparation comply with the biodegradability
criteria as laid down in Regulation (EC) No.648/2004 on detergents.
Authorisations and/or Restrictions On Use None
CoRAP Substance Evaluation Component 1: Substance identified for evaluation in 2017
15.1.2 National regulations
Wassergefährdungsklasse (Germany) Water hazard class: 3
15.2 Chemical Safety Assessment
Component 1 A REACH chemical safety assessment (CSA) has been carried out.
Component 2 A REACH chemical safety assessment (CSA) has been carried out.
SECTION 16: OTHER INFORMATION

The following sections contain revisions or new statements:
Section 8 Updated; PNECs and DNELs
Section 11 Additon of test data
Section 12 Additon of test data
Section 15 Updated S15.2
References: Safety Data Sheets for ingoing ingredients. and Existing ECHA registration(s) for: Mixture and Components
LEGEND
LTEL Long Term Exposure Limit
STEL Short Term Exposure Limit
DNEL Derived No Effect Level
PNEC Predicted No Effect Concentration
PBT PBT: Persistent, Bioaccumulative and Toxic
vPvB vPvT: very Persistent and very Toxic
OECD Organisation for Economic Cooperation and Development
Hazard Statement(s)
H302: Harmful if swallowed. H318: Causes serious eye damage.
H311: Toxic in contact with skin. H361: Suspected of damaging fertility or the unborn child.
H314: Causes severe skin burns and eye damage. H372: Causes damage to organs through prolonged or repeated exposure.
H315: Causes skin irritation. H412: Harmful to aquatic life with long lasting effects.
H317: May cause an allergic skin reaction.
Classification Procedure
Classification of the substance or mixture According to Classification Procedure

Regulation (EC) No. 1272/2008 (CLP)
Eye Dam. 1; H318 Threshold Calculation
Skin Sens. 1; H317 Threshold Calculation
Repr. 2; H361 Threshold Calculation


1272/2008 (CLP) & 2015/830
STOT RE. 2; H372 Threshold Calculation

Aquatic Chronic 3; H412 Summation Calculation
Training advice:
Consideration should be given to the work procedures involved and the potential extent of exposure as they may determine whether a higher level of
protection is required.
Disclaimers
Information contained in this publication or as otherwise supplied to Users is believed to be accurate and is given in good faith, but it is for the Users
to satisfy themselves of the suitability of the product for their own particular purpose. Carbon Clean Solutions Ltd. gives no warranty as to the fitness
of the product for any particular purpose and any implied warranty or condition (statutory or otherwise) is excluded except to the extent that exclusion
is prevented by law. Carbon Clean Solutions Ltd. accepts no liability for loss or damage (other than that arising from death or personal injury caused
by defective product, if proved), resulting from reliance on this information. Freedom under Patents, Copyright and Designs cannot be assumed.

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CUSTOMER LICENSOR

PROCESS DESIGN PACKAGE

Design and Engineering Package

5 TPD CO2 Capture Plant

TATA Steel Limited

CARBONCAPTURE TECHNOLOGIES PRIVATE LIMITED

Annexure – I: Solvent MSDS

DESIGN BASIS PROJECT

DOC. NO. TSL-DB-100

2. FEED GAS COMPOSITION

0 16.10.18 Issued for Engineering SL GK ARK

DESIGN BASIS PROJECT

DOC. NO. TSL-DB-100

3. Utilities to be supplied by TATA Steel at Battery Limits

0 16.10.18 Issued for Engineering SL GK ARK

DESIGN BASIS PROJECT

DOC. NO. TSL-DB-100

6. END PRODUCT (CO2 conditions at the battery limits)

7. PLANT LOCATION AND LOCAL CONDITIONS

0 16.10.18 Issued for Engineering SL GK ARK

DESIGN BASIS PROJECT

DOC. NO. TSL-DB-100

Unit numbering The general numbering philosophy of CCSL will be used.

0 16.10.18 Issued for Engineering SL GK ARK

DESIGN BASIS PROJECT

DOC. NO. TSL-DB-100

11. BATTERY LIMITS AND CONDITIONS

Following shall be battery limit temperature & pressure at battery limit.

S. No. Description P, bar g T,°C Location

0 16.10.18 Issued for Engineering SL GK ARK

DOC. NO. TSL-PD-200

0 02.11.18 Issued for Engineering SL GK ARK

DOC. NO. TSL-PD-200

0 02.11.18 Issued for Engineering SL GK ARK

DOC. NO. TSL-PD-200

0 02.11.18 Issued for Engineering SL GK ARK

DOC. NO. TSL-PD-200

2.4 SOLVENT STORAGE SECTION

0 02.11.18 Issued for Engineering SL GK ARK

DOC. NO. TSL-PD-200

0 02.11.18 Issued for Engineering SL GK ARK

LICENSOR: MATERIAL BALANCE DOC. NO. TSL‐HMB‐200

0 26.11.2018 Issued for Engineering SL GK ARK

Stream Number ‐ 10 11 12 ‐ Vapor 12 ‐ Liquid 13 14 ‐ Vapor 14 ‐ Liquid 15 16 17

0 26.11.2018 Issued for Engineering SL GK ARK

From Stripper Lean Solvent Pump LR Exchanger Lean Solvent Cooler Absorber Water Wash Column

0 26.11.2018 Issued for Engineering SL GK ARK

LICENSOR: MATERIAL BALANCE DOC. NO. TSL‐HMB‐200

0 26.11.2018 Issued for Engineering SL GK ARK

LICENSOR: MATERIAL BALANCE DOC. NO. TSL‐HMB‐200

0 26.11.2018 Issued for Engineering SL GK ARK

LICENSOR: MATERIAL BALANCE DOC. NO. TSL‐HMB‐200

WW Circulation WW Circulation Stripper

0 26.11.2018 Issued for Engineering SL GK ARK

DOC. NO. TSL-FC-800

S. No Fluid Name Fluid Code Remarks

4 CO2 Vapour CO2

7 Scrubbing Solution SAS

1 Cooling water Supply CWS

2 Cooling water Return CWR

5 LP Steam condensate LPC

0 02.11.18 Issued for Engineering SL GK ARK

PROCESS CONTROL DESCRIPTION