KUMAR ORGANIC PRODUCTS LIMITED Plot No. :379, Canal Road Maltr Marg, 5 Vill, Luna, Tal. Padra, Dist Vadodara-390039, Ph 02862-244016. Fax: 02662-24017 FINISHED PRODUCTS SPECIFICATION AND STANDARD TESTING PROCEDURE Name of the KOPTHIONE Reference In house Finished Products | (ZINC PYRITHIONE) 50% FPS Code KO006.2 Effective Date 20 Jou}rsib Specification No. | FPS/QC/007/07 Version No. 07 ‘Supersedes FPS/QCB/001/06~ STP No. 2 ~ FPT/QCB/001/07 Review Period APR - 2018 DEPARTMENT NAME SIGNATURE DATE Prepared By Quality Control ‘Mr. Sandeep Rai is Ss ra tafoyloord Reviewed By | Quality Control Mrs, Archana Dubey A fy pe _ figfoulzer Approved By | Quality Assurance Mr. Jaidev Dodiya ir \ 1b i 5 al? al Authorized By | Quality Assurance ‘Mr. Mukesh Patel “Fee breloujasg MASTER COPY Page 1 of 7es KUMAR ORGANIC PRODUCTS LIMITED Plot No. :379, Canal RoadMaitri Marg, Vill, Luna, Tal. Padra, Dist Vadodara-390038, Ph. 02662-244016. Fax: 02662-244017 FINISHED PRODUCTS SPECIFICATION Name of the KOPTHIONE Specification No. Version No. Finished - (ZINC PYRITHIONE) Products 50% FPS FPSIQCB/001/07 7 ‘Sr. Test(s) Specification(s) No. 01 | Appearance Off white aqueous dispersion, free from signs of impurities. eee ‘02 | Whiteness index on as is basis-using | Not less than 74.0 Konica Minolta Chromameter CR-400 03 | Identification by IR Conforms with the standard spectrum of Zinc Pyrithione 04 | Odour Very Mild Characteristic odour (05 [Assay (by Titrimetric Method) 48.0 - 50.0% wiv | 06 | Zinc Content (By Titrimetrie Method) | 9.3- 11.3% wiw 07 | PH 6% slurry in DM/ Distiled water. | 6.5-9.0 adjusted to PH 7) 08 | Particle Size Distribution Using 80% Particle are less than 1 micron Maivem Particle size analyzer Mastersizer 2000 with hydro 2000 S 09 [Iron (by AAS/ICP-OES) NMT 10.0 ppm = 10 | Heavy Metal (by AAS/ICP-OES) 10a | Arsenic NMT 3.0 ppm 105 [Lead ~ NMT 2.5 ppm 10e | Chromium NMT 3.0 ppm_ Tod | Cobalt NMT 3.0 ppm Te | Nickel NMT 5.0 ppm Tor | Mercury NMT {0 ppm—— = Total Heavy Metals NMT 20 ppm 11 | Microbiological Test Tia | Total plate countig NMT100 CFU/g (Including yeast and mold) Tip | Ecolig ‘Absent in 1g = Tic | Saureausig ‘Absent in 1g s Td | Pseudomonasig ‘Absentin 1g Tie | Enterobacterialg ‘Absentin 1g - MASTER COPYL KUMAR ORGANIC PRODUCTS LIMITED | Plot No. :379, Canal Road, Mati Marg, Vill. Luna, Tal. Padra, Dist Vadodara-390039 Ph, 02662-244016. Fax: 02662-244017 FINISHED PRODUCTS STANDARD TEST PROCEDURE Name of the KOPTHIONE ‘STP No. FPT/OCB/O01/07 Finished Products _| (ZINC PYRITHIONE) 50% FPS 01. Appearance: ‘Take small quantity about 1gm of sample in a Petridis and observe the color. 02, Whiteness: Fill the sample in a 50mI glass beaker, select the option illumination D65 in the instrument and dip the measuring head into the sample beaker. ve ‘Then press the measuring switch to checking whiteness index after beep sound result will display on screen (average of six reading will display) 03, Identification (by IR): ‘Sample Preparation _ take 200mg of ZPT 50% FPS and dry at 105°C for 30 min Procedure } Triturate about 3.0mg of the dried ZPT 50% FPS Sample with about 300mg of dry, finely powdered Potassium Bromide (IR Spectroscopy grade) ( Dry the KBr for minimum one hour at 105°C). Grind the mixture thoroughly, spread it uniformly in a suitable dye and compress under vacuum at a pressure of about 8 Tons. Carefully remove the pallet from the disc. If the pallet is not transparent reject and prepare another pallet in the same manner. Mount the pallet in the sample holder. Record IR spectrum from 4000cm-1 taking air as reference. The IR absorption spectrum of sample should be concordant with the spectrum from ZPT 50% FPS working standard recorded in the same manner (Remarks: Prepare a representative sample for IR analysis and sent to External Lab (KRC) and receives the analytical repots, it should be comply with the specification of the product. 04. Odor: ‘Take some sample in a Petri dish and smell it. 05. Ass: ‘Weigh accurately about 0.6 gm of ZPT 50% FPS into a 500 ml conical flask. Add 25 ml conc. HCl and | MASTER COPY Page 3 of 7