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Student’s Declaration:
I NAZERI ADBUL RAHMAN hereby certifies that the work entitled, INDUSTRIAL
TRAINING REPORT AT KUCHING WATER BOARD (BATU KITANG WATER
TREATMENT PLANT), KUCHING, SARAWAK (27 JUNE TO 4 SEPTEMBER 2016 )
was prepared by the above named student, and was submitted to the “FACULTY” as a *
partial KNF 3065 Industrial Training Course fulfillment for the conferment of
BACHELOR OF ENGINEERING WITH HONOURS (CHEMICAL ENGINEERING), and
the aforementioned work, to the best of my knowledge, is the said student’s work
Validation of Report
I therefore duly affirmed with free consent and willingness declared that this said Report
shall be placed officially in Department of Chemical Engineering and Energy
Sustainability with the abide interest and rights as follows:
Current Address:
NO 617, LORONG 20, TAMAN SAMARINDAH PHASE 2, JLN DATO MOHD MUSA,
94300 KOTA SAMARAHAN, SARAWAK
Report is submitted to
Faculty of Engineering, University Malaysia Sarawak
In Partial KNF 3065 Industrial Training Course Fulfillment of the
Requirements for the Degree of Bachelor of Engineering with Honors
(Chemical Engineering)
2016
Dedicated to my beloved parents, who always bestow me sustainable
motivations and encouragements
ACKNOWLEDGEMENT
First and foremost, the author would like to express utmost gratitude to
Kuching Water Board (KWB) especially to Batu Kitang Water Treatment Plant for
the opportunity given to undergo industrial training under Water Quality Control
(WQC) Unit. Apart from that, special thanks are dedicated to Mr. Wong Soon Sing, a
senior chemist and Mdm. Rahayu binti Ahmad Bohari, a chemist, for their guidance
The author would also like to toss earnest gratitude to Mr. Ngatiman bin Entol,
Mr. Ho Chin Guan, Mdm. Lo Siew Mee, , Mr John Bong, Mr. George Foreman, Mr.
Alin bin Amin, Mr. Chin Bui Phin, Mr Paul Jerry and Mr Sanusi Seman for their
willingness to share their knowledge and experiences through their warm attitude
towards the completion for the report and project. The deepest gratitude is also
extended to all staffs of KWB for their help, cooperation, knowledge and supervision
while doing this report. Lastly, the author would like to thank family and friends for
all supports and encouragement throughout the completion of the report. All
experiences and knowledge gained would not be possible without God’s permission.
RUMUSAN EKSEKUTIF
Latihan industri adalah wajib untuk semua pelajar Kejuruteraan Kimia dan
kemampanan Tenaga Universiti Malaysia Sarawak (UNIMAS). Ia adalah 10 minggu
latihan industri yang bermula pada 27 Jun 2016 dan tamat pada 04 September 2016.
Objektif utama latihan ini adalah untuk mendedahkan pelajar terhadap alam sekitar
kejuruteraan sebenar dan untuk meningkatkan kemahiran pemikiran teknikal dan
kritikal pelajar dalam melakukan aktiviti penyelidikan. Laporan ini bertujuan untuk
menyediakan laporan yang teratur berdasarkan pengalaman dan pengetahuan yang
diperolehi sepanjang tempoh internship di Loji Rawatan Air Batu Kitang KWB. KWB
adalah sebuah pertubuhan bukan keuntungan yang bertanggungjawab dalam
membekalkan air bersih kepada pengguna. Di bawah pengawasan Puan Rahayu binti
Ahmad Bohari, pelatih bertanggungjawab untuk melakukan penyelidikan projek
mengenai "Chlorine Residual Rendah dalam sistem pengagihan Loji Rawatan Batu
Kitang Air". Selain itu, semua aktiviti yang telah disertai oleh pelatih juga
dibincangkan dalam laporan ini
EXECUTIVE SUMMARY
5.0 CONCLUSION
5.1 Introduction 44
5.2 Experience Gained 44
5.2.1 Managerial Experience 45
5.2.2 Engineering Experience 45
5.2.3 Other Experiences 45
5.3 Summary 46
LIST OF REFERENCES 47
APPENDIX 48
LIST OF TABLES
Table Page
2.1 Batu Kitang water treatment plant and the location of distribution 8
tank
4.0 Residual chlorine and total coliform data at 15th Mile area 22
Sebubut Basin
4.26 38
pH Potential Hydrogen
km kilometer
CHAPTER 1.0: INTRODUCTION
This chapter will explains the overview and the purpose of this report including
the objectives for this 10 weeks industrial training. The schedule of the activities
participated by the trainee throughout the training period will be explain in this section.
1.1 Purpose of Report
The purpose of this report are to record all of the participated activities and the
training experiences in literature form including the opportunities to summarize their
experiences. By writing this industrial training report, students are able to practice
their writing skills and train them to write effectively for the preparation of Final Year
Project report writing. Besides that, the preparation, completion and submission of this
report helps in inculcating engineering skills in students.
1.2 Industrial Training Objectives
Industrial training is a compulsory program for all students in which it provide
supervised practical training. The training start from 27th June 2016 until 4th September
2016. The objectives of the industrial training are as follows:
i. To expose students to engineering experience and knowledge and
research activities which are not available during lecture session.
ii. To compare and practise the knowledge gained from the lecture with
the real situation.
iii. To use the experience and knowledge gained from industrial training
in the classroom.
iv. To familiarize students with the workplace environment after
graduation.
v. To gain experience in constructing reports for engineering works.
vi. To expose students toward engineering responsibility and engineering
ethics.
vii. To hope that the graduates will be able to choose an appropriate job
after graduation with the experience and knowledge gained throughout
the training period.
1.3 Industrial Training schedule
Within this 10 weeks of industrial training at Kuching Water Board at Batu
Kitang, many activities and tasks has been given by the supervisors to the trainee.
Trainee is placed under Water Quality Control (WQC) section under supervision of
Madam Rahayu binti Ahmad Bohari. Table 1.0 and Table 1.1 shows the lists of
activities and the Gantt chart of activities that has been participated by the trainee
throughout industrial training period.
Table 1.0: Task and training schedule of activities conducted by Water Quality
Control (WQC) department
Date Duration Task
Briefing
Safety plan
Project
1.4 Summary
The completion of the report help students enhancing their writing skills and
critical thinking skills in solving the problem related to water quality measurement.
Besides that, this industrial training gives valuable working experience and helps
student to enhance their practical skills and gives an opportunity to student to adapt
and understand the problems occurs while they in engineering working environment.
CHAPTER 2.0: COMPANY BACKGROUND
This section provides all the information regarding Kuching Water Board
(KWB) plant including the history of the company, company structure and company
main and auxiliary. KWB plant was established on January 1959 under Water Supply
Ordinance from Public Works Department, located nearby with Batu Kitang Bazaar
which is about 16 km from Kuching City and 1 km away from the bank of Sg. Sarawak
Kiri (raw water supply). KWB owned two water treatment plants which located at
Batu Kitang (Batu Kitang Water Treatment Plant) and Matang (Matang Water
Treatment Plant). Approximately about 97% of the whole water supplied are treated
at Batu Kitang Water Treatment Plant while the remaining 3% are treated at Matang
Water Treatment Plant. (KWB, 2013).
2.1 History of Kuching Water Board
Kuching Water Board (KWB) was first established on 1st January 1959 under
the Water Supply Ordinance 1959 to take over the existing Kuching Water Supply
which charged under Sarawak Public Works Department. Then on 1st January 1995,
the existing Water Supply Ordinance was replaced with Water Ordinance 1994
followed by the rebuilt of a board under Kuching Water Board in January 2001.
KWB has been operated as a government’s organization since 1959. It is a
non-profited organization that aims in providing a clean and high quality water supply
to the consumers around Kuching and nearby areas. At the first board’s establishment,
KWB only has one small water treatment plant of 18 MLD at Batu Kitang and a supply
from Matang Dam (16 MLD) that situated at 130 metres above sea level (KWB, 2013).
In 1975, the water demand outstripped the capacity of the two existing plants. Thus in
1976, Matang Storage Basin with capacity of 270 ML was established in order to
increase the reliability supply from Matang. Then in 1977, the capacity of Matang
Treatment plant was upgraded by 16 MLD as to support the water supply from Matang
Storage Basin (KWB, 2013). Table 2.0 shows the complete development of Kuching
Water Board Water treatment plant from year 1887 until year 2009.
Table 2.0: Development of water supply system in at Kuching, Sarawak (KWB,
2013)
Year Actions
1887 Construction of the first storage system where no water treatment was
yet to be introduced (0.455 MLD)
1902 Development of reservoir at Matang
1914 Flow record system was introduced at Matang (2.27 MLD)
1919 First water supply that crosses Sarawak River from Matang to Kuching
at Fort Magherita
1925 Addition of another water supply from Matang to Kuching
1952 Research and suggestion to build Batu Kitang Treatment Plant
1957 Construction of Plant 1, Module 1 (14 MLD) at Batu Kitang, Kuching
1959 Establishment of Kuching Water Board
1960 First bacteria disinfection system introduced at Matang Plant
1965 Upgrading Plant 1. Module 1, Batu Kitang Plant to 18 MLD
1966 Construction of plant at Matang (9 MLD)
1966 Introduction to fluoridation system
1970 Construction of Plant 1, Module 2, Batu Kitang Plant (9 MLD)
1976 Construction of reservoir at Sebubut (60 MLD)
1977 Upgrading Matang Plant to 16 MLD
1978 Construction of Plant 2, Module 3, Batu Kitang Plant (41 MLD)
1986 Construction of Plant 2, Module 4, Batu Kitang Plant (55 MLD)
1994 Construction of Plant 3, Module 5, Batu Kitang Plant (100 MLD)
1999 Upgrading Plant 1 to 68 MLD
2000 Construction of Plant 3, Module 6, Batu Kitang Plant (100 MLD)
2002 New raw water pipeline from Sg. Cina to Matang Plant and upgrading
live storage of Sebubut Storage Basin to 520 MLD
2005 Construction of weir across Sg. Sarawak Kiri to increase the safe yield
of raw water to an estimated 484 MLD
2006 Construction of Plant 4, Module 7, Batu Kitang Plant (100 MLD)
2011 Construction of plant 4, Module 8, Batu Kitang Plant (100 MLD)
Table 2.0 shows the development of Kuching Water Board treatment plant and
water treatment plant at Kuching, Sarawak started with the construction of Plant 1,
Module 1 at Batu Kitang in 1957 and followed by the construction and upgradation
the other three plants. Each plant consists of two modules in which each modules can
occupies varies water capacity.
KWB board member consists of four department which are Admin and Human
Resource (secretary), Deputy General Manager (planning, development and
production), Deputy General Manager (distribution) and Chief Accountant (Finance).
All this four department led by KWB General Manager, Mr. Mohd Sabari Bin
Shakeran. Meanwhile, eight units are divided under Deputy General Manager
(planning, development and production) , led by Wong Soon Sing which are
Development unit, Mechanical and electrical unit, GIS and network modelling unit,
Survey and rural water supply unit, Plant operation unit, Maintenance and transport
unit, Major development projects unit and Water quality section (WQS) unit. The
organization chart of KWB is shown in Figure 2.1.
Table 2.2 shows the operating statistic for Kuching Water Board Treatment
plant in May 2016. Each treatment plant was designed with specific capacity which
are 68, 96, 200, 200 and 16 MLD for Plant 1, Plant 2, Plant 3, Plant 4 and Matang
Plant respectively with total capacity of 580 MLD.
Table 2.2. : Monthly operating statistic for May 2016
Particular Plant 1 Plant 2 Plant 3 Plant 4 Matang Total
Plant
Design 68 96 200 200 16 580
Capacity
(MLD)
Average
Average 21.607 84.635 191.755 222.551 8.726 529.273
daily
production
(MLD)
Current 23.090 17.025 14.555 15.860 40.431 16.274
unit
production
cost
Based on Table 2.2, the total average daily production for every plant which
includes Kuching Water Board Treatment Plant and Matang Plant are 529.273 MLD
meanwhile the cost for current unit production are 23.090, 17.025, 14.555, 15.860,
40.431 for Plant 1, Plant 2, Plant 3, Plant 4 and Matang Plant respectively.
2.4 Water Treatment Process
KWB use raw water from Sungai Sarawak Kiri and treated the water before it
distribute to all residents around Kuching. There are several processes involves in
water treatment process in Sarawak which are Coagulation and Flocculation,
Sedimentation, Filtration, Disinfection, pH corrector and Fluoridation processes. The
complete steps of water treatment are illustrated in Figure 2.2.
Several parameter testing such as alkalinity, total hardness and total chloride
testing are still using a conventional method which is by titration instead of using
equipment in getting the results. Thus, this three parameter testing consumed more
time compared to other parameter testing. Based on Table 3.0, same type of equipment
which is Metro Spectrometer are used to test different types of parameter, residual
chlorine and Fluoride. However this two parameters uses different wavelength value
which are 515 nm and 570 nm for residual chlorine and fluoride test respectively.
Figure 3.1 shows Metro Spectrometer equipment which uses in residual chlorine and
fluoride testing.
Figure 3.1: Type of Metro Spectrometer used in WQC laboratory
Figure 3.2 shows the Alum parameter testing in treated water. This method
are used Colorimeter device as shown in Figure 3.3 to test the amount of Alum content
in the treated water from Module 1, 3, 4, 6, 7 and 8. However different method are
used while checking the quantity of Alum in raw water sample and mixing chamber
water sample. Figure 3.4 shows the method in testing Alum in raw water sample and
mixing chamber by using LoviBond Photometer device. Aluminium No.1 and
Aluminium No. 2 tablets are the chemicals used in Alum testing.
3.3 Summary
The main duty throughout the industrial training period is to do a research
regarding the “Loss of residual chlorine in distribution system at Batu Kitang water
treatment plant” under supervision of Madam. Rahayu binti Bohari. This research help
trainees in enhancing their critical thinking skills in solving problems and also their
practical skills in gaining data. Besides that, soft skills such as communication skills
among trainees and other staff members from other unit can also be improves while
conducting the research project. Apart from that, by doing daily water sample testing,
trainees are able to gain knowledge regarding the types of parameters and the
procedure used in parameter testing. Furthermore, the knowledge and method uses in
daily water sample testing can also be apply while doing the research project.
CHAPTER 4.0: INDUSTRIAL TRAINING DISCUSSION
In this section, detailed discussion on project involved and the activities that
has been participate by the trainee are provided.
4.1 Project Involved
In this section, several activities that has been participated by the trainee
throughout the industrial training period will be discusses in detailed. This section will
also include details information regarding the industrial training project which related
to the low residual chlorine in distribution system at Batu Kitang water treatment plant.
4.1.1 Low Residual chlorine in distribution system of Batu Kitang Water
Treatment Plant
A project entitled “ Low Residual Chlorine in distribution system of Batu
Kitang Water Treatment Plant” is assigned to the trainees. The duration given to
complete the project was about 4 weeks under supervision of Madam Rahayu. In the
completion of the project, trainee is achieving the following objectives:
i. To investigate the low residual chlorine in distributed water at
Kampung Santubong and 15th Mile
ii. To study the relationship between the number of bacteria presence in
water and low residual chlorine
iii. To investigate factors that affect the low residual chlorine in distributed
water at Kampung Santubong and 15th Mile
iv. To propose a solution for the problem of low residual chlorine in
distributed water at Kampung Santubong and 15th Mile
COLIFORM
COLIFORM
COLIFORM
COLIFORM
COLIFORM
COLIFORM
CL (ppm)
CL (ppm)
CL (ppm)
CL (ppm)
CL (ppm)
CL (ppm)
(MPN)
(MPN)
(MPN)
(MPN)
(MPN)
(MPN)
1 0.1 < 0.7 <1 0.1 < 0. < 0. < 1. <1
1 1 3 1 1 1 5
2 <0. < 0.1 <1 <0. < 0. 1 0. < 0. <1
1 1 1 1 1 1 1 3
3 0.1 < 0.1 <1 1 < 0. < 0. < 0. <1
1 1 1 1 1 1 3
4 <0. <
1 1
Mode 0.1 < 0.1 <1 <0. < 0. < 0. < 0. <1
1 1 1 1 1 1 1 3
Table 4.0: Residual chlorine and total coliform data at 15th Mile area [CL:
Residual chlorine, Coliform: Total coliform bacteria, : Violation ]
Based on Table 4.0, five residual chlorine violation while one total coliform
bacteria violation in 15th Mile has been investigated within 6 months. January and
May shows that three out of three water sample were analysed with low amount
of residual chlorine. Meanwhile in March, all of the treated water sample collected
at 15th Mile content less than 0.2 ppm total residual chlorine. Only two out of three
water sample are inadequate minimum amount of residual chlorine.
COLIFORM
COLIFORM
COLIFORM
COLIFORM
COLIFORM
CL (ppm)
CL (ppm)
CL (ppm)
CL (ppm)
CL (ppm)
CL(ppm)
(MPN)
(MPN)
(MPN)
(MPN)
(MPN)
(MPN)
0.35 1
0.9
0.3
0.8
0.25 0.7
0.6
0.2
0.5
0.15
0.4
0.1 0.3
0.2
0.05
0.1
0 0
January February March April May Jun
Figure 4.4: Residual chlorine and total coliform in distributed water at 15th Mile
0.45 25
0.4
0.35 20
0.3
15
0.25
0.2
10
0.15
0.1 5
0.05
0 0
January February March April May Jun
Figure 4.5: Residual chlorine and total coliform in distributed water at Kampung
Santubong
0.3
0.25
0.2
0.15
0.1
0.05
0
January February March April May Jun
Figure 4.6: Residual chlorine and total coliform in distributed water at 15th Mile
25
20
15
10
0
January February March April May Jun
Figure 4.7: Residual chlorine and total coliform in distributed water at Kampung
Santubong
Figure 4.9 :Distance from Batu Kitang Water Treatment Plant to Sampling Point at
15th Mile Jalan Kuching Serian.
The nearest chlorine dosing site for Kampung Santubong and 15th Mile is the Batu
Kitang Water Treatment Plant which is 48 km and 21 km away respectively. Figure
4.7 and Figure 4.9 shows the distance of Kampung Santubong and 15th Mile from
Batu Kitang Water Treatment plant respectively. These distances greatly exceed the
maximum distance in which residual chlorine can be maintained which is 19 km. Since
chlorine used for chlorination in the treatment plant is in gas form, residual chlorine
is difficult to be maintained over long distance. This is due to the volatile nature of
chlorine gas where it can easily escape through leakage along the pipeline as well as
through the pipeline joints.
Besides that, another factor that affects residual chlorine concentration is the
workers lack in skills especially in determining the ratio of chlorine and ammonia
during chlorination process in water treatment plant. Chlorine react with ammonia to
produce chloramines which consists of three different inorganic chloramines which
are monochloramine, dichloramine and trichloramine. Compared to free chlorine
compound, these three inorganic chloramines are much more persistent in water thus
it helps in slowing down the chlorine decay (Lenntech, 2016). The exact ratio of
chlorine and ammonia gas is 4:1. The dosage will be increase or decrease depending
on volume of water produced by the plant. However, an unskilled worker is unable to
determine the appropriate ratio of chlorine and ammonia based on volume of water
produced thus compromising the effectiveness of chlorination process.
Other than that, lack of skills in sampling process as well as ignoring the proper
process and procedures of taking water samples will also affect the concentration of
residual chlorine. Improper sampling techniques will alter the result of the residual
chlorine concentration. During sampling process, water from the sampling point
should be flushed for 10 minutes as shown in Figure 4.10 in order to remove stagnant
water and obtain fresh water. Stagnant water will record a lower residual chlorine since
all the chlorine has decay as well as escape through cracks and joints of the pipeline.
Residual chlorine obtained from stagnant water is not accurate as it does not represent
the actual residual chlorine concentration in water at that specific point of time. Fresh
water residual chlorine is more accurate as it represent the actual residual chlorine
concentration that is being supplied by the water treatment plant to the specific area at
that given time. Moreover, immediate testing should be done at the site of the sampling
point. The result of in-situ residual chlorine test is more reliable that laboratory testing
because the time taken for the samples to be taken back to the laboratory is longer
because of the distance. Delay testing will result in more residual chlorine decay thus
not providing a reliable result.
Figure 4.10: Worker performing flushing procedure before water sampling.
Another reason is insufficient chlorine dosing site which is only at Batu Kitang
Water Treatment Plant. Chlorine dosing is only done after sedimentation tank and at
the treated water tank as shown in Figure 4.11 which then will be distributed to water
users. Since the distance between Batu Kitang Water Treatment Plant, Kampung
Santubong and 15th Mile are situated at a great distance, more chlorine will decay
along the distribution pipeline which can cause residual chlorine violation. Thus, in
order to overcome this issue, more chlorine dosing site should be added. Other than
that, water sampling point should not be taken at the end of the distribution pipeline
since it gives inaccurate residual chlorine readings. This is because the water at the
end of the distribution pipeline becomes stagnant since there is minimal water flow
afterwards as there are less water users at the end of the pipeline.
Figure 4.11: Treated Water Tank at Batu Kitang Water Treatment Plant.
,
Figure 4.13: Independent Chlorine Dispenser (Aqua 8) (Aqua 8, 2015)
4.2 Activities
In the duration of ten weeks, several side activities has been participated by the
trainee which will be discussed in this chapter.
4.2.1 Site Visit to Batu Kitang Water Treatment Plant
In order to understand more regarding water treatment process in Batu Kitang
water treatment plant, trainees has been given an opportunity to visit the plants. During
site visit, trainees are able to analyse type of process involved in the plant and type of
risks that possibly occur at the plant. Several precaution need to be taken and followed
in order to reduce the risk of injury when visiting the water treatment plant. This
includes the uses of enclosed, flat shoes that must be worn for the duration of the tour,
any operating infrastructure, pipes, valves or controls must not be touched.
The first site visit was guided by Mr Sanusi Seman to plant 1 and plant 2 where
he was the one who responsible to explain the process involved in water treatment
plant. Each of plant consists of two modules in which plant 1 consists with module 1
and module 2 meanwhile plant 2 consists of module 3 and module 4. Both water
treatment at plant 1 and plant 2 are carried out by using conventional method with
high quantity of chemical dosage. The raw water from Sungai Sarawak Kiri are
pumped to mixing chamber where chemical dosing takes place. Then the raw water
will undergo coagulation, flocculation, sedimentation, filtration and disinfectants
process as mentioned in Chapter 2. All of the treated water from plant 1 is supplied to
Bau area while treated water from plant 2 is distributed to 9th Mile and Datuk Muda
Tank area.
On the same day, trainees are brought to visit the weir located nearby to Sungai
Sarawak Kiri. Weir is act as a barrier and it is a small overflow-type dam which
commonly used to raise the level of a river. The crest of an overflow spillway on a
large dam is often called a weir. At Batu Kitang, the salinity reading and TDS reading
during drought season are very high. Thus in order to overcome this problems, weir is
constructed to reduce the salinity intrusion especially during dry season. Besides that,
the construction of weir capable in preventing raw water shortage supply during low
level of water at Sungai Sarawak Kiri.
Figure 4.29: Tree planting by Mr Wong Soon Sing, Deputy General Manager
It is a simple but lively ceremony since the other staffs from other section such
as from Matang Water treatment plant, Bintawa store, Batu Kitang water treatment
plant were come together and joined the ceremony. Four location or also known as
zone has been prepared for tree planting ceremony at KWB Batu Lintang. There are
Zon Salju, Zon Jernih, Zone Pelangi and Zon Embun. Figure 4.29 shows Mr Wong
Soon Sing, Deputy General Manager for planning, development and production
during tree planting at Zone Embun.
Figure 4.30: Short briefing from Figure 4.31: Performance by the General
Mr Mohamad Sabari bin Manager and KWB staffs
Shakeran
Other than that, a very well-managed soft skills while dealing with different
people with different personality are also important in managerial field. Work ethic,
attitude, communication skills, emotional intelligence and other personal attributes are
the lists of soft skills that are crucial for career success. Due to friendly working
environment at KWB, trainee also tends to experience and enhance their soft skills by
getting along with people and displaying a positive attitudes towards other colleagues.
5.3 Summary
In conclusion, the objectives of this industrial training have been achieved
especially on environment exposure. 10 weeks duration of industrial training are able
to expose trainee towards real engineering environment and challenges. The
knowledge learnt in the university might not covered all the skills and knowledge used
in the industrial training. Working in a real environment is far different from the
learning in the university. Trainee also must have a strong determination to learn and
positive mind during industrial training process in which this will help the trainee to
be more capable to adapt towards engineering environment and any challenge
situations.
LIST OF REFERENCES
Aqua 8. (2015). Independent Chlorine Dispenser. Sarawak: Kuching Water Board
Batu Kitang
Chlor 8. (2015). Mengekalkan baki klorin dalam air terawat di system agihan.
Sarawak: Kuching Water Board Batu Kitang.
Environmental protection agency (EPA). (2016). Total Coliform rule. Available at:
https://www.epa.gov/dwreginfo/revised-total-coliform-rule-and-total-coliform-rule.
Accessed on: 3 August 2016.
KWB (2010). Selamat datang ke loji rawatan air Batu Kitang [ PowerPoint slides]
KWB (2013). Kuching water board annual report of 2013. Sarawak: KWB Batu
Kitang
Reagents:
1. Phosphate Buffer Solution
2. DPD Indicator solution
3. Potassium Iodise (KI) 20%
Procedure:
(a) Preparation of blank solution
1. Add 0.5 mL of Phosphate buffer solution and 0.5 mL of DPD indicator solution
in test tube.
2. Add 10mL of distilled water into the test tube to form blank solution. Mixed
well.
pH
Hazen/ Colour
Fluoride
Reagents:
1. SPANDS solution
Apparatus:
1. Test tube
2. spectrophotometer
Procedure:
1. Turn on the spectrophotometer.
2. Warm up until the spectrophotometer is stable( normally 15 – 30mins).
3. Set the wavelength
4. Put the Reference Solution into sample compartment.
5. Press the “0 ABS/ 100% T” key.
(a) Preparation of sample for fluoride determination
6. Measure 10 ml of water sample and pour into 50 ml dry test tube. Then add 2
ml of SPADNS Solution and mixed.
7. Transfer the sample to a spectrophotometer sample cell and raed the
“ABSORBANCE” reading from display of the spectrophotometer and
compare the reading to the calibration table provided.
Total Chloride
Apparatus:
1. Burette
2. Measuring Cylinder 100 ml
3. Conical Flask 250 ml
4. Pipette 1 ml
Reagents:
1. Potassium Chromate Indicator
2. Silver Nitrate
Procedure:
1. Place 50 ml of the sample in a conical flask, add 1 ml of potassium chromate
solution and titrate with silver nitrate solution with constant stirring until there
is the slightest perceptible reddish coloration die to the formation of silver
chromate.
2. Subtract 0.2 ml from titration figure to allow the excess of reagent required to
form silver chromate. If a water sample requires more than 25 ml of silver
nitrate solution, repeat the determination with suitable dilution
Reagents:
1. Sulphuric Acid N/10
2. Methyl Orange Indicator
Procedure:
1. Measure 125 ml of the sample into a conical flask. Add a few drops of methyl
orange indicator and mix.
2. Titrate over a white surface with N/10 standard acid to the proper equivalence
point. The indicator change to orange at pH 4.6 and pink at 4.0.
3. The endpoint is very faint orange while the comparison blank is constant
yellow.
Determination of Alkalinity
Total Alkalinity = (titrant x 4)ppm
Total Hardness
Apparatus:
1. Burette 50 ml
2. Conical Flask 100 ml
3. Measuring Cylinder 25 ml
4. pipette 1 ml
Reagents:
1. EDTA Solution
2. Buffer Solution
3. Solochrome Black Indicator
Procedure:
1. Measure 25 ml of the sample into a conical flask, add 0.5 ml of buffer solution and
mix. Then add 1-2 drops of indicator solution and mix. The solution alternatively
magnesium ion.
2. For exceptionally hard water, the indicator solution should be added before the
addition of buffer solution.
3. Titrate immediately with standard EDTA titrant 0.005M with continuous mixing.
The colour changes from purple to blue at end point.
4. Do not allow the time taken for the titration to exceed five minutes after adding the
buffer solution.
5. Remove from the water sample and clean it with distilled water.