Escolar Documentos
Profissional Documentos
Cultura Documentos
By
CHOKKAPU SYAM KIRAN
(Regd. No-315132920059)
2016-2019
TABLE OF CONTENT
1. LITERATURE
2. DECLARATION
3. AKNOWLEDGEMENT
Page | 2 4. ABSTRACT
5. LIST OF FIGURES
6. LIST OF TABLES
INTRODUCTION:
HEAT TRANSFER
TYPES OF HEAT TRANSFER
TYPES OF FLOWS
TYPES OF HEAT EXCHANGERS
WORKING PRINCIPLE OF SHELL AND TUBE
TYPES OF Fluid
HEAT TRANSFER BY HEAT EXCHANGER
REVIEW OF LITERATURE
TYPES OF NANO FLUIDS
SOLUBLE NANO FLUIDS
WORKING OF DI/AG+ NANO FLUID
WORKING OF DI/ALUM NANO FLUID
THERMAL ANALYSIS OF HEAT TRANSFER USING HEAT EXCHANGER
EXPERIMENT SETUP
1. AL 7075 T6 ALLOY CYLINDER PIPE WITH ANGULAR PASSAGES
2. SHELL AND TUBE TYPE HEAT CYLINDER
3. ELECTRONIC SKETCH
4. ELECTRICAL WIRING (LAYOUT)
Page | 3
CERTIFICATE
Mr. P.N.E NAVEEN M.Tech, (Ph.D.) Ms. M. CHAITANYA MAYEE M.Tech, (Ph.D)
Assistant Professor, Head of the Department
Dept. of Mechanical engineering, Dept. of Mechanical engineering,
S.V.P. Engineering College, S.V.P. Engineering College,
Visakhapatnam. Visakhapatnam.
EVALUATION SHEET
External Examiners :
Internal Examiner :
I am very much thankful to the principal Prof. (Dr.) RAMJEE, S.V.P. Engineering College for
his encouragement and cooperation to carry out this work.
I am very much thankful to Associate Prof. P.N.E NAVEEN & Associate Prof. D.RAVI
VIKRANTH, Department of Mechanical, S.V.P Engineering College for his encouragement
and cooperation to carry out this work.
I express sincere thanks to all the teaching staff and non-teaching staff of Department of
Mechanical for providing a great assistance in accomplishment of my project.
I am very much thankful to the management of S.V.P. Engineering College for their
encouragement and cooperation to carry out this work.
I would like to thank my parents, friends, and classmates for their encouragement throughout my
project period directly or indirectly in completing this project successfully.
record of an original work done by me for the award of the degree, Master of
This work is not submitted to any other institutions for award of other degree as it is
Forced convective heat transfer from a vertical circular tube conveying deionized
(DI) water or very dilute Ag-DI water Nano-fluids (less than 0.02% volume fraction)
Page | 7
in a cross flow of air has been investigated experimentally. Some experiments have
been performed in a wind tunnel and heat transfer characteristics such as thermal
conductance, effectiveness, and external Nusselt number has been measured at
different air speeds, liquid flow rates, and nanoparticle concentrations. The cross
flow of air over the tube and the liquid flow in the tube were turbulent in all cases.
The experimental results have been compared and it has been found that suspending
Ag nanoparticles in the base fluid increases thermal conductance, external Nusselt
number, and effectiveness. Furthermore, by increasing the external Reynolds
number, the external Nusselt number, effectiveness, and thermal conductance
increase. Also, by increasing internal Reynolds number, the thermal conductance
and external Nusselt number enhance while the effectiveness decreases.
The procedure consists of measuring the temperature of a certain heating material in
horizontal and vertical orientation. Experimental studies of forced convection heat
transfer from horizontal and vertical heat sources in carried out. It is conducted to
determine the effects of Reynolds number and nusselt number on heat transfer. The
air stream velocity was varied from (28 to 72) m/s to obtain the large range of the
Reynolds numbers .The experiment results for horizontal tubes are obtained for
range of Reynolds number (2.6 × 104 to 6.4 × 104), Nusselt number (37.75 – 226.98)
and for vertical tubes are obtained for the range of Reynolds number (4 × 104 to 6.9
× 104), Nusselt number (41.45 – 245.56). A correlation for the convective heat
transfer coefficients is obtained. The present experimental correlation is compared
with available correlation equations and experimental data. The comparisons show
very good agreement.
A correlation for convective heat transfer coefficient of Nano-fluids, based on
transport property and D/x for 8 mm tube has been evolved. The correlation predicts
variation in the local Nusselt number along the flow direction of the Nano-fluid. A
good agreement (±10%) is seen between the experimental and predicted results.
Page | 8
INTRODUCTION
• Surfaces, fins, mini-channels and micro-channels appears to be inadequate for the next
generation of electronic and optical devices. The other important areas that have also
experienced similar problems in thermal management are the areas of power generation,
chemical processing, air-conditioning, transportation, microelectronics and optical devices
which include lasers, high-power x-rays, optical fibers and communication devices.
Further enhancement in heat transfer is always in demand, as the operational speed of these
devices often depends on the cooling rate. Improving the thermal conductivity is the key
idea to improve the heat transfer characteristics in many heat transfer applications
conventional fluids, such as water, engine oil and ethylene glycol are normally used as heat
transfer fluids. Although various techniques are applied to enhance the configuration of the
heat transfer device, the low heat transfer performance of conventional fluids affects the
enhancement of performance, and in turn the compactness of heat exchangers, Thus the
usage of extended cs of conventional fluids. It is well known fact that metals in solid form
have higher thermal conductivities than those of fluids. It has been shown in many
references that, fluids containing suspended metal particles are expected to manifest
significantly enhanced thermal conductivities relative to pure fluids. The use of Nano size
solid particles as an additive suspended into the base fluid (nanofluids) is a technique for
the enhancement of heat transfer. Besides enhanced heat transfer, it is also found that the
nanofluids eliminate most of the problems arising with micro size slurries like
sedimentation, clogging of small channels, erosion, excessive pressure drop, etc. Thus,
nanofluids have greater potential for heat transfer enhancement and are highly suited to
application, in practical heat transfer processes. Investigation in convective heat transfer
characteristics of nanofluids is being carried out worldwide. One early study by Ahuja
showed the capability of micron sized polystyrene suspensions to enhance the convective
heat transfer under laminar flow conditions. The results showed significant enhancements
of Nusselt number and heat exchanger effectiveness when polystyrene spheres were added
to a single phase liquid. However, the use of micron sized particle colloids generally causes
particle settling, tube erosion and channel clogging. This issue has been eliminated with
the use of stable Nano sized particulate colloids, and this has paved way for researchers to
further investigate the enhancement of convective heat transfer with the addition of nano
sized particles. Pak and Cho experimentally investigated the hydrodynamic and convective
heat transfer characteristics of γ-Al2O3 particles suspended in water at 1-3% volume
concentrations. It was found that the Nusselt number for the dispersed fluids increased with
increasing volume concentration and Reynolds number. Eastman et al. conducted heat
transfer tests to assess the thermal performance of copper oxide and metallic nanofluids
under turbulent flow conditions. Results showed that the heat transfer coefficient of water
containing 0.9 vol. % of CuO nanoparticles was improved by more than 15% when
compared with pure water. Xuan and Li studied experimentally the single phase flow and
Page | 9 heat transfer performance of a nanofluid in tubes for the turbulent flow regime and
proposed a heat transfer correlation for the experimental data.
• Nanofluids in the entrance region under laminar flow conditions and proposed particle
migration to be a reason for the heat transfer enhancement. The nanofluids have higher
heat transfer coefficients than that of the base-fluids for the same Reynolds number. Such
improvements become more important with increases in the volume concentration of the
particle loading. A summary of published experimental investigations on convective heat
transfer performance of various nanofluids is presented in Table1
.
HEAT TRANSFER:
Heat transfer is a discipline of thermal engineering that concerns the generation, use, conversion,
and exchange of thermal energy (heat) between physical systems. Heat transfer is classified into
various mechanisms, such as thermal conduction, thermal convection, thermal radiation, and
transfer of energy by phase changes. Engineers also consider the transfer of mass of differing
chemical species, either cold or hot, to achieve heat transfer. While these mechanisms have distinct
characteristics, they often occur simultaneously in the same system.
Types of Heat Transfers
Convection describes heat transfer between a surface and a liquid or gas in motion. As the fluid or
gas travels faster, the convective heat transfer increases. Two types of convection are natural
convection and forced convection. In natural convection, fluid motion results from the hot atoms
in the fluid, where the hot atoms move upwards toward the cooler atoms in the air--the fluid moves
under the influence of gravity.
Heat transfer due to emission of electromagnetic waves is known as thermal radiation. Heat
transfer through radiation takes place in form of electromagnetic waves mainly in infrared region.
Radiation emitted by a body is a consequence of thermal agitation of its composing molecules.
TYPES OF FLOWS:
1. Laminar flow
2. Turbulent flow
3. Transitional flow
4. Steady flow and unsteady flow
5. Compressible and incompressible flow
6. Viscous and non-viscous flow
7. Rotational and irrotational flow
1. Laminar flow:
Occurs when the fluid flows in parallel layers, with no mixing between the layers. Where the center
part of the pipe flow the fastest and the cylinder touching the pipe isn’t moving at all.
Page | 11 The flow is laminar when Reynolds number is less than 2300.
2. Turbulent flow:
In turbulent flow occurs when the liquid is moving fast with mixing between layers. The speed of
the fluid at a point is continuously undergoing changes in both magnitude and direction.
The flow is turbulent when Reynolds number greater than 4000.
3. Transitional flow:
Transitional flow is a mixture of laminar and turbulent flow, with turbulence flow in the center of
Page | 12 the pipe and laminar flow near the edges of the pipe. Each of these flows behaves in different
manners in terms of their frictional energy loss while flowing and have different equations that
predict their behavior.
The flow is transitional when Reynolds number is in between 2300 and 4000.
Steady. In steady fluid flow, the velocity of the fluid is constant at any point.
Unsteady. When the flow is unsteady, the fluid’s velocity can differ between any two
points.
For example, suppose you’re sitting by the side of a stream and note that the water flow is not
steady: You see eddies and backwash and all kinds of swirling. Imagine velocity vectors for a
hundred points in the water, and you get a good picture of unsteady flow — the velocity vectors
can be pointing all over the map, although the velocity vectors generally follow the stream’s overall
average flow.
Fluid flow can be compressible or incompressible, depending on whether you can easily compress
the fluid. Liquids are usually nearly impossible to compress, whereas gases (also considered a
fluid) are very compressible.
A hydraulic system works only because liquids are incompressible — that is, when you increase
the pressure in one location in the hydraulic system, the pressure increases to match everywhere
in the whole system. Gases, on the other hand, are very compressible — even when your bike tire
is stretched to its limit, you can still pump more air into it by pushing down on the plunger and
squeezing it in.
Liquid flow can be viscous or non-viscous. Viscosity is a measure of the thickness of a fluid, and
very gloppy fluids such as motor oil or shampoo are called viscous fluids.
Viscosity is actually a measure of friction in the fluid. When a fluid flows, the layers of fluid rub
against one another, and in very viscous fluids, the friction is so great that the layers of flow pull
against one other and hamper that flow.
Viscosity usually varies with temperature, because when the molecules of a fluid are moving faster
(when the fluid is warmer), the molecules can more easily slide over each other. So when you pour
pancake syrup, for example, you may notice that it’s very thick in the bottle, but the syrup becomes
quite runny when it spreads over the warm pancakes and heats up.
Fluid flow can be rotational or irrotational. If, as you travel in a closed loop, you add up all the
components of the fluid velocity vectors along your path and the end result is not zero, then the
flow is rotational.
To test whether a flow has a rotational component, you can put a small object in the flow and let
the flow carry it. If the small object spins, the flow is rotational; if the object doesn’t spin, the flow
is irrotational.
For example, look at the water flowing in a brook. It eddies around stones, curling around
obstacles. At such locations, the water flow has a rotational component.Some flows that you may
think are rotational are actually irrotational. For example, away from the center, a vortex is actually
an irrotational flow! You can see this if you look at the water draining from your bathtub. If you
place a small floating object in the flow, it goes around the plug hole, but it does not spin about
itself; therefore, the flow is irrotational.
Page | 14 On the other hand, flows that have no apparent rotation can actually be rotational. Take a shear
flow, for example. In a shear flow, all the fluid is moving in the same direction, but the fluid is
moving faster on one side. Suppose the fluid is moving faster on the left than on the right. The
fluid isn’t moving in a circle at all, but if you place a small floating object in this flow, the flow on
the left side of the object is slightly faster, so the object begins to spin. The flow is rotational.
HEAT EXCHANGERS:
A heat exchanger is a device used to transfer heat between two or more fluids. Heat
exchangers are used in both cooling and heating process.
The fluids may be separated by a solid wall to prevent mixing or they may be in direct contact.
They are widely used in space heating, refrigeration, air conditioning, power
stations, chemical plants, petrochemical plants, petroleum refineries, natural-gas processing,
and sewage treatment.
The classic example of a heat exchanger is found in an internal combustion engine in which a
circulating fluid known as engine coolant flows through radiator coils and air flows past the
coils, which cools the coolant and heats the incoming air. Another example is the heat sink,
which is a passive heat exchanger that transfers the heat generated by an electronic or a
mechanical device to a fluid medium, often air or a liquid coolant.
Page | 15
Shell and tube heat exchanger design
There can be many variations on the shell and tube design. Typically, the ends of each tube are
connected to plenums (sometimes called water boxes) through holes in tube sheets. The tubes
may be straight or bent in the shape of a U, called U-tubes.
In nuclear power plants called pressurized water reactors, large heat exchangers called steam
generators are two-phase, shell-and-tube heat exchangers which typically have U-tubes. They are
used to boil water recycled from a surface condenser into steam to drive a turbine to produce
power. Most shell-and-tube heat exchangers are either 1, 2, or 4 pass designs on the tube side. This
refers to the number of times the fluid in the tubes passes through the fluid in the shell. In a single
pass heat exchanger, the fluid goes in one end of each tube and out the other.
The following are some of the most commonly used heat-transfer fluids and their properties.
Consult a solar heating professional or the local authority having jurisdiction to determine the
requirements for heat transfer fluid in solar water heating systems in your area.
Air
Air will not freeze or boil, and is non-corrosive. However, it has a very low heat capacity, and
tends to leak out of collectors, ducts, and dampers.
Water
Water is nontoxic and inexpensive. With a high specific heat, and a very low viscosity, it's easy
to pump. Unfortunately, water has a relatively low boiling point and a high freezing point. It
can also be corrosive if the pH (acidity/alkalinity level) is not maintained at a neutral level.
Page | 16 Water with a high mineral content (i.e., "hard" water) can cause mineral deposits to form in
collector tubing and system plumbing.
Glycol/water mixtures
Glycol/water mixtures have a 50/50 or 60/40 glycol-to-water ratio. Ethylene and propylene
glycol are "antifreezes." These mixtures provide effective freeze protection as long as the
proper antifreeze concentration is maintained. Antifreeze fluids degrade over time and
normally should be changed every 3–5 years. These types of systems are pressurized, and
should only be serviced by a qualified solar heating professional.
Hydrocarbon oils
Hydrocarbon oils have a higher viscosity and lower specific heat than water. They require more
energy to pump. These oils are relatively inexpensive and have a low freezing point. The basic
categories of hydrocarbon oils are synthetic hydrocarbons, paraffin hydrocarbons, and
aromatic refined mineral oils. Synthetic hydrocarbons are relatively nontoxic and require little
maintenance. Paraffin hydrocarbons have a wider temperature range between freezing and
boiling points than water, but they are toxic and require a double-walled, closed-loop heat
exchanger. Aromatic oils are the least viscous of the hydrocarbon oils.
These are commonly used as the heat transfer fluid in refrigerators, air conditioners, and heat
pumps. They generally have a low boiling point and a high heat capacity. This enables a small
amount of the refrigerant to transfer a large amount of heat very efficiently. Refrigerants
respond quickly to solar heat, making them more effective on cloudy days than other transfer
fluids. Heat absorption occurs when the refrigerant boils (changes phase from liquid to gas) in
the solar collector. Release of the collected heat takes place when the now-gaseous refrigerant
condenses to a liquid again in a heat exchanger or condenser.
Silicones
Silicones have a very low freezing point, and a very high boiling point. They are noncorrosive
and long-lasting. Because silicones have a high viscosity and low heat capacities, they require
more energy to pump. Silicones also leak easily, even though microscopic holes in a solar loop.
REVIEW OF LITERATURE
The addition of nanoparticles to improve the thermo physical properties of fluids has been studied
Page | 17 since the mid- 1990s, but it was only in the early 2000s the first experimental study on Nano-fluids
heat transfer was published. Since then, around 2000 publications on experimental studies with
Nano-fluids have been presented, of which nearly 50% belong to the last 3 years.
The compilation of data which is presented here, is based on an under-development database which
collects experimental data of several thermo physical properties, isobaric heat capacity, thermal
conductivity k, and dynamic viscosity for a number of Nano-fluids consisting of a pure fluid or
binary mixture, and a single type of nanoparticles. As a function of the studied property,
nanoparticle, and base fluid. As it can be observed, the number of studies on aqueous Nano-fluids
exceeds the rest, in the same way that the most studied nanoparticles are Al2O3 and CuO, which
could be a consequence of their lower cost.
Reynolds number:
Reynolds number is the ratio of inertial forces to viscous forces within a fluid which is subjected
to relative internal movement due to different fluid velocities, which is known as a boundary
layer in the case of a bounding surface such as the interior of a pipe. A similar effect is created by
the introduction of a stream of higher velocity fluid, such as the hot gases from a flame in air. This
relative movement generates fluid friction, which is a factor in developing turbulent flow.
laminar flow occurs at low Reynolds numbers, where viscous forces are dominant, and is
characterized by smooth, constant fluid motion;
Turbulent flow occurs at high Reynolds numbers and is dominated by inertial forces, which
tend to produce chaotic eddies, vortices and other flow instabilities. The Reynolds number is
defined as
Nusselt Number:
The Nusselt number is a dimensionless number, The Nusselt number is used to describe the
ratio of the thermal energy convected to the fluid to the thermal energy conducted within the
fluid. Nusselt number is equal to the dimensionless temperature gradient at the surface, and it
Page | 18 provides a measure of the convection heat transfer occurring at the surface. The conductive
component is measured under the same conditions as the heat convection but with a stagnant
fluid. Thus, the Nusselt number is defined as:
Prandtl Number:
Depends only on fluid & its properties.
It is the ratio of momentum diffusivity to heat diffusivity of the fluid.
It is also the ratio of velocity boundary layer to thermal boundary layer.
Pr = small, implies that rate of thermal diffusion (heat) is more than the rate of
momentum diffusion (velocity). Also the thickness of thermal boundary layer is much larger
than the velocity boundary layer.
Grashof Number:
Ratio of Buoyancy force to viscous force in natural convection.
Reynolds number is used in forced convection of fluid flow, whereas Grashof
number is used in natural convection
.
ABOUT NANO FLUIDS
• A Nano-fluid is a fluid containing nanometer-sized particles, called nanoparticles. These
fluids are engineered colloidal suspensions of nanoparticles in a base fluid. The
Page | 19 nanoparticles used in Nano-fluids are typically made of metals, oxides, carbides, or carbon
nanotubes. Common
• Base fluids include water, ethylene glycol and oil.
• Nano-fluids have novel properties that make them potentially useful in many applications
in heat transfer,[4] including microelectronics, fuel cells, pharmaceutical processes,
and hybrid-powered engines,[5] engine cooling/vehicle thermal management, domestic
refrigerator, chiller, heat exchanger, in grinding, machining and in boiler flue gas
temperature reduction. They exhibit enhanced thermal conductivity and the
convective heat transfer coefficient compared to the base fluid. Knowledge of
the rheological behavior of Nano-fluids is found to be critical in deciding their suitability
for convective heat transfer applications. Nano-fluids also have special acoustical
properties and in ultrasonic fields display additional shear-wave reconversion of an
incident compressional wave; the effect becomes more pronounced as concentration
increases.
• In analysis such as computational fluid dynamics (CFD), Nano-fluids can be assumed to
be single phase fluids; however, almost all new academic papers use a two-phase
assumption. Classical theory of single phase fluids can be applied, where physical
properties of Nano-fluid is taken as a function of properties of both constituents and their
concentrations. An alternative approach simulates Nano-fluids using a two-component
model.
• The spreading of a Nano-fluid droplet is enhanced by the solid-like ordering structure of
nanoparticles assembled near the contact line by diffusion, which gives rise to a
structural disjoining pressure in the vicinity of the contact line. However, such
enhancement is not observed for small droplets with diameter of nanometer scale, because
the wetting time scale is much smaller than the diffusion time scale
Nano-fluid, which is a term used to describe fluids containing dispersed particles of nano scale,
can be formed from nanoparticles of single element (e.g., Cu, Fe, and Ag), single element oxide
(e.g., CuO, Cu2O, Al2O3, and TiO2,), alloys (e.g., Cu-Zn, Fe-Ni, and Ag-Cu), multi element
oxides (e.g., CuZnFe4O4, NiFe2O4, and ZnFe2O4), metal carbides (e.g., SiC, B4C, and ZrC),
metal nitrides (e.g., SiN, TiN, and AlN), and carbon materials (e.g., graphite, carbon nanotubes,
and diamond) suspended in water, ethanol, EG, oil, and refrigerants. They can be classified into
two main categories: single material Nano-fluids and hybrid Nano-fluids.
Page | 20 This category of Nano-fluid was first proposed by Choi, in 1995, and is considered as the
conventional form of Nano-fluids used, where a single type of nanoparticles is used to produce the
suspension via different preparation methods [5]. It was reported by many authors that Nano-fluids
of such category are superior in performance, due to having much more favorable thermo physical
properties than their base fluid.
Hybrid Nano-fluids
Hybrid Nano-fluids are an advanced category of Nano-fluids which are made of a combination of
more than one type of nanoparticles suspended in a base fluid. This type of fluids was first studied
experimentally by Jana et al., in 2007, in order to enhance the fluid thermal conductivity beyond
that of a conventional single material type Nano-fluid. In their study, Cu nanoparticles, carbon
nanotubes (CNTs), and Au nanoparticles dispersed in water, as well as their hybrids (CNT–
Cu/H2O and CNT–Au/H2O) were examined. The results showed that the thermal conductivity of
Cu/H2O Nano-fluid was the highest among the tested samples and increased linearly with the rise
of particle concentration. Nevertheless, the stability of the CNT–Cu/H2O Nano-fluid achieved
longer settling time than the other types of Nano-fluids. This enables the fluid to conserve its
thermal conductivity much longer before degrading.
Table 3
A selection of thermal conductivity measurements from several Nano-fluid studies.
Thermal
Particle
Nanoparticle Working Fluid Fraction Enhancement Reference
Size (nm)
(%)
Metals
Thermal
Particle
Nanoparticle Working Fluid Fraction Enhancement Reference
Size (nm)
Page | 21 (%)
0.3–0.9
Ag <100 Water 30 at 50 °C [50]
vol %
0.1–1.0
Ag 100–500 Ethylene Glycol 18 [205]
vol %
0.01–0.05
Cu <10 Ethylene Glycol 41 [67]
vol %
0.1–0.55
1Fe 10 Ethylene Glycol 18 [103]
vol %
Metal Oxides
2–10 vol
Al2O3 9 Water 29 [207]
%
Thermal
Particle
Nanoparticle Working Fluid Fraction Enhancement Reference
Size (nm)
Page | 22 (%)
Water/Ethylene
Al2O3 28 3–8 vol % 41 [100]
Glycol
0.5–4 vol
Al2O3 650–1000 Transformer oil 20 [208]
%
0.5–5 vol
TiO2 15 Water 30 [159]
%
Carbons
4.4–7.7
Carbon Black 190 Water 10 at 35 °C [55]
vol %
Thermal
Particle
Nanoparticle Working Fluid Fraction Enhancement Reference
Size (nm)
Page | 23 (%)
Dia. 10–50
0.25–1 vol
SWCNT Len. 0.3– Diesel Oil 10–46 [212]
%
10 µm
25 nm ×
MWCNT Oil 1 vol % 150 [79]
50 µm
Dia. 10
Gum Arabic & 0.14-0.24
MWCNT Len. 5–15 10 [213]
Water vol %
µm
A selection of carbon allotropes that have been examined for use in Nano-fluids.
Nano-Diamond Nano-fluids
In recent years, several researchers have appraised the thermal conductivity properties of Nano-
diamond Nano-fluids. Studies by Ghazvini et al. investigated Nano-fluids composed of
water/engine oil mixtures and small quantities of Nano-diamonds (ND). They found the addition
of small mass fractions (~1.0 wt %) could produce thermal conductivity enhancements of around
25%. While studies by Ma et al. found the addition of small quantities of NDs (0.01 vol %) to
water-based Nano-fluids increased the pure waters thermal conductivity from 0.581 W m−1K−1 to
1.003 W m−1K−1.
Preparation of Nano-fluids
Uniformity of the particle dispersion depends mainly on the preparation method used and can
have a significant effect on the thermo physical properties of the Nano-fluid. Meaning that if two
similar Nano-fluids were to be prepared using different preparation methods, their thermo
physical properties and tendency to agglomeration are most likely to vary from each other. This
is because Nano-fluids are not simply formed from a solid-liquid mixture but requires special
conditions to be present in the suspension such as homogeneity, physical and chemical stability,
durability, and dispersibility. There are mainly two techniques used to fabricate Nano-fluids,
namely, the bottom-up approach known as the one-step method and the top-down approach
identified as the two-step method.
Stability of Nano-fluids
Part of the challenges that faces commercializing Nano-fluids is their poor stability due to the
interaction between the particles themselves and between the particles and the surrounding liquid.
This kind of behavior can be linked to two opposing forces: the well-known Van der Waals
attractive forces on the particles surface which causes the particles to be attracted to each other
into forming clusters or agglomerations of particles and then separate from the base-fluid and settle
at the bottom due to gravitational force and the electrical double layer repulsive force which tends
to separate the particles from each other via steric and electrostatic repulsion mechanisms.
NANOFLUID PREPARATION AND STABILIZATION
The process of preparation of Nano-fluid and stabilization is an important activity since
extracting the benefits of nanoparticle in thermal cycle needs proper preparation and stabilization.
Page | 26
Poorly prepared Nano-fluids results in biphasic heat transfer (i.e. solid–liquid). Particle instability
results in particle fouling in reservoir, pipes, pumps and other equipment of thermal cycle, as well
as reduced pressure, all of which are considered undesirable factors in our experiment.
The nanoparticles used in this study were Silver oxide and copper oxide nanoparticles of
approximately 15 nm in diameter and 95% purity. As for the AG+/Water Nano-fluid, samples of
0.1% to 0.3%, fluid were prepared without surfactants solely with magnetic stirring for 1 h and
subsequent ultrasonic irradiation for 2 h. These samples proved highly appropriate in terms of
homogenous dispersion and long term stability. As for the CuO/EG Nano-fluid, samples of 0.1%
to 0.3% weight copper oxide in base fluid (EG) were prepared using the surfactant sodium dodecyl
sulfate (SDS) alongside magnetic stirring for 1 h and subsequent ultrasonic irradiation for 2 h.
These samples proved appropriate for a cyclic system in terms of homogenous dispersion and long
term stability. The fig 1 (a) and (b) shows the SEM image of CuO and DI/AG+ Nano-fluid. The
particles are homogenously dispersed throughout the base-fluid in an acceptable fashion.
pH Control of Nano-fluids:
Manipulating the pH value of Nano-fluids changes the nanoparticles surface and can strongly
improve the stability of the dispersed nanoparticles. This is because the stability of a Nano-fluid
is directly related to its electro kinetic properties. Therefore, the zeta potential can be
increased/decreased by changing the pH value of the Nano-fluid and as mentioned previously, zeta
potential values of Nano-fluids above +30 mV or below −30 mV are considered to be more stable
because of the high repulsive force generated between the charged nanoparticles. The pH value of
a Nano-fluid can be increased or decreased by adding an appropriate nonreactive alkaline or acidic
solution, respectively.
Many studies were carried out to demonstrate the effect of pH level on the stability of Nano-fluids.
Witharana et al. examined the settling and aggregation behavior of alumina (Al 2O3)/H2O Nano-
fluid of 0.5 wt%, 46 nm particle size, and of spherical particle shape at pH values of 6.3 and 7.8.
They discovered that the suspensions were stable at a pH value of 6.3 for more than 30 min
compared with the pH value of 7.8 which had endured a complete particle separation and
settlement after 30 min. Manjula et al. studied in their work the effect of added surfactants and pH
level on the dispersion behavior of water based alumina Nano fluid through its sedimentations.
Their results showed that adding surfactant and optimizing the pH level maximized the stability of
the Nano-suspension. Zhu et al. investigated the influence of different concentrations of SDBS and
pH values on the behavior of Al2O3/H2O suspension. They found out that the effective thermal
conductivity and stability of their Nano-fluid were significantly dependent on the SDBS
concentration and pH value of the fluid, where the effective thermal conductivity was increased
by 10.1% at a pH value of 8 and particle concentration of 0.15 wt%.
WORKING OF DI/AG+ NANO FLUID:
Silver nanoparticles have unique optical, electrical, and thermal properties and are being
incorporated into products that range from photo-voltaics to biological and chemical sensors.
Page | 27 Examples include conductive inks, pastes and fillers which utilize silver nanoparticles for their
high electrical conductivity, stability, and low sintering temperatures. Additional applications
include molecular diagnostics and photonic devices, which take advantage of the novel optical
properties of these Nano-materials. An increasingly common application is the use of silver
nanoparticles for antimicrobial coatings, and many textiles, keyboards, wound dressings, and
biomedical devices now contain silver nanoparticles that continuously release a low level of silver
ions to provide protection against bacteria.
Figure 1: Transmission electron microscopy (TEM) images of silver nanoparticles with diameters
of 20 nm, 60 nm, and 100 nm respectively. Scale bars are 50 nm.
Understanding how the size, shape, surface, and aggregation state of the silver nanoparticles
change after integration into a target application is critical for optimizing performance. We offer
precisely manufactured mono-disperse silver nanoparticles that are free from agglomeration,
making them ideal for research, development, and use in a variety of innovative applications
(Figure 1). Each batch of nanoparticles is extensively characterized using transmission electron
microscopy (TEM) images, dynamic light scattering (for particle size analysis), Zeta potential
measurements, and UV/Visible spectral analysis to ensure consistent materials in every order.
Figure 2: (Left) Surface plasmon resonance where the free electrons in the metal nanoparticle are
driven into oscillation due to a strong coupling with a specific wavelength of incident light.
(Right) Dark field microscopy image of 60 nm silver nanoparticles.
Figure 3. (Left) Extinction (scattering + absorption) spectra of silver nanoparticles with diameters
ranging from 10-100 nm at mass concentrations of 0.02 mg/mL. (Right) Extinction spectra of
silver nanoparticles after the addition of a destabilizing salt solution.
For silver nanoparticle solutions that have not agglomerated and have a spectral shape that is
identical to the as-received suspension, the UV/Visible extinction spectra can be used to quantify
the nanoparticle concentration. The concentration of silver nanoparticle solutions is calculated
using the Beer-Lambert law, which correlates the optical density (OD, a measure of the amount of
light transmitted through a solution) with concentration. Due to the linear relationship between
OD and concentration, these values can be used to quantify the concentration of nanoparticle
solutions.
Diagnostic Applications: Silver nanoparticles are used in biosensors and numerous assays
where the silver nanoparticle materials can be used as biological tags for quantitative
detection.
Antibacterial Applications: Silver nanoparticles are incorporated in apparel, footwear,
paints, wound dressings, appliances, cosmetics, and plastics for their antibacterial
properties.
Conductive Applications: Silver nanoparticles are used in conductive inks and integrated
into composites to enhance thermal and electrical conductivity.
Optical Applications: Silver nanoparticles are used to efficiently harvest light and for
enhanced optical spectroscopies including metal-enhanced fluorescence (MEF) and
surface-enhanced Raman scattering (SERS).
THEORITICAL ANALYSIS:
Page | 31 Shell and tube type heat exchangers are designed normally by using Kern’s method. Kern’s method
is mostly used for the preliminary design. In this we have designed a simple shell and tube type
heat exchanger to heat water from 40℃ to 70℃ by using steam at 140℃ temperature by using
Kern’s method. The steps of designing are described as follows:
a) First we consider the energy balance to find out the values of some unknown temperature values.
Certainly some inputs like hot fluid inlet and outlet temperatures, cold fluid inlet temperature, and
mass flow rates of the two fluids are needed to serve the purpose. The energy balance equation
may be given as: Q = mh Cph (ݐℎ1-ݐℎ2) = mCc (tc2-tc1)
b) Then we consider the LMTD expression to find its Value: LMTD = (ΔT1−ΔT2) / In (ΔT1/ΔT2)
Where, ΔT1 = th1-tc2 and ΔT2 = tℎ2-tc1.
c) Our next step is to calculate the area required of the heat exchanger (on the basis of assumed
U0), number of tubes, tube bundle diameter, diameter of shell and its thickness with the help of
following expressions:
A = Q / (UoΔT) Nt = A / (πdtol) Db = dto (Nt / K1)1/n1 Di = Db + additional clearance Do = Di
+ 2 × thickness
d) Then we calculate the proper baffle dimension viz. its diameter, thickness and baffle spacing.
e) Our next step is to find out heat transfer coefficients on the inner and outer surface of the tubes
using following correlation: 1/U = (1/Ui) + (/Uo)
f) Then by the values obtained by the above equation we calculate the actual value of heat transfer
coefficient and check whether the actual value is greater than the assumed one or not.
In the present project, the methodology used in the design of the heat exchanger is studied and
presented. The thermal design involves the calculation of shell side and tube side heat transfer
coefficients, heat transfer surface area and pressure drops on the shell side and tube side. The
mechanical design involves the calculations of thickness of pressure parts of the heat exchanger
such as the shell, channel, tube etc. to evaluate the rigidity of part under design pressures. The
design of the heat exchanger is then modeled in Pro-Engineer and finally analyzed using ANSYS
software. In this system oil is taken as hot fluid and cold fluid is water. Where no phase change
occurs.
EXPERIMENTAL SETUP:
Al 7075 T6 ALLOY CYLINDRICAL PIPE WITH ANNULAR PASSAGES:
• A vertical test section was casted by preparing a furnace. The furnace is prepared by using
cylindrical steel tin. In that tin insulating material PLASTER OF PARIS is placed at the
internal surface of tin.
• A hole was prepared at the lower end of tin and a steel pipe was welded at the hole to flow
Page | 32
the blower air into the furnace.
• The whole internal section was coated with POS.
• In forging l, we prepared the pattern by using wooden piece and make it like the annular
passage. The wooden piece is placed at centre of cope box and rammed the sand into the
box. After completing this process we removed the pipe from box.
• During casting process, the aluminum metals were melted by using the furnace.
• The molten metal was poured into the cavity of test section. After passage of molten metal
by the cavity the test section was prepared.
• The test section was prepared by removing the boxes by ramming process.
• A number of holes of diameter 6mm are drilled on one side of test section to insert the
thermocouples.
FRAME:
• By using ¾ sized angular was welded by arc welding process into a closed rectangular
shaped frame. The edges are welded and grinded.
• At distance of 35cm from one side of frame another rectangular block should be welded to
place the Heater inside.
• On the side from a distance of 10cm two angulars of size 15mm are welded perpendicular
to surface to hold the vertical test section.
• Sheet metal process was done by adding screws to the angular and the whole frame was
closed by the sheet metal.
• A hole is prepared at another side to place the blower hole.
THERMOCOPLES:
• Thermocouples are connected to the aurduno board to visualize the readings of
temperatures inside the chamber and test section.
• Two thermocouples are used to know the temperature at inlet and chamber T1 AND T2.
• Four thermo couples are used to know the temperature inside the vertical test section T3,
T4, T5 andT6.
CONTROL PANEL:
• Control panel was made by wooden board, the placements of the switches and plug points,
temperature monitors, aurdino board and fuse.
• Plug point are placed to supply power to heater and blower.
Page | 33
1. FRAME CVERED WITH SHEET METAL 2.VERTICAL TEST SECTION & TANK
TANK:
The Nano-fluid is stored in the tank besides to the vertical test section.
Two motors are connected to the copper tubes in order to pump the fluid through pipes in
vertical test section.
REFERENCES
1. Y.M. Xuan, Q. Li, Investigation on convective heat transfer and flow features of nanofluids,
ASME J. Heat Transfer, 125 (2003), 151-155.
2. S. Zeinali Heris, M. Nasr Esfahany, S.Gh. Etemad, Numerical investigation of nanofluid
laminar convective heat transfer through circular tube, J. Numer. Heat Transfer A: Appl. 52
(2007), 1043–1058.
3. S.U.S. Choi, Developments and Application of NonNewtonian Flows, ASME FED-
V.231/MD-V.66, New York, 1995, pp.99–105.
4. S. Lee, S.U.S. Choi, S. Li, J.A. Eastman, Measuring thermal conductivity of fluids containing
oxide nanoparticles, J. Heat Transfer, 121 (1999), 280–289.
5. Y. Xuan, Q. Li, Heat transfer enhancement of nanofluids, Int. J. Heat Fluid Flow 21 (2000),
58–64.
6. D. Wen, Y. Ding, Experimental investigation into convective heat transfer of nanofluids at
the entrance region under laminar flow conditions, Int. J. Heat Mass Transfer 47 (2004),
5181–5188.