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JANUARY 2018
years

129
The technical service magazine for the rubber industry Volume 257, No. 4

Prediction of rolling resistance factor


with a rebound resilience tester

Characterization of rubber compounds

Rheology of EPDM compounds


made of equal Mooney, equal composition polymers

Characterizing rubber’s resistance


against chip and cut behavior

Instrumentation/Testing Labs Directories


www.rubberworld.com

ACS Events, page 74

@rubberworld
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Contents Vol. 257, No. 4 January 2018

FEATURES
JANUARY 201
8

22 Prediction of rolling
years

129
The technical

resistance factor (RRF)


service mag
azine for the
rubber indu
stry Volume 257
, No. 4

by S.L. Agrawal, B.B. Sharma and Virendra


Rathod, Reliance Industries Ltd., India. Rolling
Prediction of
resistance factor of conveyor belt cover with a rebou rolling resis
nd resilience tance factor
tester
compounds is examined. Characterizat
ion of rubber
compounds
Rheology of
EPDM comp

25 Characterization of
made of eq ounds
ual Mooney,
equal composition
polymers
Characterizing
rubber

rubber polymers and cut behav ’s resistance


against chip
ior

Instrumentat
by Alina K. Latshaw and Thomas Rauschmann, ion/Testing
Labs Director
ies
TA Instruments Waters. Advanced rheological

.comorld
measurements are correlated to polymer chain

www.rubberw
architecture. ACS Events
, page 74

31
@rubberworl

Rheology of EPDMs
d

by Juan Tuberquia, Colin Li Pi Shan, Sharon Cover photo: Courtesy of MonTech


Wu, Greg Li, Lena Nguyen, Teresita Kashyap,
Tianzi Huang, David Gillespie, Cory Thomas and
Kristel Blackwell, Dow Chemical. The rheology
of EPDM compounds made of equal Mooney, 41 Instrumentation and
equal composition polymers is assessed. testing laboratories
directories
38 Cut and chip resistance
by Radek Stocek, PRL Polymer Research
Directories provide products, services
and contact information for independent
Laboratory; William V. Mars and Christopher testing laboratories serving the rubber
G. Robertson, Endurica LLC; and Rheinhold industry, and suppliers of rubber
Kipscholl, Coesfeld GmbH. Analytical methods instrumentation and test equipment.
to characterize the fracture of rubber Cross-referenced grids match companies
occurring during lab-simulated operation of to the products and/or services they
tire tread in rough terrain are described. provide.

DEPARTMENTS Digital Edition Content


4 Editorial See the January digital edition of
Rubber World for additional content
7 Business Briefs not found in the print edition
12 Market Focus
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14 Silicone/Medical Update  ‡([SDQGHGEXVLQHVVQHZV
16 The Rubber Economist  ‡([SDQGHGHTXLSPHQWLQIRUPDWLRQ
71 Meetings  ‡([SDQGHGLQVWUXPHQWDWLRQLQIRUPDWLRQ
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78 Suppliers Showcase
84 People in the News Visit: www.rubberworld.com

FOLLOW US ON TWITTER @rubberworld 3


From the Editor Jill Rohrer

Recycled rubber turf approved Rubber Division calls for papers


The Institute of Scrap Recycling Industries applauded the 5XEEHU 'LYLVLRQ $&6 LV DFFHSWLQJ DEVWUDFWV IRU WKH WK
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7XUI$WKOHWLF)LHOGV0DGHRI5HF\FOHG5XEEHU,Q¿OO´FDOOHG annual Independent Testing Laboratories Directory (page
for science to take precedence over conjecture in assessing  IROORZHGE\DJULGOLVWLQJWKHW\SHVRIWHVWLQJVHUYLFHV
UHF\FOHGUXEEHUDQGIRUWKHWLPHO\FRPSOHWLRQRIWKHIHGHUDO R൵HUHG E\ HDFK FRPSDQ\ Rubber World's comprehensive
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3UHVLGHQW 5RELQ:LHQHU ³7KHUH DUH FXUUHQWO\ PRUH WKDQ  LQJ UHVLVWDQFH UXEEHU FRPSRXQG FKDUDF-
SHHUUHYLHZHGVFLHQWL¿FVWXGLHVGHPRQVWUDWLQJWKHUHLVQRLQ- WHUL]DWLRQUKHRORJ\RI(3'0FRPSRXQGV
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LQJUHF\FOHGUXEEHUZLWKRXWFUHGLEOHHYLGHQFHWRWKHFRQWUDU\´ DJDLQVWFKLSDQGFXW Jill Rohrer

The Rubber WorldSOXVLFRQDSSHDULQJWKURXJKRXWWKHPDJD]LQHVLJQL¿HVPRUHLQIRUPDWLRQLV


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EDITORIAL STAFF BUSINESS STAFF


RUBBER WORLD, (ISSN-0035-9572),
January, 2018, Vol. 257, No. 4, Copy-
Jill Rohrer editor Chip Lippincott publisher right: Lippincott & Peto, Inc. 2018; all
rights reserved. J.H. Lippincott, Chair-
Patrick J. DiMauro technical editor Dennis Kennelly senior vice president, man. Published monthly at 1741 Akron-
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by Lippincott & Peto, Inc. Editorial and
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s2UBBER7ORLDFOR#HINA January, 2018. All rights
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s2UBBER7ORLD$IGITAL%DITION

4 RUBBERWORLD.COM ‡ JANUARY 2018


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Business Briefs
ARDL expands with
thermal test systems
Akron Rubber Development Laboratory (www.ardl.com),
Akron, OH, a global independent testing and development
laboratory, has increased its capabilities with the addition

A ,
of a C-Therm TCi ther-
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er. The modular system
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development and quality control.
Wacker Chemical (www.wacker.com), Adrian, MI, part of
the global chemical group Wacker Chemie AG, is planning a
number of concurrent expansion projects to support regional
growth and demand for silicones and HDK pyrogenic silica.
9IN STOCK
Triple digit million dollar investments in North America align
with Wacker's overall expansion strategy to add capacity in
Europe and Asia.
Continental (www.contitech.us), Fairlawn, OH,
announced a $9.3 million expansion of the rubber mixing
9GREAT SERVICE
operations at its industrial hose plant in Norfolk, NE, to
accommodate its North American manufacturing facilities by
providing rubber for industrial hoses and whitewall tires for
passenger cars.
High Duty &
Wabash MPI and Carver (www.wabashmpi.com/www.
carverpress.com), Wabash, IN, announced the completion of
a recent expansion at their Wabash, IN, facility in response to
Dumping Fees
continued growth. This 5,000 square foot expansion includes
new warehouse and service areas which allow for reorganiza-
tion of the companies' current space for new offices, increased Call us today and see how
manufacturing capacities and improved efficiency for Wabash
and Carver's hydraulic and pneumatic presses. HB Chemical can save you money.
Orion Engineered Carbons (www.orioncarbons.com),
Luxembourg, a global supplier of specialty and high-perfor-
mance carbon black, has completed construction of a carbon
black production line at its plant in Yeosu, South Korea, to
produce specialty products.
Tahoma Rubber and Plastics (www.tahomarubberplas-
tics.com), Barberton, OH, added a 170 mm gear pump strainer
to its Abbeville, SC, plant to provide new capabilities to meet
customer demand. The strainer allows for the removal of cured
particles or contamination from rubber compounds. The plant
has also installed the capacity to produce sheeted fiber-filled
rubber compounds.
Smithers Rapra (www.smithersrapra.com), Akron, OH,
HB
CHEMICAL
1665 Enterprise Pkwy, Twinsburg, OH 44087
has invested in expanded tire testing capabilities at its tire and Ph: (800) 991-2436 F: (330) 920-0971
wheel testing laboratory in Suzhou, China. The testing equip- www.hbchemical.com
ment gives the Suzhou lab a 35% boost in capacity.

FOLLOW US ON TWITTER @rubberworld 7


Business Briefs
Nakata names BPS The International Rubber Study Group (www.rub-
berstudy.com), Singapore, announced that Kelani Valley
its agent in Americas Plantations PLC and Dongwha Enterprise Ltd. have joined
the organization.
BPS Engineering, LLC (www.bps-engineering.com), Cooper Tire & Rubber (www.coopertire.com), Findlay,
Greenback, TN, announced that Nakata Engineering, Kobe, OH, announced that its Cooper Zeon LTZ Pro tire in size
Japan, makers of tire ply extrusion and rubber processing 285/60R18 has been selected as original equipment on the HSV
machinery, has named BPS as Colorado SportsCat pickup truck.
C ONTRACTS , its agent in North and South
America. BPS Engineering
The Association for Rubber Products Manufacturers
(www.arpminc.org), Indianapolis, IN, recognized the following
LICENSES will provide new and existing companies for continuous membership for five years or more:
Nakata Engineering custom- Blachford RP, Blair Rubber, Bridgestone APM, Cascade
ers with sales, support and a complete inventory of commonly Gasket & Manufacturing, Chardon Custom Polymers
required spare parts for Nakata machinery. LLC, Chemspec Polymer Additives, Columbia Engineered
Goodyear Tire & Rubber (www.goodyear.com), Akron, Rubber, Continental ContiTech Custom Rubber, Eagle
OH, is introducing its fleet services business model to shared Elastomer, Eaton - Hydraulics, Fenner Dunlop Americas,
mobility providers to improve urban fleet operations. Goodyear Gates, Hamilton Kent LLC, HBD/Thermold, Hexpol
is launching an advanced tire maintenance pilot program with Compounding, Ice Miller LLP, Lauren Manufacturing,
Stratim, a San Francisco-based startup whose technology plat- MBL (USA), Megadyne America LLC, Molded Dimensions,
form tracks, monitors and oversees fleet maintenance in tens of Parker Hannifin, Preferred Compounding, R&R Rubber
thousands of vehicles operated by more than 50 mobility ser- Molding, Rep, The Rubber Group, Salem-Republic Rubber,
vices in more than 25 markets across North America. Superior Tire & Rubber, Timken and Zeon Chemicals L.P.

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got SBR?
Business Briefs
Cooper Tire wins
Good Design awards
Cooper Tire & Rubber (www.coopertire.com), Findlay, OH,
announced that the Cooper Evolution H/T, an all-season high-
way tire for the U.S. market, and the Mastercraft Courser
Sport 100, an ultra-
C ORPORATE , high performance tire
for drivers in Asia,
FINANCIAL NEWS have earned 2017

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Good Design awards
from the Chicago Athenaeum Museum of Architecture
and Design in cooperation with the European Center for
Architecture, Art, Design and Urban Studies for their design
excellence. The winning tires were selected from several thou-
sand entries spanning more than 55 countries.

9IN STOCK
Sumitomo Rubber North America (www.srigroup.co.jp),
Kobe, Japan, announced that MicroStrategy has awarded it
the 2017 Ventana Research Leadership Award in the digital
technology category. Using MicroStrategy Mobile, SRNA is
responsible for the sales and distribution for Falken, Dunlop
Motorcycle and Ohtsu branded tires throughout North America
and the Caribbean markets.
The Association for Rubber Products Manufacturers
(www.arpminc.org), Indianapolis, IN, released its revised
Application Guide for Radial Lip Type Shaft Seals (OS-4). The
ARPM OS-4 is a guide for the selection of radial lip seals.
9GREAT SERVICE
The U.S. Tire Manufacturers Association (www.ustires.
org), Washington, D.C., hails the vote of the Ohio Senate to
pass motorist safety legislation that prohibits the installation of
unsafe used tires as an important consumer production measure.
HB Chemical has the SBR you
need, in stock, duty-free, and
Quality registrations
without the high anti-dumping
The Material Research Center of CoreTech System Ltd.
(Moldex3D) (www.moldex3d.com), Taiwan, has successfully fees you are currently paying.
passed ISO/IEC 17025 certification. Its materials characterization
abilities on shear viscosity, heat capacity and dynamic viscosity are
approved in compliance with international standards.
Mokon (www.mokon.com), Buffalo, NY, a designer and man-
ufacturer of advanced heating and cooling equipment for industrial
markets, has successfully transitioned from ISO 9001:2008 to the

HB
ISO 9001:2015 quality standard.
PolyOne (www.polyone.com), Cleveland, OH, a global pro-
vider of specialized polymer materials, services and solutions, has
been certified to the American Chemistry Council's Responsible
Care Management System.
Vortex Global Limited (www.vortexglobal.com), Darlington,
U.K., has been certified to the ISO 9001:2015 standard.
CHEMICAL
For all the latest 1665 Enterprise Pkwy, Twinsburg, OH 44087
Ph: (800) 991-2436 F: (330) 920-0971
business briefs
click here: www.hbchemical.com

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Market Focus
Moderate growth projected for SBR market
According to a Future Market Insights of global market value estimated in the gion. Favorable industrial regulations in
exclusive study, the global styrene buta- study. these countries will continue to support
diene rubber market will witness a mod- By the end of 2026, over $5.7 billion mass-scale production of SBR solutions
erate growth at 4.3% CAGR during the worth of SBR solutions is expected to be and emulsions. Moreover, India, South
forecast period 2017-2026. The study sold in the global market. The demand Korea and China are at the forefront
estimates that by the end of 2026, over for SBR is also anticipated to remain of global automobile production. The
$8.2 billion worth of SBR products will high in the automotive industry for its demand for SBR in these countries is
be sold across the globe. predominant application in the produc- expected to be high compared to other
Key products made of styrene buta- WLRQ DQG D൶[DWLRQ RI WLUHV 2YHU WKH parts of the world. Through 2026, the
diene rubber can be categorized into forecast period, the automotive tire ap- PDUNHWLQWKH$VLD3DFL¿FUHJLRQLVDQ-
emulsions and solutions. Based on their plications of SBR are expected to regis- ticipated to register a 4.6% CAGR. Sty-
exceptional properties, SBR emulsions ter revenue growth at 4.5% CAGR. The rene butadiene rubber is also expected
have been widely used in the produc- report further reveals that sales of SBR to be in great demand in some parts of
tion of footwear, tires and polymer in footwear applications will net a little North America, Europe, and Middle
PRGL¿FDWLRQ SURFHVVHV 5HJDUGOHVV WKH over $115 million in global revenues by East and Africa, according to the study.
competency of SBR solutions in indus- the end of 2026.
trial applications surpasses that of SBR Throughout the forecast period, the
emulsions. In 2017, SBR solutions sold global sales of styrene butadiene rubber
Auto adhesives to grow
across the globe are anticipated to ac- are expected to remain concentrated in The automotive adhesives market is set
count for more than a two-thirds share WKH $VLD3DFL¿F H[FOXGLQJ -DSDQ  UH- WR JURZ UDSLGO\ RYHU WKH FRPLQJ ¿YH
years as manufacturers move to light-
weight vehicle designs, meet increased
NR countries to slow down exports demand for CUVs and SUVs, and use
The International Tripartite Rubber Council, comprised of Thailand, Indonesia and D ZLGH UDQJH RI GL൵HUHQW PDWHULDOV DF-
Malaysia, has agreed to withhold natural rubber exports in an attempt to boost NR cording to a Smithers Apex report that
prices. The three countries will implement an agreed export tonnage scheme where forecasts a $7 billion market by 2022.
each is committed to withhold exports of 350,000 metric tons of NR through March The market for adhesives in automo-
31. This will be implemented through their respective domestic regulators, includ- tive applications is currently estimated
ing business commitments under existing forward contracts. Implementation will to be worth $4.33 billion in 2017, and is
be closely monitored by the ITRC Monitoring and Surveillance Committee. The forecast to reach $7 billion by 2022, at a
three countries will also cooperate to increase NR consumption domestically, and compound annual growth rate (CAGR)
DUHFRQ¿GHQWWKDW15SULFHVZLOOUHFRYHUDQGFRQWLQXHWREHIDLUDQGUHPXQHUDWLYH of 10.1%. By volume, the automotive
to all rubber smallholders and other stakeholders in the NR industry. adhesives market will increase from 637
metric tons in 2017 to 908 metric tons by
2022, at a CAGR of 7.4%.
Global TPE market to reach 5.1 percent CAGR For modern cars, manufacturers use a
The global thermoplastic elastomers market is expected to reach 7,505.08 metric range of materials besides steel sheets,
tons by 2024 from 5,100.00 metric tons in 2016, at a CAGR of 5.1% in the forecast including aluminium, thermoplastics
period 2017 to 2024, according to a report from Data Bridge Market Research. The DQGFDUERQ¿EHU7KLVPL[RIPDWHULDOV
major factors driving the growth of this market are TPEs substituting for thermo- is also held together by adhesives. Ma-
sets, increasing application from the HVAC/automotive industry, and growth in jor usage areas include adhesives and
end-use industries. On the other hand, unstable raw material prices may hinder the sealants for lighting; coatings and adhe-
growth of the market, according to the DBM study. sives for weatherstrip sealing; composite
The market is dominated by styrenic block copolymer (SBC), with a 45.7% mar- PDWUL[ UHVLQ IRU FDUERQ DQG JODVV ¿EHU
ket share in 2016, growing at the highest CAGR of 4.4% in the forecast period. composites; structural and elastic bond-
Besides substituting thermosets and increasing application from the HVAC/auto- ing solutions for metal and plastic com-
motive industry and growth in end-use industries, increasing applications in the ponents; sustainable metal pretreatments
medical industry and growing demand for bio-based thermoplastic elastomers will for corrosion protection of metal parts;
drive the market in the future. and primers and adhesives for glass
bonding.

12 RUBBERWORLD.COM ‡ JANUARY 2018


Silicone & Medical Update
Liquid silicone rubber eliminates post-curing
Wacker has introduced its Elastosil LR 5040 line of liquid of choice when manufacturers want to dispense with thermal
VLOLFRQH UXEEHU JUDGHV WR IXO¿OO WKH VWULQJHQW UHJXODWRU\ UH- post-treatment altogether. Typical applications include anti-
quirements that apply to silicone articles in many medical- FROLFYDOYHVERWWOHWRSVRUUHVSLUDWRUPDVNV
WHFKQRORJ\DSSOLFDWLRQV&XUHGUXEEHUSURGXFWVPDGHRI(/5 The product line will initially cover a hardness range from
5040 are said to feature excellent mechanical properties, even WRGXURPHWHU$,QWKHFXUHGVWDWHWKHDFWXDOKDUGQHVVRI
without thermal post-treatment, and contain very few volatile WKH QRQSRVWFXUHG VLOLFRQH GHYLDWHV IURP VSHFL¿FDWLRQ E\
VXEVWDQFHVDOORZLQJPDQXIDFWXUHUVWRHOLPLQDWHWKHSRVWFXU- RQO\“SRLQWV(ODVWRVLO/5FDQEHUHDGLO\SURFHVVHGE\
LQJVWHSDIWHUIDEULFDWLRQLQPDQ\FDVHV LQMHFWLRQ PROGLQJ 6LQFH PROGHG SDUWV QR ORQJHU KDYH WR EH
 7KDQNVWRWKHLUSXULW\DQGJRRGVNLQFRPSDWLELOLW\VLOLFRQHV SRVWFXUHGLQPDQ\FDVHVSURGXFWLRQSURFHVVHVFDQEHJUHDWO\
LQFUHDVLQJO\¿QGXVHLQPHGLFDOWHFKQRORJ\DSSOLFDWLRQV7KH streamlined and automated to a high degree. This facilitates
product is said to feature excellent tear strength after curing, YHU\UDSLGH൶FLHQWDQGFRVWH൵HFWLYHODUJHVFDOHSURGXFWLRQ
allowing manufacturers of medical devices to dispense with even under cleanroom conditions.
thermal post-treatment in many cases.
E-LR 5040 cures to a translucent elastomer whose volatiles Toyoda Gosei licensing Slide-Ring
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SHUFHQW,QLWVQRQSRVWFXUHGVWDWHWKHVLOLFRQHH[KLELWVDKLJK Toyoda Gosei and Advanced Softmaterials of Japan have con-
level of tear resistance equivalent to that of post-cured high cluded an exclusive licensing agreement for the use and sale
tear strength standard materials. As a result, it can withstand RI6OLGH5LQJPDWHULDODNH\PDWHULDOLQH5XEEHU7KHDJUHH-
such mechanical stresses as may occur in the usage of medical ment is limited to applications of the material in dielectric ac-
devices, for example. WXDWRUVDQGGLHOHFWULFVHQVRUV$60ZDVHVWDEOLVKHGLQ
These properties are said to make E-LR 5040 the material with the aim of commercializing the Slide-Ring material de-
veloped at Tokyo University. It has acquired an exclusive li-
FHQVH IRU WKH EDVLF XPEUHOOD SDWHQW IRU 6OLGH5LQJ PDWHULDO
TPEs for injection molded masks from Tokyo University.
 7KHEDVLFVWUXFWXUHRIWKH6OLGH5LQJPDWHULDOLVWKHVXSUD-
Teknor Apex has introduced two new families of medical
molecular networks comprised of nano-sized "necklace" su-
grade thermoplastic elastomers for injection molded face
pramolecules called polyrotaxane with crosslinking points of
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ERQGHGPROHFXODUQHFNODFHVRUPROHFXODUQHFNODFHVZLWKRWKHU
masks, and a series of gels that provide a gas-tight cushion
polymers. These molecules consist of polyethylene glycol
for rigid ones molded from polypropylene.
linear polymers, cyclodextrin ring molecules and adamantan-
 7KH0HGDOLVW6HULHV73(VIRUÀH[LEOHPDVNVDUH
amine stopper molecules.
more deformation-resistant than PVC, and, as thermoplas-
At the University of Tokyo, the amount of clathrate in the
tics, provide a more economical alternative to silicones. In
cyclic molecules (cyclodextrin) of a molecular necklace (poly-
respiratory therapy oxygen masks, the Medalist TPEs are
rotaxane) was controlled and given free movement in a linear
ÀH[LEOHHQRXJKWRSURYLGHDFRPIRUWDEOH¿WRQWKHIDFH\HW
SRO\PHUWKHUHE\FURVVOLQNLQJERQGHGF\FOLFPROHFXOHVF\FOR-
retain their shape during packaging and storage, without
dextrin or a component of Slide-Ring material. Taking this as
need for inserts. Their PVC-like transparency facilitates
DFURVVOLQNLQJSRLQWFURVVOLQNLQJWKHERQGHGPROHFXODUQHFN-
patient monitoring. Medalist 50100 Series compounds are
ODFHVZLWKRWKHUSRO\PHUVHQDEOHVIUHHPRYHPHQWRIFURVVOLQN-
DYDLODEOHLQGXURPHWHU$KDUGQHVVHVRIDQG
LQJ SRLQWV WR EXLOG VXSUDPROHFXODU QHWZRUNV &URVVOLQNLQJ
The Medalist 10100 Series TPE gels for rigid mask cush-
SRLQWV DUH XVHG IRU D SXOOH\ H൵HFW HTXDOL]LQJ WKH WHQVLRQV
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providing a less expensive alternative to the traditional air-
has unique mechanical properties that conventional plastics
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rigid component. The super-soft cushion conforms to the
meric material with completely new functions.
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Dielectric sensors show promise for use as tactile/pressure
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sensors and motion sensors that take advantage of this softness
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IULFWLRQGXUDELOLW\HWF 

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The Rubber Economist
Rubber industry exhibits cyclical behavior
Is there regularity or predictability of variables influencing the ment. In the past, a complete rubber consumption cycle was
rubber industry? One sometimes hears comments such as “win- about five years. However, the China effect during the 2000s,
tering is due, therefore the natural rubber (NR) supply should
be declining and the price firming up,” or “it is approaching
summer holidays in North America and Europe, thus rubber Highlights
demand should be falling and the prices are likely to be weaken- s The growth estimate for world rubber consumption this year
ing.” What we would like to know is: “Do rubber demand, sup- has been revised downward, but should still show a faster
rate than last year.
ply and prices move in a predictable behavior, or do they move
s The slower global growth rate is due to a lower forecast for
randomly, independent from just one or a few variables?” If we PRVWUHJLRQVLQFOXGLQJWKH$VLD3DFL¿F
look at the monthly growth rate of world rubber consumption s7KHPRUHSHVVLPLVWLFRXWORRNLVGXHWRDVORZHUUXEEHUR൵WDNH
from January 1971 to December 2017, as shown in figure 1, for all four of the largest rubber consuming countries: China,
we can see the growth rate does move in a cyclical manner, and USA, India and Japan.
the speed and length of the upturns and downturns are generally s7KHGRZQZDUGUHYLVLRQIRUWKHJOREDOUXEEHUR൵WDNHZDV
quite similar. mainly a revision of a slower growth for NR.
s Despite the revision, consumption of NR is expected to be
Four elements of a time series more rapid than SR, bringing the percentage of global SR
consumption down by 2019.
A time series is usually composed of four elements, including a
s World NR production for this year is now expected to increase
seasonal component, an irregular component, a long-term secu- HYHQIDVWHUWKDQSUHYLRXVO\HVWLPDWHGGHVSLWHDORZHU¿JXUH
lar trend and a long-term cyclical movement. We will come to for the output in the major producing countries.
discussing in detail the seasonal factors in the rubber industry s There is a detailed analysis: “Do rubber demand, supply and
next, but to give you an example, one of the macro-economic prices move in a predictable behavior, or do they move very
variables is the seasonal fluctuation of housing starts in the much more randomly, independent from just one or a few
USA, which usually peaks around April-June and reaches a variables?”
low around December-February. An irregular movement for the s World SR output in 2017 is now expected to show an increase
even slower than last year, as all regions are expected to show
rubber consumption was the financial crisis in 2008 and 2009,
DQHJDWLYHJURZWKUDWHZLWKWKHH[FHSWLRQRI$VLD3DFL¿FDQG
which caused the growth rate to fall sharply in 2008 and 2009, Latin America.
and an equally sharp increase in 2010 (figure 1). Many economic s The picture on rubber stocks has changed from the last report,
variables and those related to the rubber industry, such as rubber DV15LVH[SHFWHGWRVKRZDVPDOOVXUSOXVUDWKHUWKDQGH¿FLW
consumption, have long-term influencing trends, from the rising The reason is that the increase in demand for NR has not been
level of the population to GNP. as rapid as anticipated, and supply from smaller producers has
LQFUHDVLQJO\EHFRPHPRUHVLJQL¿FDQW
Cyclical movements s Global NR stocks are now expected to increase and surpass
If one takes away the seasonal factor, the irregular movement the record level reached in 2014.
s65GH¿FLWZLOOFRQWLQXHIRUWKHQH[WWKUHH\HDUVEULQJLQJ
and the long-term trends from a time series, such as the rubber
global SR stocks down to the lowest level since 2001.
consumption growth rate, we will be left with a cyclical move- s Despite record levels expected for global stocks, the NR stock
to consumption ratio may not show a sharp rise.
s There may be a sharper decline in SR stocks in both absolute
Figure 1 - growth rate of world rubber and relative terms to consumption.
consumption, January ’71 - December ’17 s NR prices have fallen quite sharply in recent months, e.g., the
average prices in November of STR20 fell to the lowest level
20 since September 2002.
15 s7KHUHKDVEHHQDORWRIQHZVDQGHYHQWVD൵HFWLQJUXEEHUSULFHV
10 but the gradual increase in the stock/consumption ratio was
OLNHO\WREHWKHPRVWLPSRUWDQWIDFWRULQÀXHQFLQJWKHZHDN
Percent

5 rubber prices.
0 s If the stocks/consumption ratio may increase only marginally,
-5 the short term price outlook is not going to change much and
rubber prices may just remain at a relatively low level.
-10 s There has also been a similar movement to NR of SR prices in
-15 North America, Europe and Asia. For both NR and SR, the
Jan. '71 Jan. '81 Jan. '91 Jan. '01 Jan. '11 latex was holding up better than the dried counterpart.

16 RUBBERWORLD.COM ‡ JANUARY 2018


The Rubber Economist
Figure 2 - seasonality of NR output Figure 4 - seasonality of NR consumption and
production
1.4 Indonesia
1.3 Malaysia 1.3
1.2 Thailand 1.2 Consumption
1.1 Production
1.1
1.0 1.0
0.9
0.9
0.8
0.7 0.8
0.6 0.7
Jan. Feb. Mar. Apr. May Jun. Jul. Aug. Sep. Oct. Nov. Dec. 0.6
Jan. Feb. Mar. Apr. May Jun. Jul. Aug. Sep. Oct. Nov. Dec.
which was followed by the industrialization process in other
Asian countries, may have lengthened the cycle somewhat. The is a greater degree of seasonality for NR production than con-
usefulness of knowing a cyclical pattern of a variable such as sumption (figure 4). NR consumption generally peaks in March
rubber consumption is to have a general idea of its future direc- and declines in July and August when factories in many rubber
tion. Many of the rubber variables are analyzed using their cycli- consuming countries close for the summer holiday. December
cal patterns in the Rubber Economist forecasts. also sometimes shows relatively lower rubber consumption
because there are more holidays during the month.
Seasonality of NR output
Seasonality is a form of cyclical behavior that occurs on a regu- NR prices and seasonality of production/consumption
lar calendar basis. There is no doubt that in a typical year, NR Judging from the seasonality of NR production and consump-
output varies because of seasonal factors. The seasonal factors tion, NR prices should be strengthening in January because of
vary geographically and may change over time. For three major seasonally low stocks and increased buying interest due to sup-
Southeast Asia NR producing countries, Thailand, Indonesia and ply shortages anticipated in forthcoming months from the onset
Malaysia, the patterns of output are quite similar (figure 2). NR of the wintering season. The market can be quiet in February due
production generally peaks in January and declines over the next to the Chinese New Year. From February to May, there may be a
three months because of wintering of the rubber trees to reach the tendency for rubber prices to increase because of peak consump-
lowest level of production in April. It then recovers during May tion period and supply shortages due to seasonal low production
to July/August. Output tends to be relatively stable over the next during the wintering period. Then the prices may weaken from
two months or so, before rising towards the end of the year. June to August, as well as towards the end of the year, partly
because of the holiday season. Judging from the monthly aver-
Seasonality of NR consumption age TSR20 price in Singapore, shown in figure 5, there is some
Normally, NR rubber end-use production, and hence NR con- degree of seasonal influence on the NR price.
sumption, have a clearer seasonality pattern in Europe and North
America than in Asia (figure 3). It is also generally true that there Seasonality cannot always explain price movements
One cannot expect rubber prices to change in relation to sea-
sonality in NR output or consumption alone. As mentioned ear-
Figure 3 - seasonality of NR consumption lier, there are three other elements in a time series. The irregular
component was quite in evidence during 2008-2010 (financial
1.3 Germany crisis) and 2016-2017 (unseasonal rains and floods in Thailand,
1.2
Japan the release of stockpiles by the Thai government, and an increase
U.S.A. in speculative futures trading). Seasonal factors can generally
1.1 be predicted with a reasonable degree of accuracy, but irregular
movements are unforeseen. Long-term cyclical movements
1.0 and a long-term secular trend are not always easy to iden-
tify. Therefore, the factors underlying price movements are more
0.9 complex. Although demand and supply of NR are the ultimate
and the most important factors determining its price, factors such
0.8 as currency movements, psychological factors, economic and
Jan. Feb. Mar. Apr. May Jun. Jul. Aug. Sep. Oct. Nov. Dec. political news, etc., can also have an impact on prices. As these

FOLLOW US ON TWITTER @rubberworld 17


The Rubber Economist
Figure 5 - monthly average TSR20 price in Figure 6 - seasonality of SR consumption and
Singapore production

2008 2009
6,000 2010 2011 1.2 Consumption
2012 2013
2014 2015 Production
5,000 2016 2017 1.1
$ per ton

4,000 1.0
3,000 0.9

2,000 0.8

1,000 0.7

0 Jan. Feb. Mar. Apr. May Jun. Jul. Aug. Sep. Oct. Nov. Dec.
Ja

M
Ap .
M
Ju
Ju
Au
Se .
O
No
Fe

De
ct
ar

ay
n.

n.
l.

g
r.

p.
b.

v.
c.
or if the winter is mild. It is sometimes necessary to distinguish
.

between short-term or long-term and fundamental or normal


factors show little seasonal pattern, it is quite likely that one can influences on NR prices.
find that there is very little overall seasonality in rubber prices.
Furthermore, normally, seasonal factors are more or less taken Seasonality of SR production and consumption
into account by market participants. NR prices can strengthen Let us turn to the seasonality of synthetic rubber (SR) consump-
or weaken because of unusually strong winter or wet weather, tion and production, shown in figure 6. SR consumption rises in
the first three months of the year to the peak level in March, and
then declines over the next five months to reach the lowest point
at the height of the summer holidays in August. SR consumption
improves in September and October before slowing down again
during the last two months of the year.
The seasonal pattern of SR production tends to follow that
of consumption; e.g., they both peak in March and bottom out
in August. This is not the case for NR, shown in figure 4. This
is not surprising considering that SR is a petrochemical based
product and there is forward and backward integration of SR
manufacturers, while NR is a product of a tropical crop produced
by millions of small farmers.
Furthermore, production of NR shows a greater seasonality
pattern than that of SR. However, as expected, there is a similar-
ity in the seasonality of SR and NR consumption. Both NR and
SR are derived demand and a rubber product is bought because it
is required, and normally without concern for the type of rubber
used.

Conclusion
In conclusion, there is a degree of regularity or predictability in
rubber production and consumption, but not so much for rubber
prices.

Dr. Prachaya Jumpasut is the managing di-


rector of The Rubber Economist, a quarterly
analysis and forecast of the industry. The Rub-
ber Economist is a registered limited company
in the U.K., and is incorporated under the Com-
panies Act of 1985. Please email info@therub-
bereconomist.com for more information.

18 RUBBERWORLD.COM ‡ JANUARY 2018


Patent News For additional industry patent
information click here:

Butyl rubber ionomer-thermoplastic Assigned: Wright Asphalt Products black-rich rubber tread zone to the car-
graft copolymers and methods for Key statement: This invention encom- bon black-rich tread base layer by an
production thereof passes rubber modified asphalt cement extension of a lateral tread zone or by
U.S. patent: 9,815,929 compositions, as well as systems, an intermediate carbon black-rich rub-
Issued: November 14, 2017 apparatuses, methods for preparing, as ber bridge.
Inventors: Conrad Siegers and Richard well as methods for using rubber-mod-
Steevensz ified asphalt cement compositions.
Assigned: Lanxess 3 2 6
7A 7 7 7B
Key statement: The present invention Tire with rubber tread of intermedi- 5A 5B
is directed to the functionalization of al and lateral zones with path of 6A 6B
butyl rubber ionomer and optionally least electrical resistance 8A 8B
4
the grafting of polyamide to halobutyl U.S. patent: 9,809,058 9 9
rubber ionomers. Specifically, dis- Issued: November 7, 2017
closed are methods and products Inventors: Roberto Cerrato Meza, Jun-
resulting therefrom for creating func- ling Zhao and Austin Gale Young
tionalized ionomers and grafting poly- Assigned: Goodyear Tire & Rubber
amide to halobutyl ionomers via reac- Key statement: The invention relates
tive extrusion. The process comprises to a tire having a rubber tread of a cir-
reacting a halobutyl polymer with at cumferentially zoned tread. The tread
least one nitrogen and/or phosphorous zones are comprised of three circum-
based nucleophile to provide a halobu- ferential load bearing zones, with each
tyl ionomer comprising conjugated zone containing a portion of the run- Combined tire
diene units; grafting of an amine-reac- ning surface of the tread, comprised of U.S. patent: 9,815,331
tive dienophile to said ionomer to form a silica-rich intermedial rubber zone Issued: November 14, 2017
a functionalized ionomer; and option- positioned between and extending Inventor: Garyg Gong
ally blending the resulting functional- beneath two carbon black-rich lateral Assigned: Xiamen Lenco
ized ionomer with polyamide. tread zones. The tread configuration Key statement: Disclosed is a com-
contains an underlying carbon black- bined tire, including a tire casing and a
System and method for high rich base rubber layer. The intermedial core. The tire casing is an annular
throughput preparation of rubber- and stratified lateral zones are com- member having a core groove around
modified asphalt cement prised of rubber compositions having the periphery; the core is an annular
U.S. patent: 9,803,085 differentiated rebound physical proper- member nested within the core groove
Issued: October 31, 2017 ties. A path of least electrical resis- of the tire casing in an interference fit,
Inventor: Theodore P. Flanigan tance extends from a lateral carbon and forms a gap with the inner wall of

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20 RUBBERWORLD.COM ‡ JANUARY 2018


Patent News
the core groove of the tire casing. The ments and/or residues of expanded sol- when the modified polymer is formed
present invention can ensure high pro- ids, where the solids are selected from into a rubber composition, a rubber
duction efficiency. The tire casing and the group containing expandable composition containing the modified
the core of the present invention can graphite and microspheres. In some polymer, and a pneumatic tire in which
employ materials of different hardness, aspects, the microspheres include at the rubber composition is used. The
offering better comfort. least isobutane and/or isopentane as modified polymer of the present
blowing agents. The microspheres may invention is a modified polymer
also have a shell containing at least obtained by modifying a styrene-con-
one polymer, and in some cases the jugated diene copolymer (A) with a
polymer is at least one copolymer of nitrone compound (B). In the modified
acrylonitrile and methyl acrylate. The polymer, the content of styrene units in
self-sealing tire sealant may further the styrene-conjugated diene copoly-
include graphene structures. In some mer (A) is 10% by mass or greater,
aspects the interior of a pneumatic and the proportion of vinyl bonds
vehicle tire has the self-sealing tire among all the double bonds contained
sealant disposed on the inner surface, in the styrene-conjugated diene copo-
2 opposite the tire tread, and the layer lymer (A) is 5 mol % or greater.
13
12 22 thickness of the tire sealant may be
1 21 from 0.5 to 8 mm.
F
11
F 3 7
Modified polymer, rubber composi-
Self-sealing tire sealant and pneu- tion and pneumatic tire
matic vehicle tire U.S. patent: 9,803,031
U.S. patent: 9,802,446 Issued: October 31, 2017 4
Issued: October 31, 2017 Inventors: Ryota Takahashi, Manabu
2
Inventors: Markus Dahlke, Dieter Kato, Takahiro Okamatsu and Yoshiaki
Jeromin, Joe Guardalabene, Thomas Kirino
Volker, Fei Liu, Andreas Tyburski and Assigned: Yokohama Rubber
Martin Convey Key statement: The purpose of the 6
Assigned: Continental Reifen present invention is to provide a modi- 5 1
Key statement: Self-sealing tire seal- fied polymer that significantly reduces 6
ants are provided which contain frag- heat build-up due to the modification

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FOLLOW US ON TWITTER @rubberworld 21


Prediction of rolling resistance factor (RRF)
for conveyor belt cover compounds with a
rebound resilience tester
by S.L. Agrawal, B.B. Sharma and Virendra Rathod, Reliance A variety of analytical and computational methods exists for
Industries Ltd., India calculating the indentation rolling resistance of conveyor belts.
These include both one- and two-dimensional analytical ap-
Energy consumption reduction is a national goal for many rea- proaches (refs. 5-9), and two-dimensional finite element methods
sons, from economic and national security to improving air qual- (refs. 10-12). One-dimensional Winker Foundation models pro-
ity and decreasing the greenhouse effect. An increase in the price vide a simple and direct way to analyze the rubber deformation.
of energy is affecting consumers and businesses, and also con- Jonkers (ref. 13) focuses on the energy dissipation rate of the
tributing to increases in the Consumer Price Index in the last few cover material in a steady deformation cycle, whereas Lodewijks
years. (ref. 14) and others determine the power of the stress distribution
There has been significant technical progress in the transport at the idler/backing interface. Direct indentation rolling resis-
of bulk materials in the last few years. Conveyors have always tance measurement is practically limited to a small set of operat-
moved materials over uneven terrain, through mountain tunnels ing conditions compared to the wide range of loads on a belt
and around horizontal curves; but today, the next step to im- conveyor or the operating environment for a particular applica-
proved conveyor efficiency is the reduction of power required to tion.
operate these high performance systems. Just as some tires pro- Analytical and computational methods rely on the measure-
vide lower rolling resistance, depending on their construction and ment of the dynamic mechanical properties of the bottom cover
compounds, a conveyor belt can also be designed to provide compounds. These properties are typically measured using dy-
lower resistance as it rolls over the supporting idlers. namic mechanical analysis (DMA) equipment. DMA machines
The factor energy efficiency (ref. 1) will gain significance in rely on time-temperature transformations to simulate high fre-
the future as a criterion for the acquisition, and therefore as a quency cyclic tests, where low frequency, low temperature data
target value in the phase of development of technical systems, as are shifted along the frequency axis to simulate higher frequency
well as in the bulk materials handling technique. This tendency tests at the temperature being analyzed. The measured rubber
will be determined on the one hand due to increasing energy properties are then used in the theoretical models based on the
costs, which will focus more on the life cycle costs of machines frequency of indentation and operating temperature.
and systems when decisions of investment are made. On the A lower tan delta value is expected to provide lower rolling
other hand, the general climate debate encourages ecological losses on a field conveyor, and therefore less horsepower con-
thinking in the context of sustainable economic activities. The sumed. Tan delta results can be gathered from tension, compres-
ecological action, i.e., the economical handling of resources such sion or shear methods. The tan delta component of energy loss is
as electric current, which will also become more attractive finan- a valuable tool for correlating rolling resistance of rubber com-
cially in the future, as shown above, offers two advantages from pounds (ref. 15).
the entrepreneur’s point of view: The ecological necessity is now A wide variety of experimental techniques for measuring
also economically reasonable. dynamic mechanical properties of rubber compounds has been
The belt conveyor system also has ecological advantages, as developed in research laboratories for specific investigations
shown in a case study by Zamorano (ref. 2), which provides a (refs. 16-40).
comparison between a dumper and a belt conveyor system with In a rebound resilience tester, deformation is an indentation
regard to the carbon dioxide emissions for two different con- due to a single impact. The ratio of energy returned to the energy
veyor lines. applied is termed the resilience. When deformation is an indenta-
Rubber is a viscoelastic material, and it has viscous as well as tion due to a single impact, this ratio is termed the rebound resil-
elastic phases. Under deformation of rubber, energy input is in- ience. The value of rebound resilience for a given material is not
volved, part of which is returned when the rubber returns to its a fixed quantity, but varies with temperature, strain distribution,
original shape. That part of energy, which is not returned as me- strain rate, strain energy and strain history (ref. 41).
chanical energy, is dissipated in the form of heat in the rubber In a dynamic mechanical analyzer (DMA1000+), dynamic
(ref. 3). properties are measured using a strip specimen between -20°C to
Many rubber products are used for applications in which they +70°C at 2% dynamic strain and 10 Hz frequency in tension
undergo rapid cyclic deformations at a certain range of frequen- mode. The properties that can be measured in a dynamic me-
cy, e.g., tire sidewalls, or tread and engine mounts, which serve chanical analyzer (ref. 42) are as follows:
the purpose of isolating engine vibration from a chassis or build- s Elastic or storage modulus, E’, is the real part of the com-
ing. The dynamic mechanical properties are strongly dependent plex modulus, E*. It represents the rigidity of an elastic material
on temperature, frequency, the presence of fillers and the extent (elastic component) and is proportional to the maximum energy
of deformation (refs. 3 and 4). stored during a load cycle.

22 RUBBERWORLD.COM ‡ JANUARY 2018


blacks (a major contributing
Table 1 - formulations used element to viscoelastic prop-
erties) are mixed in a 1.5 liter
Ingredients RRF1 RRF2 RRF3 RRF4 RRF5 RRF6 RRF7 RRF8 RRF9
Natural rubber 0.00 60.00 40.00 0.00 70.00 40.00 50.00 0.00 20.00 laboratory internal mixer and
PBR, Cisamer 01 0.00 40.00 10.00 0.00 30.00 60.00 50.00 100.00 80.00 are given in table 1. The mix-
Stylamer SBR1502 0.00 0.00 50.00 100.00 0.00 0.00 0.00 0.00 0.00 ing is done following the
Stylamer SBR1783 137.50 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 power integrator method of
Carbon black 68.80 70.00 50.00 50.00 24.00 33.00 30.00 60.00 39.00 mixing. The discharged
Ppt. silica 0.00 10.00 13.00 0.00 18.00 12.00 14.00 0.00 8.00
Aromatic oil 0.00 16.00 18.00 0.00 2.00 2.00 2.00 15.00 2.00 compounds from the internal
Zinc oxide 3.00 4.00 4.00 3.00 4.00 4.00 4.00 3.00 4.00 mixer are sheeted out using a
Stearic acid 1.00 2.00 2.00 1.00 2.00 2.00 2.00 2.00 2.00 laboratory two-roll mill.
Antidegradants 2.00 3.00 2.00 2.00 2.00 2.00 2.00 2.00 2.00 The green compounds
Accelerator 1.4 1.0 1.0 1.0 1.0 2.0 1.0 0.9 2.0 are cured in an electrically
Soluble sulfur 1.75 1.90 2.00 1.75 2.00 2.00 2.00 1.50 1.00
heated laboratory hydraulic
curing press. The curing con-
dition maintained for deter-
Table 2 - prediction of rolling resistance factor (RRF) by rebound value mination of rebound resil-
ience is at 150°C for tc90 + 5
Sample Rebound at E’ measured E” measured RRF measured RRF predicted %
identification 25°C (%) by DMA by DMA by DMA by Rebound variation minutes and at 150°C for
(MPa) (MPa) tc90 + 2 minutes for dynam-
RRF1 37.6 13.01 5.72 0.187 0.175 -6.4 ic mechanical properties.
RRF2 41.3 15.99 6.10 0.151 0.158 4.6 The dynamic mechanical
RRF3 42.2 11.67 4.12 0.156 0.154 -1.3 properties are measured us-
RRF4 49.8 15.25 4.27 0.113 0.119 5.3
RRF5 56.8 7.10 1.16 0.085 0.087 2.4 ing a viscoanalyzer (Metra-
RRF6 58.7 8.27 1.31 0.078 0.078 0.0 vib DMA1000+) following
RRF7 58.9 8.70 1.48 0.083 0.077 -7.2 ASTM D 5992, and rebound
RRF8 59.3 8.98 1.48 0.079 0.076 -3.8 resilience is measured using
RRF9 61.0 10.11 1.62 0.074 0.068 -8.1 a rebound resilience tester
Correlation
coefficient (-) 0.99 following ISO 4662.
The rolling resistance fac-
tor is predicted by using lin-
s Viscous or loss modulus, E”, is the imaginary part of the ear regression analysis and R2 coefficient of regression (ref. 43)
complex modulus, E*. It represents the viscous component and with the help of equation B:
is proportional to the energy dissipated during a load cycle.
s/RVVIDFWRUWDQįLVWKHUDWLRRIWKHORVVPRGXOXV(RYHU Y=m*X+C (B)
the storage modulus, E'.
s Rolling resistance factor, RRF, is calculated as: Where, X is measured rebound resilience; Y is predicted rolling
resistance factor using rebound; m is slope of the trend line; and
RRF (measured by DMA) = (E”)/(E’)4/3 (A) C is intercept.

Experimental Results and discussion


Nine compounds having different rubber blends and carbon Rebound resilience at 25°C is measured by a rebound resilience
tester, and rolling resistance factor (RRF) is measured by a
DMA1000+. The predicted, measured and percent variations are
Figure 1 - linear regression analysis summarized in table 2.
The percent variations of measured and predicted rolling re-
RRF measured by DMA1000+

0.19
sistance factor values are calculated using equation C:
0.17
0.15 Percent variation = [(Predicted value – measured
0.13 value)/measured value] x 100 (C)
0.11
We have also calculated the correlation coefficient be-
0.09
y = 0.0046x + 0.3483 tween rebound resilience and RRF with a dynamic mechani-
0.07 R2 = 0.98 cal analyzer. The coefficient of correlation value is found to
0.05 be 99%.
35.0 40.0 45.0 50.0 55.0 60.0 65.0
Linear regression used for prediction of rolling resistance fac-
Rebound measured by rebound resilience tester tor and its coefficient of regression are mentioned in figure 1.

FOLLOW US ON TWITTER @rubberworld 23


Conclusion 16. M.C. Putman and G. Bradnick, Rubber World, p. 37, Vol.
Rolling resistance factor (RRF) values measured by both pieces 232, No. 6, September 2005.
of equipment show excellent correlation (coefficient of correla- 17. S.L. Agrawal, S. Bandyopadhyay, S. Dasgupta and R. Muk-
tion = 99%). The rolling resistance factor prediction by rebound hopadhyay, Rubber World, p. 31, Vol. 237, No. 4, January 2008.
shows less than 10% variation as compared to the value mea- 18. L.E. Nielsen, Mechanical Properties of Polymers and Com-
sured by the DMA1000+. The dynamic mechanical analyzer posites, ch. 4, Dekker, New York, 1974.
(DMA) is a very costly tester as compared to the rebound resil- 19. A.C. Edwards and G.N.S. Ferrand, The Applied Science of
ience tester, and it is very difficult for small-scale rubber produc- Rubber (W.J.S. Nauton, ed.), ch. 8, Arnold, London, 1961.
ers to measure dynamic mechanical properties with a DMA tes- 20. J.R. Scott, Physical Testing of Rubbers, p. 181, MacLaren,
ter. Therefore, the above experiment will assist in predicting the London, 1965.
viscoelastic properties measured by DMA by simply measuring 21. R.J. Schaefer, Rubber World, May 1994 to June 1995.
through a comparatively much less expensive tester, the rebound 22. B. D’ Cruz, P.R.S. Shaktawat and R. Mukhopadhyay, “Char-
resilience tester. acterization, process design and performance prediction of
elastomeric material through simulation testing,” p. 358, pro-
References ceedings of Asia RubTech Expo 2002 conference, New Delhi,
1. W.A. Günthner, Ch. Tilke and S. Rakitsch, “Energy efficiency India, November 28-30, 2002.
in bulk materials handling,” Bulk Solids Handling, pp. 138-142, 23. J. S. Dick and H. Pawlowski, Rubber World, p. 21, Vol. 215,
Vol. 30, No. 3, 2010. No. 4, January 1997.
2. S. Zamorano, “Overland conveyors: A relevant tool in reduc- 24. J. Frohlich and H.D. Luginsland, Rubber World, p. 28, Vol.
ing environmental impact in the minerals industry,” Tagungs- 224, No. 1, April 2001.
band BulkEurope 2008, Prague, 2008. 25. H.G. Burhin, “Dynamic mechanical analysis for tire com-
3. S. L. Agrawal, S.K. Mandot, S. Bandyopadhyay, R. Mukhopad- pounds, processability and quality control,” p. 234, proceedings
hyay and A.S. Deuri, Rubber World, p. 28, Vol. 233, No. 1, Octo- of RubTech 2000, New Delhi, India, February 18-19, 2000.
ber 2005. 26. J. Shim-Ton, K.A. Kennedy, M.R. Piggott and R.T. Wood-
4. P.R.S. Shaktawat, R. Mukhopadhyay and A.K. Kalidaha, hams, Rubber Chemistry and Technology, p. 88, Vol. 53, No. 1,
“Correlation between tan delta and heat build-up of tire compo- March-April 1980.
nents,” p. 267, proceedings of the RubTech 2000 conference, 27. P. Kainradl and G. Kaufmann, “Viscoelastic properties of
New Delhi, India, February 18-19, 2000. truck tire compounds and the related heat build-up,” paper pre-
5. S. Hunter, “The rolling contact of a rigid cylinder with a vis- sented at a meeting of the Division of Rubber Chemistry, Ameri-
coelastic half space,” Journal of Applied Mechanics, pp. 611- can Chemical Society, Cleveland, OH, October 12-15, 1971.
617, Vol. 28, 1961. 28. N.R. Manoj, S. Barman, R.D. Raut, B.C. Chakraborty, R.
6. C. Jonkers, “The indentation rolling resistance of belt convey- Ramesh and R.M.R. Vishnubhatla, “Studies on viscoelastic ma-
ors,” Fordern und Heben, pp. 312-318, Vol. 30, No. 4, 1980. terials for damping of structural vibration,” p. 342, proceedings
7. C. Spaans, “The calculation of the main resistance of belt of Asia RubTech Expo 2002 conference, New Delhi, India, No-
conveyors,” Bulk Solids Handling, pp. 809-826, Vol. 11, No. 4, vember 28-30, 2002.
1991. 29. T. Kurian, “Effect of plasticizers and filler on ionic thermo-
8. G. Lodewijks, “Dynamics of belt systems,” Ph.D. thesis, Delft plastic elastomer based on EPDM,” p. 415, proceedings of the
University of Technology, Netherlands, 1996. International Rubber Conference (IRC98) held at Chennai,
9. X. Qiu, “Full two-dimensional model for rolling resistance: India, December 7-9, 1998.
Hard cylinder on viscoelastic foundation of finite thickness,” 30. A.I. Medalia, Rubber Chemistry and Technology, p. 437, Vol.
Journal of Engineering Mechanics, pp. 1,241-1,251, Vol. 132, 51, No. 3, July-August 1978.
No. 11, 2006. 31. H. Takino, R. Nakayama, Y. Yamada, S. Kohjiya and T. Mat-
10. C. Wheeler, “Analysis of the main resistances of belt convey- suo, Rubber Chemistry and Technology, p. 584, Vol. 70, No. 4,
ors,” Ph.D. thesis, The University of Newcastle, 2003. September-October 1997.
11. F.A. Lynch, “Finite element method of viscoelastic stress 32. S. Futamura, Rubber Chemistry and Technology, p. 648, Vol.
analysis with application to rolling contact problems,” Interna- 69, No. 4, September-October 1996.
tional Journal for Numerical Methods in Engineering, pp. 379- 33. A. Scurati and C.J. Lin, Rubber Chemistry and Technology,
394, Vol. 1, 1969. p. 170, Vol. 79, No. 1, March-April 2006.
12. L. Nordell, “The power of rubber - part 1,” Bulk Solids Han- 34. L. Gonzalez, A. Rodiguez, J.L. De Benito and A. Marcos,
dling, pp. 333-340, Vol. 16, 1996. Rubber Chemistry and Technology, p. 266, Vol. 69, No. 2, May-
13. C.O. Jonkers, “The indentation rolling resistance of belt June 1996.
conveyors - a theoretical approach,” Fordern und Heben, pp. 35. R.A. Francis, “Carbon silica dual phase fillers - applications
312-317, Vol. 30, No. 4, 1980. for enhanced performance,” p. 275, proceeding of the Interna-
14. G. Lodewijks: “The rolling resistance of conveyor belts,” tional Rubber Conference (IRC98) held at Chennai, India, De-
Bulk Solids Handling, pp. 15-22, Vol. 15, No. 1, 1995. cember 7-9, 1998.
15. David Gallagher, International Rubber Conference, Mel- 36 M. Hensel and K.H. Menting, “Improved processing of car-
bourne, Australia, October, 2000. (continued on page 30)

24 RUBBERWORLD.COM ‡ JANUARY 2018


Characterization of rubber polymers
and compounds
by Alina K. Latshaw and Thomas Rauschmann, TA Instruments ture at the sample edge, and compressive forces to prevent sample
Waters slippage during testing. Both features are imperative for obtaining
accurate data in the non-linear regime, particularly during large
Traditional rubber testing methods, such as Mooney viscometer amplitude oscillatory strain (LAOS) testing. The viscoelastic
and MDR curemeter testing, have been used for several decades properties of EPDM, BR and rubber compounds were obtained in
to monitor the quality of mixed batches. However, as elasto- the RPA using standard oscillation testing, such as frequency
meric product performance becomes more demanding, and sweeps and strain sweeps. Frequency sweeps were performed
highly engineered materials are required to meet these demands, from 0.0628 rad/s to 314 rad/s or 0.01 Hz to 50 Hz using an ap-
testing methodologies with greater sensitivity to differences in propriate strain amplitude within the linear viscoelastic regime of
viscoelastic properties are essential. the testing specimen, while strain sweeps were performed from
Physical and structural properties of raw polymer lots, includ- 0.1° to 90° degrees of arc using an appropriate frequency of oscil-
ing molecular weight, molecular weight distribution and the de- lation. Approximately 5.5 grams of material (+\- 5%) were uti-
gree of long-chain branching, are among the most influential lized and compressed in the testing cavity using a clamping pres-
parameters linked to changes in bulk compound and flow behav- sure of 4.5 bar. Samples were allowed to relax for 10-15 minutes
ior. Differences in the polymer architecture directly impact pro- in the testing cavity before viscoelastic measurements were per-
cessability and flow behavior, such as flow rate, die swell, melt formed in order to allow ample time for any internal stresses ex-
stability, recoverable shear and internal stresses in blow molding, perienced during the loading process to dissipate.
injection molding, sheet forming, cable jacket extrusion, among
other production processes (refs. 1-3). Rheological characteriza- Results and discussion
tion utilizing a rubber process analyzer (RPA) provides a quick Processing challenges with EPDM
and easy method to measure these properties, delivering a means In this example, the raw material supplier was switched from
to understand polymer structure and develop bulk property- EPDM 1 to EPDM 2. Both samples had similar product specifi-
structure relationships. These methods can provide production cations, with Mooney viscosities equal to 65 MU, ethylene per-
engineers and compounders with invaluable, predictive informa- cent around 50%, and the ENB content at 9% and 7.5%, respec-
tion regarding the processability of raw polymers and elasto- tively. Despite similar specifications, compounds produced with
meric compounds, which can be used to expedite and efficiently EPDM 2 experienced significant processing challenges, such as
develop solutions to processing problems. difficulties with extrusion and oil incorporation. A frequency
This article provides insights into advanced rheological mea- sweep was used to measure the viscoelastic response of each
surements both in the linear viscoelastic, small-strain regime, and sample as a function of time or frequency. The complex viscos-
in the nonlinear, high-strain regime, and how to correlate these ity as a function of frequency is shown in figure 1A. The com-
measurements to polymer chain architecture for elastomeric plex viscosity is a measurement of a material's ability to flow. A
products. We evaluate differences in polymer and rubber com- higher complex viscosity indicates the sample will exhibit a
pounds based on molecular weight, molecular weight distribu- greater resistance to flow compared to a sample with a lower
tion and long chain branching using a rubber process analyzer complex viscosity. Analyzing the complex viscosity as a function
(RPA). We present scenarios where the RPA was used to identify of frequency can be used to understand the overall flow profile
key differences in samples which correlated to processing differ- of the polymer compound through a production process. For
ences. Some of the testing techniques include standard frequency example, both samples show shear thinning behavior, demon-
sweeps and the linear and non-linear responses from standard strated by the complex viscosity decreasing as the shear rate or
strain sweep experiments. Results from these tests are also com- frequency increases. This correlates with a reduction in power
pared to standard tests such as Mooney viscosity and cure curves required to produce these materials, since materials of lower
from a moving die rheometer (MDR). viscosity generally require less energy to process compared to a
higher viscosity compound. EPDM 1 is shown to shear thin to a
Experimental greater degree, with the complex viscosity lower than EPDM 2
The RPA Elite (TA Instruments, New Castle, DE) is an advanced, at the higher frequencies.
rotorless rotational shear rheometer dedicated to the complete In addition to complex viscosity, data from a frequency sweep
viscoelastic characterization of polymers, rubber and rubber com- can also be analyzed by plotting the tangent delta as a function of
pounds at all stages of manufacturing. The RPA Elite provides frequency, shown in figure 1B. The tangent delta is simply the
invaluable data related to the viscoelastic behavior of materials in ratio of the viscous modulus to the elastic modulus (G”/G’), and
the pre-cure state, through the curing process, and in situ cured is related to a material’s elasticity. We can see that the tangent
state. Samples are sealed in a biconical die and compressed under delta for both samples is similar at a shear rate around 1.6 1/s,
high pressure forces, as is standard in the rubber industry. This which correlates to the shear rate applied to a sample in a
design provides a closed testing cavity which prevents melt frac- Mooney test. This is expected, since both samples were shown to

FOLLOW US ON TWITTER @rubberworld 25


Figure 1 - data from a frequency sweep show the complex viscosity (A) and tangent delta (B)
as a function of shear rate for EPDM 1 and EPDM 2; the frequency spectra demonstrate
viscoelastic differences between the two materials, despite similar Mooney viscosity
specifications

106 1.4
A EPDM 1 B
EPDM 2 1.2
Viscosity, K *(Pa.s)

1.0
105

Tan delta
0.8

0.6
104
0.4

0.2

103 0.0
0.01 0.1 1 0.01 0.1 1 10
Shear rate (1/s) Shear rate (1/s)

have a Mooney viscosity of 65 MU. Conversely, larger differ- predicting the flow behavior of these materials in processes
ences in behavior are observed at low shear rates, which are where a low shear rate is experienced, such as during start-up of
equivalent to longer time scales. EPDM 1 shows a lower tan the manufacturing processing, and especially as a material re-
delta value around 0.85 at the lowest tested shear rate, while laxes and flows within a mold.
EPDM 2 is approximately 1.25. A smaller tangent delta value A strain sweep was then used to investigate the presence and
indicates a larger amount of elasticity within the material, which degree of long chain branching between the two samples, shown
can correlate to a higher molecular weight or the presence of in figure 2. Both samples show similar behavior at small strains,
branching. Significant differences in the complex viscosity and with the elastic modulus, G’, around 80 kPa at low strains. The
tangent delta are observed at low frequencies which correlate to elastic modulus is related to the elastic component in the mate-
long time scales, indicating that the polymer architectures, such rial and correlates with the degree of structure within a material.
as molecular weight or degrees of branching, are different. Prob- A high modulus value corresponds to a strong microstructure,
ing within the low frequency region yields information associ- such as high molecular weight, a more rigid polymer chain
ated with molecular weight, which the Mooney test fails to chemistry, or interactions between the polymer and additives. At
measure. The low frequency response is particularly useful for strains less than approximately 2° of arc, the modulus for both
samples is independent of strain. This is expected and is identi-
fied as the linear viscoelastic regime. At strains higher than the
Figure 2 - data from a strain sweep are critical strain of 2° of arc, both moduli decrease, showing a de-
plotted as the elastic modulus (G’) and pendence on strain. This region is known as the non-linear re-
tangent delta as a function of strain; gime and can provide insight into the branching nature of the
significant differences between EPDM 1 material. Significant differences between the two polymers are
and EPDM 2 are observed at high strains, observed as deviations in tangent delta at high strain amplitudes.
in the non-linear regime Testing at strains within the non-linear regime show greater sen-
sitivity to differences in polymer architecture.
100 10
Shear modulus, G’ (kPa)

EPDM 1
9
Upon closer observation of the Lissajous plot at 90° of arc or
EPDM 2 1,255% strain, which is constructed by plotting the transient
8
stress versus shear rate, as shown in figure 3, the difference in
Tan delta

7
6 sample response is apparent. It is known that a Lissajous plot
10 5 showing secondary loops is indicative of a linear polymer archi-
4 tecture, while the absence of secondary loops is characteristic of
3 a branched polymer architecture (ref. 4). The data show EPDM
2 1 to be a branched polymer compared to EPDM 2, which is a
1 linear polymer. Further quantitative analysis can be performed by
1 0 calculating a long chain branching (LCB) index number based
0.1 1 10 100
on the stress versus shear rate response (refs. 5 and 6). A negative
Strain (° of arc)
LCB index is indicative of a linear polymer, while branched

26 RUBBERWORLD.COM ‡ JANUARY 2018


Figure 3 - the raw stress versus shear rate Figure 4 - moving die rheometer (MDR) cure
plot, known as a Lissajous plot, shown for curves of two batches of rubber compound;
EPDM 1 and EPDM 2 at 90° of arc or 1,255% the minimum torque of both curves is
strain; secondary loops are observed for similar, indicating they should process
EPDM 2 and an absence of loops is seen for similarly; however, behavior in the
EPDM 1, indicating differences in the manufacturing process differed
presence of long chain branching
14
300,000
12
250,000
10
150,000

S’ (dNm)
8
100,000
Shear stress (Pa)

6
50,000
4
0
-10 -8 -6 -4 -2 0 2 4 6 8 10 2 Sample 1
-50,000 Sample 2
0
-100,000 0 2 4 6 8 10 12 14 16 18 20
EPDM 1 EPDM 2
-150,000 Time (minutes)
LCB 1.21 -1.25
-200,000
index
manufacturing process, cured more slowly than sample 2, which
-250,000
showed no processing issues. In addition, both curves show a
Shear rate (1/s) similar minimum torque around 1 dNm. The results from the
MDR tests were unable to distinguish the differences between
polymers are indicated by a positive value. In this case, EPDM 1 the materials, and were not showing the information needed to
has an LCB index of 1.21, while EPDM 2 has an LCB index of identify the root cause of the processing issues.
-1.25, confirming that EPDM 1 is a branched architecture, while Frequency sweep tests on the RPA were performed to charac-
EPDM 2 is linear. The branched nature of EPDM 1 is also veri- terize both samples and correlate differences in viscoelasticity
fied by a higher viscosity and lower tangent delta at low frequen- with their processing behavior. The complex viscosity is shown
cies, shown in the frequency sweep in figure 1, both of which are as a function of angular frequency in figure 5. Both samples
indicative of a material with more elasticity. In addition, EPDM
1 demonstrated a greater degree of shear thinning compared to
EPDM 2. Long chain branching can improve additive incorpora- Figure 5 - data from a frequency sweep
tion and a material’s ability to shear thin, which aids with pro- show the complex viscosity as a function of
cessing. The processing issues experienced when switching from angular frequency for samples 1 and 2;
EPDM 1 to EPDM 2 can be traced back to the lack of long chain the frequency spectra show similar
branching in EPDM 2. Testing on the RPA was used to help behavior in processability between both
troubleshoot and discover the root cause of the processing chal- samples, especially in the high shear rate
lenges after switching EPDM suppliers. Few other analytical range which correlates with flow behavior
techniques are available to practically characterize these impor- in an extrusion process
tant polymer properties.

Extrusion instability of a rubber compound


Not only can the RPA be used to troubleshoot issues in process-
Viscosity, K *(Pa.s)

ing by measuring the viscoelastic properties of the raw polymer


material, but it can also be used to measure the properties of
rubber compounds. Differences in viscoelastic properties can 104
lead to difficulties within the production process. In this example,
extrusion instabilities were experienced during production. One
batch of material processed with no problems, while the other
batch demonstrated scorch problems in the extruder, resulting in Sample 1
a product with orange skin or orange peel texture. Both batches Sample 2
103
of rubber were tested with the moving die rheometer (MDR),
1 10 100
with representative curves shown in figure 4. The cure curves
show that sample 1, which exhibited scorch behavior during the Angular frequency (rad/s)

FOLLOW US ON TWITTER @rubberworld 27


show shear thinning behavior, with the complex viscosity de-
Figure 6 - data from a frequency sweep creasing as the angular frequency, and consequently shear rate,
show the tangent delta as a function of increase. However, sample 1 is shown to have a slightly lower
angular frequency for samples 1 and 2; viscosity at elevated frequencies, which corresponds to high
significant differences in the viscoelastic shear rates. Conversely, sample 1 also shows a higher viscosity
response between the samples are at the low angular frequencies, corresponding to a stronger resis-
observed at low angular frequency, which tance to flow. This usually correlates with a higher degree of
correlates with polymer architecture; elasticity. The difference in elasticity between the samples is
sample 1 shows a lower tangent delta highlighted in figure 6, by replotting the same data as tangent
value, indicating a higher degree delta as a function of frequency. The tangent delta between both
of elasticity samples is significantly different, with sample 1 showing a value
of 0.725 at 1 rad/s compared to 0.89 for sample 2. This indicates
1.0
sample 1 is more elastic compared to sample 2. The increase in
0.9 elasticity can be attributed to higher molecular weight or the
0.8 presence of long chain branching.
0.7 Further analysis included a large amplitude oscillatory shear
(LAOS) test on both samples, where the strain was varied from
Tan delta

0.6
0.5 0.3% to over 1,000% strain. The storage modulus (G’) and the
0.4 tangent delta for both samples are shown as a function of strain
percent in figure 7. Deviations in behavior are seen as the applied
0.3
strain increases in the non-linear regime. The storage modulus for
0.2 Sample 1 sample 1 remains higher than for sample 2, indicating a stronger
0.1 Sample 2 elastic structure within the material. As previously discussed, this
0 equates to a stronger microstructure, usually as a result of higher
1 10 100
molecular weight, polymer rigidity and additive interactions. This
Angular frequency (rad/s)
is also corroborated by the tangent delta signal, with sample 1
showing a lower tangent
delta, which corresponds to a
Figure 7 - data from a strain sweep are plotted as the elastic modulus larger degree of elasticity.
(G’) and tangent delta as a function of strain; significant differences The data at 90° of arc, or
between the rubber compound samples are observed at high strains; in strain percent of 1,255%, can
the non-linear regime, the Lissajous plot shown for both samples at be recast by plotting the tran-
90° of arc (inset) indicates differences in long chain branching and sient shear stress against the
energy dissipated during the applied oscillation shear rate in the Lissajous
plot. The long chain branch-
6 ing index can be calculated
Sample 1 from the Lissajous plot. Both
Sample 2 Lissajous plots show a lack
Sample 1 Sample 2 of secondary loops, indicat-
5
LCB index 2.73 0.18 ing the presences of long
chain branching. This is con-
Shear modulus, G’ (kPa)

Wdiss 177 J 169 J


4 firmed with positive long
Strain 90.018 (Grad.)
chain branching index values
Tan delta

150,000
of 2.73 and 0.18 for samples
100,000
Stress, V (Pa)

10 3 1 and 2, respectively. The


50,000
long chain branching index
0
-50,000 indicates that sample 1 has a
100,000 2 higher degree of long chain
branching compared to sam-
-20 -10 0 . 10 20 ple 2, which was confirmed
Shear rate, J(1/s)
1 through the tangent delta
value in the frequency and
amplitude spectra. Recall,
1 0 sample 1 demonstrated a
0.1 1 10 100 1,000 lower tangent delta, which
Strain (%) corresponds to a higher de-
gree of elasticity.

28 RUBBERWORLD.COM ‡ JANUARY 2018


Figure 8 - the tangent delta and long chain branching (LCB) index before and after the mixing
simulation for two samples of butadiene rubber are shown; the viscoelastic properties of BR 1
are relatively unaffected by shear and temperature, while BR 2 shows a significant change,
indicating some instability within the material

5.0 8 Before aging


Before aging
After aging After aging
4.0
6

LCB index
Tan delta

3.0
4
2.0

2
1.0

0.0 0
BR 1 BR 2 BR 1 BR 2

The presence of long chain branching contributes to the elas- sample 1 shows a larger amount of energy dissipated at high
tic character of the material. Usually, the presence of long chain shear which is akin to the shear rates experienced within the ex-
branching improves processability; however, process engineers truder. The larger amount of energy dissipation could cause local
saw challenges and scorching problems with sample 1, despite temperature increase within the sample as it is sheared within the
the higher degree of long chain branching. The work dissipated extruder.
during oscillation and shear can be calculated from the Lissajous Despite the MDR cure curve showing sample 1 would cure
plot by measuring the area within the ellipse when plotting tran- more slowly, local temperature elevations within the sample as a
sient stress against strain. This work is associated with viscous result of energy dissipation from the induced shear in the ex-
heating; this heat must be removed from the material or it will truder could result in scorching of sample 1 during the extrusion
result in local temperature rise. Analysis at 90° of arc, or strain process. The RPA was able to quantify differences between the
percent of 1,255%, shows the work dissipated to be 177 J and two rubber compounds and help process engineers optimize their
169 J for samples 1 and 2, respectively. Compared to sample 2, processing conditions by decreasing the extruder speed, and then
re-evaluating the compound formulation.

Figure 9 - the percent change in BR 1 and Stability differences in BR from different suppliers
BR 2 due to the simulated mixing step is For some polymers, such as BR, SBR and NBR, it is important
shown; the tangent delta and LCB index in to understand the amount of aging experienced when subjected
BR 1 are unaffected, with a percent change to shear and temperature, such as in a mixing process. In this
less than 3% and 15%, while the case, the RPA can be used to stress the polymer under high shear
viscoelastic properties for BR 2 are highly and temperature, mimicking the mixing procedure while evalu-
affected, with changes on the order of 50% ating the changing of the structure of the polymer by measuring
and 100% the viscoelastic properties. With a proper testing method, the
RPA can be used to characterize a material before the mixing
120
Difference before/after aging (%)

process, simulate a mixing procedure, and then characterize the


101.74
100 Tan delta material after the mixing simulation, all in one test. Two samples
LCB index of BR containing the same specifications of 45 MU, cis-1,4
80 content % > 96 were obtained from different suppliers. The
aging process was simulated in the RPA by applying an oscilla-
60 53.76 tory strain of 400% at 1 Hz over 10 minutes at 150°C. The vis-
coelastic properties were measured using a frequency sweep
40
and amplitude sweep before and after the aging process. The
20 14.45 tangent delta and long chain branching index before and after
2.74 the aging process are shown in figure 8. The viscoelastic proper-
0 ties for BR 1 were not significantly changed during the simu-
BR 1 BR 2 lated mixing step, with the tangent delta remaining around 2.5
and the LCB index increasing by less than 1. However, the

FOLLOW US ON TWITTER @rubberworld 29


tangent delta for BR 2 after the simulated mixing step decreased used to measure the stability of butadiene rubbers and identify a
from over 4 to below 3, and the LCB index increased from less lack of polymer stability due to an increase in long chain branch-
than 4 to over 7, indicating a significant change in polymer ar- ing.
chitecture due to the mixing process. The changes in BR 1 for Understanding the flow behavior of a material over several
tangent delta and the LCB index were less than 3% and 15%, shear rates is becoming more important, since a wider variety
respectively. In comparison, the tangent delta changed over 50% of synthesis techniques with varying catalysts is now being
and LCB index over 100% for BR 2, shown in figure 9. The used, which can lead to an array of viscoelastic properties from
decrease in tangent delta and increase in LCB index correspond supplier to supplier and even batch to batch. Testing data from
to an increased degree of branching after the mixing step. It is an RPA can be used to identify variations in polymer architec-
known that for some butadiene rubber samples, a shear-induced ture, providing insight to the flow behavior so production pa-
reaction can occur on the carbon-carbon double bond on the rameters can be optimized in advance, and waste can be re-
backbone, which can create long chain branches in the polymer, duced.
depending on the stabilization method used during synthesis.
Testing these two butadiene rubbers shows BR 2 to be less sta- References
ble than BR 1. Quantifying and measuring the changes in poly- 1. H.A. Barnes, An Introduction to Rheology, Elsevier, 1989.
mer architecture due to the mixing process can help process 2. C.W. Macosko, Rheology: Principles, Measurements and Ap-
engineers screen early in the manufacturing process and make plications, VCH Publishers, New York, 1994.
adjustments as needed. 3. N.W. Tschoegl, The Phenomenological Theory of Linear Vis-
coelastic Behavior, Chapter 9, pp. 443-483, Springer-Verlag,
Summary 1989.
The RPA can be used to measure the viscoelastic properties of 4. R.H. Ewoldt and G.H. McKinley, Rheol Acta (2010), 49: 213,
rubber compounds and raw polymers as a function of shear rate https://doi.org/10.1007/s00397-009-0408-2.
and deflection, which are directly linked to flow and processing 5.F.J. Stadler, A. Leygue, H. Burhin and C. Bailly (2008), “The
behavior. Data obtained from frequency sweeps and amplitude potential of large amplitude oscillatory shear to gain an insight
sweeps can be used to identify differences in polymer architec- into the long-chain branching structure of polymers,” In: The
ture, such as the presence of long chain branching and variations 235th ACS national meeting, polymer preprints ACS, vol. 49,
in molecular weight and molecular weight distribution. Testing New Orleans, LA, pp 121-122.
on the RPA was able to distinguish differences in EPDM lots 6. H.G. Burhin, C. Bailly, R. Keunings, N. Rossion, A. Leygue
from varying suppliers and rubber compounds where the stan- and H. Pawlowski (2008), “A study of polymer architecture with
dard Mooney and MDR tests failed. FT-rheology and large amplitude oscillatory shear (LAOS),” In:
In addition, the RPA could be used to simulate the mixing XV International Congress on Rheology: The Society of Rheol-
process by inducing shear at a controlled temperature. Viscoelas- ogy 80th Annual Meeting, Monterey, CA, The Society of Rheol-
tic testing before and after the simulated mixing step could be ogy, Abstract Booklet, EM18.

Prediction of rolling resistance


(continued from page 24)
bon silica dual phase filler in green tire tread formulations,” p.
342, proceedings of the International Rubber Conference
Blue Book, Rubber Red (IRC98), Chennai, India, December 7-9, 1998.
37. J.E. Bice, S.D. Paktar and T.A. Okel, Rubber World, p. 58,
Book and the Chemical Vol. 217, No. 1, October 1997.
Resistance Guide for 38. L. Ladouce-Stelandre, Y. Bomal, L. Flandin and D. Labarre,
Rubber Chemistry and Technology, p. 145, Vol. 76, No. 1, March-
Elastomers April 2003.
39. M. Gerspacher, C.P. O’Farrell, H.H. Yang and L. Nikiel,
Buy online at Website: Rubber World, p. 27, Vol. 220, No. 1, April 1999.
www.rubberworld.com 40. C.R. Stone, M. Hensel and K.H. Menting, Kautschuk Gummi
Magazine’s
Kunststoffe, p. 568, Vol. 51, No. 9, 1998.
Blue Book
41. Instrument User Manual for Rebound Resilience Tester
Materials, compounding ingredients, machinery and services for the rubber industry.

(EKT-2108-RR), Cat. No. ekt-1005-1e from Ektron Tek Co. Ltd.,


Taiwan.
42. Dynatest Software User Manual for DMA1000+ Model from
W
NE ION Metravib R.D.S., France.
DIT
E 43. Richard I. Levin and David S. Rubin, Statistics for Manage-
A Lippincott and Peto Publication

ment, 7th Edition, 1998.

30 RUBBERWORLD.COM ‡ JANUARY 2018


Rheology of EPDM compounds made of
equal Mooney, equal composition
polymers: Differentiation beyond typical
EPDM parameters
by Juan Tuberquia, Colin Li Pi Shan, Sharon Wu, Greg Li, the discussion of how to define polymer architecture.
Lena Nguyen, Teresita Kashyap, Tianzi Huang, David Gil- In this scenario of multiple options, when a rubber chemist is
lespie, Cory Thomas and Kristel Blackwell, Dow Chemical confronted with choosing a polymer, three additional questions
should be considered: 1) How is it possible to categorize any
EPDM rubber has a proven track record of more than 50 years, molecular weight distribution and LCB combinations? 2) How
which has resulted in today’s availability of more than 200 grades does such categorization relate to processability and performance
within a broad window of Mooney viscosity, ethylene and diene properties? 3) Besides the specific window of possibilities tradi-
content. From the polymer architecture point of view, EPDM of- tionally available, what other polymer architectures are available
ferings have been traditionally defined by the capabilities of the today? A few hints to address these questions were discussed in
Ziegler Natta catalysts and process. However, the scope of poly- previous research (ref. 1) after exemplifying how Mooney vis-
mer architectures expanded in 1997 with the appearance of metal- cosity is an insufficient predictor of the polymer molecular
locene catalysts, and today with advanced molecular catalysts weight and how other architectural parameters such as molecular
(AMC) and state-of-the-art solution process technology. weight distribution and long-chain branching needed to be con-
Based on the broad selection of EPDM, a key question fo- sidered. For that purpose, a series of 32 Mooney, EP polymers
cuses on understanding if comparable polymers (similar Mooney
viscosity and composition) can be considered a “drop in” for
processing and performance. There are multiple aspects to con- Figure 1 - key degrees of freedom to define
sider in addressing this question; however, the first of them is to the polymer architecture and composition
have a base understanding that the polymer architecture attempts of EPDM
to balance a high molecular weight fraction responsible for good
physical properties and high filler loading, and a low molecular Low MW component
weight component that reduces overall polymer viscosity to
favor processability. As expected, complexity increases with not High MW component
only composition, but also as branching (ref. 1) is considered as
Weight fraction

part of the design. In this article, branching is an architectural Long chain


parameter defined by the presence of polymer branches, their branching
frequency per chain, their length, and how much of the popula-
tion has a branched character. Branching can manifest as a rheo-
logical effect, such that with the increase of any of these features, ENB composition
the higher the viscosity, the elasticity and the shear thinning be-
havior. This situation can be exemplified, as shown in figure 1, C2 composition
after considering a specific EPDM with an average Mooney
viscosity (MV), ethylene (C2) and diene content made of high
and low molecular weight components that can be individually Molecular weight (MW)
tailored. As shown in figure 1 and table 1, if we use the weight Low High
fraction, the molecular weight, the composition (diene,
C2), and the degree of branching of one of the components
as degrees of freedom, there would be more than 100 dif- Table 1 - selected examples of the degrees of
ferent ways to design a single polymer. Such an example freedom that define the polymer architecture and
uses two levels of variation for both molecular weight and composition of EPDM
long chain branching (LCB), and three levels for weight
High MV component versus low MV component
fraction, diene and C2 content. Such a level of variation is
Variable Weight Molecular Diene C2 Overall
relative between the high and low molecular weight com-
fraction fraction content content LCB
ponents and defined as: 1) high, 2) low and 3) “same,”
3 2 3 3 2
which refers to equal relative amounts. The situation ex-
plains how, in addition to the traditional parameters Levels High High High
High Low
(Mooney viscosity [ref. 2], C2, diene), both molecular Same
Low
Same Same
High
weight distribution and branching have been brought to Low Low Low

FOLLOW US ON TWITTER @rubberworld 31


with a high ethylene content (80% ethylene) were characterized bulged after the trimming step to a test gap of 2 mm. The method
and compounded using a 210 phr rubber-rich formulation. Dif- had an additional five minute delay built in to allow the system
ferences in the mixing profile among the samples were attributed to reach thermal equilibrium. Tests were performed under a ni-
to their distinct rheological profile, with the highly elastic poly- trogen atmosphere.
mer exhibiting fast filler breakup and incorporation, rapid tem- Mooney viscosity (ML1+4) of the EPDM rubbers was mea-
perature rise and fast transition to the final power uptake plateau. sured at 125°C, and that of the compounds at 100°C in accor-
Despite these appreciable observations, a couple of aspects re- dance with ASTM D1646-04, with a one minute preheat time
quire further consideration: 1) the effect of crystallinity above and a four minute rotor operation time. The instrument was an
room temperature (CATR), and 2) access to higher molecular Alpha Technologies Mooney viscometer MV2000E.
weights to better decouple molecular weight distribution and A high temperature gel permeation chromatography (GPC)
LCB. system consists of an infrared concentration/composition detec-
Evaluating every single variation of the polymer architecture tor (IR-5) and three Agilent mixed B 10 um columns. The carrier
at a fixed overall composition and Mooney viscosity is impracti- solvent was 1,2,4-trichlorobenzene (TCB). The main oven was
cal; however, we can categorize both molecular weight distribu- operated at 150°C. The sample solutions were made at a concen-
tion and LCB at two extreme levels (low and high) to probe their tration of 2 mg/mL by dissolving samples for two hours at
effect. For this purpose, in this article, MWD' is defined as the 160°C. The injection volume was 200 μl, and the flow rate was
Mz/Mn ratio measured by GPC to capture the low and high aver- 1.0 mL/minute. The GPC column set was calibrated by narrow
age molecular weights characteristic of a distribution. Molecular polydispersity polystyrene standards, then we converted the PS
weight distribution (MWD') for the polymer set evaluated in the molecular weight to polypropylene relative molecular weight
previous study was below 7 (ref. 1). As mentioned, branching using the universal calibration concept. The IR-5 composition
translates into a rheological effect and can be captured by any mode was calibrated using a PE reference (0% of propylene) and
YLVFRVLW\ DWVKHDURUH[WHQVLRQ HODVWLFLW\ 7DQį¨į9DQ*XUS a PP reference (100% of propylene). The calibration and the
Palmen plot) (ref. 3), or shear thinning indicator. Out of these, calculation of wt% of co-monomer at each elution component
elasticity was selected as an LCB indicator measured by dy- were performed using the response ratio of the methyl window
QDPLFPHFKDQLFDOVSHFWURVFRS\ '06 DWƒ&DVWKH¨įRU over methylene window of the IR-5 composition detector.
difference in the phase angle at 0.1 and 100 Rad/s. In this article, Differential scanning calorimetry (DSC) is used to measure
we focus on the effect of mixing for both amorphous (A) and crystallization behavior of polymers. The sample is first melt
semicrystalline (SC) EPDM polymers at a constant Mooney pressed (25,000 pounds for about 10 seconds) into a thin film, at
viscosity of 70, and an ethylidene norbornene (ENB) content of about 175°C, and then cooled to room temperature. About 5 to 8
5%. This study first focused on amorphous polymers in the C2 mg of polymer film sample is cut with a die punch and is
window from 46-54% for simplicity, as any effect of crystallinity weighed and placed into a DSC pan. The lid is crimped on the
is negligible. Analysis intends to provide an integral view of the pan to ensure a closed atmosphere. The sample pan is placed into
mixing process in a high filler formulation (425 phr), by not only a calibrated DSC cell purged with nitrogen gas, and then heated
focusing on the temperature rise and power uptake, but also in- at a rate of approximately 10°C/minute to a temperature of
corporates RAM distance information to provide an idea of 180°C. The sample is kept at this temperature for three minutes.
mixer volume utilization. Subsequently, the article compares the Then the sample is cooled at a rate of 10°C/minute to -40°C to
mixing of the semicrystalline polymers within a C2 window record the crystallization trace, and kept isothermally at that
from 69-71%. Mixing semicrystalline grades has an additional temperature for three minutes. The sample is next reheated at a
complexity component from the remaining crystallinity above rate of 10°C/minute until complete melting. Crystallization
room temperature (CATR). For this reason, before making any above room temperature (CATR) was calculated as the enthalpy
observations about the effect of polymer architecture, both the above 25°C during the second heat.
effect of CATR and that of the formulation are considered.
EPDM selected examples
Experimental section Based on their GPC and rheology characterization, polymers
Characterization methods were categorized at two extreme levels of MWD' (broad: bMWD'
The elasticity effect of representative polymer examples was and narrow: nMWD') and elasticity (high: HE and low: LE). For
EDVHGRQWKHLU¨įRUGLIIHUHQFHLQWKHSKDVHDQJOHDWDQG this purpose, MWD' was defined by the Mz/Mn ratio measured
Rad/s obtained by a dynamic mechanical spectroscopy (DMS) by GPC, and elasticity of representative polymer examples was
frequency sweep test at 190°C at a strain of 5%. Tests were per- EDVHGRQWKHLU¨įRUGLIIHUHQFHLQWKHSKDVHDQJOHDWDQG
formed on stainless steel parallel plates of 25 mm diameter by Rad/s measured by dynamic mechanical spectroscopy (DMS) at
using strain controlled rheometers (ARES-G2 by TA Instru- 190°C. Polymers A/bMWD'/HE and SC/bMWD'/HE are com-
ments). Compression molded disks were prepared on a Carver mercially available Ziegler Natta EPDMs. The rest of the poly-
press at 190°C and 25,000 psi for five minutes; samples were mers discussed throughout this document were made with InSite
cooled down to room temperature on a counter top. Disks of 3.3 advanced molecular catalyst (AMC) technology. Both amor-
mm thickness were placed between parallel plates at 190°C and phous and semicrystalline polymers used in this document have a
squeezed to a gap of 2.1 mm. The excess material was trimmed Mooney viscosity of 70, and an ethylidene norbornene (ENB)
after the normal force relaxed below 300 g. The sample was content of 5%. C2 variation for the amorphous polymers ranged

32 RUBBERWORLD.COM ‡ JANUARY 2018


Table 2 - composition, MV, MWD' and the Figure 2 - categorization of elasticity and
¨į information for four amorphous and molecular weight distribution
four semicrystalline, 70 MV, 5% ENB
polymers

Molecular weight distribution


Polymer type % C2 % ENB MV Mz/Mn ¨į CATR, Broad
J/g
A/bMWD'/HE 54.0 4.5 73 10.3 0.2 --
A/bMWD'/LE 47.1 4.8 69 8.7 0.9 --
A/nMWD'/HE 46.4 5.1 68 5.5 0.4 --
A/nMWD'/LE 50.1 5.0 72 5.1 0.8 --
SC/bMWD'/HE 71.0 4.6 72 8.9 0.2 18.7 Narrow
SC/bMWD'/LE 70.7 4.7 71 10.0 1.5 28.3
SC/nMWD'/HE 69.7 4.8 65 6.1 0.2 15.3
SC/nMWD'/LE 70.8 4.9 72 5.7 0.7 23.3
Low High
from 46-54%, while for Elasticity
Table 3 - compound the semicrystalline from
formulation 69-71%. The characteris- make these polymers reveals the Ziegler Natta examples exhibit
tics of these polymers are the bMWD'/HE combination, while AMC examples exhibit the
Ingredient Phr
Rubber 100 shown in tables 2 and 4. nMWD'/LE combination. Interestingly, the graph also reveals
N-660 carbon black 156 that the AMC catalyst system enables the access to two unprec-
Oil 104 Compound preparation edented architecture combinations: the broad MWD', low elastic-
Atomite 45 Compounds were pre- ity (bMWD'/LE) and the narrow MWD', high elasticity (nMWD'/
Zinc oxide 10 pared using the upside HE). As mentioned in a previous study, these examples clearly
Calcium oxide 10
Sulfur 1.5 down material addition show how, in addition to MV, additional parameters such as Mz/
Total 426.5 method where fillers and 0QDQG¨įDUHUHTXLUHGWREHWWHUGHVFULEH(3'0SRO\PHUV
oil were first added to a As a result of the MWD' and elasticity differences between
1.6 L Farrell Banbury the polymers described in this article, we focus the attention on
mixer (BR 1600) at a rotor speed of 50 rpm and mixed with the their mixing behavior. We first focus on the analysis of amor-
ram up for up to one minute. Subsequently, the polymer was phous polymers for simplicity, as any effect of crystallinity is
added to the bowl and the ram was brought to closure. The mix- practically negligible in the C2 window from 46-54%. Analysis
ing time was set at four minutes to ensure complete incorporation intends to provide an integral view of the mixing process by not
and dispersion of the formulation components. Mixing was only focusing on the temperature rise and power uptake, but also
completed on a 6” two-roll mill. incorporates ram distance information to provide an idea of
mixer volume utilization. All polymers in this study were mixed
Results and discussion using the formulation in table 3. Formulations were mixed in a
As mentioned, one of the purposes of this article is to categorize 1.6 L internal mixer for four minutes using an upside down
two extreme levels of MWD' (broad: bMWD' and narrow: method. The internal mixer was instrumented to record mixing
nMWD') and elasticity (high: HE and low: LE) in an effort to power, temperature rise, ram position and energy consumption
compare distinct polymer architectures. For this purpose, MWD' during compounding, as shown in figure 3.
is defined by the Mz/Mn ratio measured by GPC, and elasticity The figure shows the evolution of power, temperature, ram
LQIRUPDWLRQLVFDSWXUHGE\WKH¨įRUGLIIHUHQFHLQWKHSKDVHDQJOH position and total energy consumption over time for the four
at 0.1 and 100 Rad/s measured by dynamic mechanical spectros- amorphous samples. In terms of the power consumption, the four
copy (DMS) at 190°C. Table 2 shows the composition, the MV samples exhibited a single peak related to filler incorporation
LQIRUPDWLRQWKH0:'
DQGWKH¨įLQIRUPDWLRQIRUIRXUDPRU- right after the ram closed, followed by a gradual decay until it
phous and four semicrystalline, 70 MV, 5% ENB polymers. As reaches a plateau at around 3 kW at the end of the mixing cycle.
shown, the C2 range for the amorphous grades ranges from 46% This decay is comparable for all samples, except for the bMWD'/
to 54%, and that for the semicrystalline grades has a tighter range
from 69% to 71%. The MWD' represented by the Mz/Mn ranged
from 5 for nMWD' to 11 for bMWD' polymers. In the case of Table 4 - characteristics of two
HODVWLFLW\WKH¨įZDVVHOHFWHGDPRQJRWKHU/&%LQGLFDWRUVDQG semicrystalline, bMWD'/LE, 70 MV, 5% ENB
its values ranged from 1.5 for LE to about 0.2 for HE. polymers with two levels of crystallinity at
To categorize the extremes represented by the selected poly- 71% and 66% C2
mer examples, figure 2 plots Mz/Mn based on their elasticity.
The figure shows four distinct regions representing elasticity: Polymer C2 MV Mz/Mn ¨į Temp.,°C CATR, J/g
P1 70.7 71 10.0 1.5 43.2 28.3
MWD' combinations, each one having an amorphous and a P2 65.8 69 12.7 1.5 9.3 3.8
semicrystalline example. A look at the catalyst system used to

FOLLOW US ON TWITTER @rubberworld 33


Figure 3 - mixing profile of the amorphous, constant Mooney viscosity EPDM samples

8 25
7.5
7 LE HE
6.5 bMWD' 20

Ram distance (mm)


6
5.5
5 nMWD' 15
KW (kW)

4.5
4
3.5 10
3
2.5
2 5
1.5
1
0.5 0
0 30 60 90 120 150 180 210 240 0 20 40 60
Time (seconds) Time (seconds)
115 0.75
110 0.7
105 0.65

Total specific energy (kJ/kg)


100 0.6
Batch temperature (°C)

95 0.55
90
85 0.5
80 0.45
75 0.4
70 0.35
65 0.3
60 0.25
55 0.2
50
45 0.15
40 0.1
35 0.05
0 30 60 90 120 150 180 210 240 0
0 30 60 90 120 150 180 210 240
Time (seconds) Time (seconds)

considered fast to mix; however, an integral view of the mixing


Table 5 - carbon black to oil ratios used to parameters showed that this polymer was slower to incorporate
explore the effect of formulation on the other ingredients in the mixing volume, and had a higher ten-
mixing profile dency to convert the mechanical energy of the mixing into ther-
mal energy (heat).
Samples S2 S3 S4 S5 S6 After establishing the profile of amorphous polymers, we
CB/oil 1.5 1.4 1.3 1.2 1
MV 55.4 49.9 44.4 38.9 30.8
move forward and compare the mixing of semicrystalline poly-
mers within a C2 window from 69-71%. Mixing semicrystalline
grades has an additional complexity component from the remain-
HE polymer, which exhibited a slower decay. Evolution of the ing crystallinity above room temperature (CATR). For this reason,
batch temperature corresponded to the power uptake profile, before making any observations about the effect of polymer archi-
with samples exhibiting a drop temperature between 105 and tecture, both the effect of CATR and that of the formulation were
115°C. The corresponding higher dropping temperature for the considered. To evaluate the effect of CATR, table 4 shows the
bMWD'/HE polymer shows the tendency of this type of elastic characteristics of two semicrystalline polymers at 71% and 66%
material to develop more shear heating relative to the other poly- C2, both exhibiting a bMWD'/LE architecture at 70 MV and 5%
mers. Similarly, bMWD'/HE also took the longest of all samples ENB. Similar to the amorphous polymers, these two were mixed
to bring the ram to closure in the first minute of the mixing cycle. in a similar fashion using the recipe in table 3. The effect of the
Note that a common practice in the industry is to complete the formulation in the mixing profile is assessed by modifying the
mixing cycle based on the batch temperature. The dropping tem- recipe in table 3 to expand the carbon black (CB) to oil ratio from
perature is a tight window, typically above 90°C and below 1 to 1.5 using a polymer similar to the P1 shown in table 4.
125°C for fully formulated, one pass mixing to balance the good Figure 4 shows the effect of CATR on the mixing of bMWD'/
mixing/dispersion of all ingredients in the formulation and mix- LE polymers with a Mooney viscosity of 70. The figure shows
ing process safety (scorch safety). The mixing profile from this that the low CATR polymer (P2) exhibited a similar mixing
study shows that the bMWD'/HE polymer would have been profile to the amorphous 70 MV polymers described earlier. In

34 RUBBERWORLD.COM ‡ JANUARY 2018


Figure 4 - effect of crystallinity on the mixing profile of two bMWD'/LE polymers

8 25
7.5
7
6.5 P1 20

Ram distance (mm) 2


6 P2
5.5
5 15
KW (kW)

4.5
4
3.5 10
3
2.5
2 5
1.5
1
0.5 0
0 30 60 90 120 150 180 210 240 0 20 40 60
Time (seconds) Time (seconds)
115 0.75
110 0.7
105 0.65

Total specific energy (k/kg)


100 0.6
Batch temperature (°C)

95 0.55
90 0.5
85 0.45
80 0.4
75 0.35
70 0.3
65 0.25
60 0.2
55 0.15
50 0.1
45 0.05
40 0
35
0 30 60 90 120 150 180 210 240 0 30 60 90 120 150 180 210 240
Time (seconds) Time (seconds)

particular, the power uptake exhibited a fast CB incorporation figure, the power uptake profiles exhibit either one peak, like that
peak that gradually decayed until reaching about 3 kW. However, at a CB/oil ratio of 1, or two at a ratio of 1.5. The single peak at
in the case of the high CATR polymer (P1), the power uptake the low CB/oil ratio was attributed to the initial sluggish filler/oil
exhibited two distinct peaks correlated with CB incorporation incorporation peak. As the CB/oil ratio increased, the incorpora-
and dispersion. Note the filler incorporation peak at about 15 tion became faster and the incorporation peak gradually moved
seconds coincidentally matches the melting temperature of P1. to shorter times due to the absence of the lubricating effect. The
We suspect incorporation and dispersion of carbon could only be second filler dispersion peak started developing at a CB/oil ratio
achieved when the EPDM reached the melting temperature and of 1.4, to fully appear at a ratio of 1.5. As observed, the presence
softened. However, as described later, the formulation has a clear of large amounts of oil has a detrimental impact on the CB incor-
impact on the position of this peak. The graph also shows that the poration, which translates into late incorporation peaks and a
low CATR polymer exhibited a faster temperature rise, as well as dramatic reduction in the temperature rise. Note that the tem-
a more effective use of the mixer volume, with the ram position perature rise profile clearly shows two temperature ramps: 1) a
coming down to zero much faster. Note that despite the fact the fast ramp at the beginning of the mixing cycle clearly associated
final temperature is the same for both polymers, the figure shows with CB incorporation and dispersion, and 2) a slower ramp
that the energy required for the high CATR polymer is greater comparable within the evaluated window of CB/oil ratios associ-
and that it translates into a higher temperature rise for mixing ated with having a homogeneous compound.
cycles beyond four minutes. As mentioned, to understand the effect of architecture in the
Figure 5 shows the effect of varying the CB/oil from 1 to 1.5 mixing profile of semicrystalline polymers, we need to consider
at a constant overall phr of 426. Maintaining a constant overall the effect of CATR as an additional variable compared to the
phr was a key parameter in this set of experiments in an attempt amorphous set. Furthermore, we recognized that any trends
to maintain a constant polymer basis where CB increased at the made are formulation dependent and may vary for different phr
expense of oil. A CB/oil ratio of 1 offers an oil rich environment, formulations. In an attempt to make a fair comparison, we se-
while a ratio of 1.5 refers to a high filler loading. As shown in the lected a series of polymers within a tight C2 window between

FOLLOW US ON TWITTER @rubberworld 35


HE polymer had the most intense dispersion peak of all the
Figure 5 - effect of the CB/oil ratio in the polymers; however, its profile takes the longest to reach a flat
mixing profile of a semicrystalline, bMWD'/ power draw at the end of the mixing cycle. On the other hand,
LE polymer nMWD'/HE exhibited the least intense dispersion peak, the fast-
est decay in power and, interestingly, it exhibited a single CB
14
13 incorporation peak. Since neither of the HE polymers seems to
12 n CB conclusively be the fastest mixing, then crystallinity does not
11 appear to be the dominant effect at the CATR levels in this study.
10
9 To better capture the observations related to polymer architec-
ture during mixing, table 6 listed five attributes associated with
Offset kW

8
7 distinct events during this process and categorized their perfor-
6 mance. Based on this table, the nMWD' polymers exhibited a
5
4 fast temperature rise throughout the mixing cycle; the ram came
3 down the fastest to a closed position, and the power draw had a
2 fast stabilization at about 3 kW. In the case of the nMWD'/LE
1
0 architecture, the polymer also exhibited strong intensity of the
-1 CB incorporation peak comparable to the bMWD' polymers.
Note that the differences in architecture played a more prominent
0
20
40
60
80
100
120
140
160
180
200
220
240
differentiating role in the case of mixing semicrystalline poly-
Time (seconds) mers. Compared to the amorphous polymers, the bMWD'/HE
architecture characterized in both the amorphous and semicrys-
105 talline polymers exhibited a slow decay in the power draw and
100 took more time for the ram to fully close.
95
90
Batch temperature (°C)

85 Summary
80 To understand the effect of polymer architecture on the mixing
75
70 process of EPDM, this article selected a series of representative
65 EPDM polymers and categorized them into four distinct MWD'/
60
55 n CB LCB combinations. LCB information was captured by its effect
50
RQHODVWLFLW\XVLQJWKH¨įRUGLIIHUHQFHLQWKHSKDVHDQJOHDW
45 and 100 Rad/s, but observations can be equally extended to other
40 rheological indicators of viscosity or shear thinning. The selected
polymers covered both amorphous and semicrystalline composi-
tions at 70 MV, and 5% ENB. Mixing cycle information in-
0
20
40
60
80
100
120
140
160
180
200
220
240

cluded power uptake, temperature rise, ram distance position and


Time (seconds) total energy consumption to provide an integral view of the
process using a common formulation of 425 phr. Results enabled
69.5 and 71%; nevertheless, the CATR varied significantly be- characterizing the response of these parameters as a function of
tween 15 and 30 J/g. Mixing profile information is shown in molecular architecture, crystallinity and variation in the formula-
figure 6 for the semicrystalline polymers,
following a similar compounding process to
that of the amorphous ones and still using the Table 6 - desired mixing attributes based on polymer
formulation in table 3. architecture for the semicrystalline polymers
If we start the discussion based on the ef-
Attribute bMWD'/HE bMWD'/LE nMWD'/HE nMWD'/LE
fect of CATR, table 2 would suggest that the Strong intensity of the CB ++++ +++ + ++++
low values exhibited by the HE polymers incorporation peak (0 to 30
would translate into features denoting easy seconds)
mixing. Note that both a fast development of Temperature rise ramp at the + ++ +++ ++++
an intense CB incorporation peak and a fast beginning of the cycle (0 to
30 seconds)
decay in power at the end of the mixing cycle Fast stabilization of the RAM + ++ ++++ +++
are typically considered attributes of a fast at the closed position (first
mixing polymer. The CATR variation in de- minute of cycle)
scending order is: Fast decay of power + ++ ++++ +++
HE polymers (bMWD' and nMWD') > (second minute of cycle)
Temperature rise ramp at the + ++ +++ ++++
nMWD'/LE > bMWD'/LE end of the cycle (last minute
The power curves show that both HE poly- of cycle)
mers exhibited distinct profiles. The bMWD'/

36 RUBBERWORLD.COM ‡ JANUARY 2018


Figure 6 - mixing profile of the semicrystalline, constant Mooney viscosity EPDM samples

8 25
7.5 LE HE
7
6.5 bMWD' 20

Ram distance (mm) 2


6
5.5 nMWD'
5 15
KW (kW)

4.5
4
3.5 10
3
2.5
2 5
1.5
1
0.5 0
0 30 60 90 120 150 180 210 240 0 20 40 60
Time (seconds) Time (seconds)
115 0.75
110 0.7
105 0.65

Total specific energy (kJ/kg)


100 0.6
Batch temperature (°C)

95 0.55
90
85 0.5
80 0.45
75 0.4
70 0.35
65 0.3
60 0.25
55 0.2
50
45 0.15
40 0.1
35 0.05
0 30 60 90 120 150 180 210 240 0
0 30 60 90 120 150 180 210 240
Time (seconds) Time (seconds)

tion. Mixing cycle information was categorized into five attri- cosity-molecular weight relationships,” Fall 186th Technical
butes associated with distinct events during the process and re- Meeting of the Rubber Division, ACS, Cleveland, OH, 2015.
lated back to polymer architecture. 2. J. Noordermeer, “Ethylene-propylene elastomers,” Encyclo-
pedia of Polymer Science and Technology, 4th ed.; John Wiley &
References Sons, Inc., Vol. 6, pp. 178-196.
1. J.C. Tuberquia, C. Li Pi Shan, T. Clayfield, L. Nguyen, T. 3. H.C. Booij, “Long-chain branching and viscoelasticity of
Kashyap and K. Blackwell, “Long chain branching in EPDM ethylene-propylene-diene elastomers,” Kautschuk Gummi
polymers: An open door to a complete spectrum of Mooney vis- Kunststoffe 1991, 44 (2), pp. 128-130.

Aging of Rubber - Accelerated Heat


Aging Test Results
by R.P. Brown (Author), T. Butler (Contributor), S.W. Hawley (Contributor)

This report details the results of accelerated heat aging studies undertaken on re-mixed
samples of those materials studied for the natural aging study and on the 20 new com-
SRXQGVFKRVHQWRUHSUHVHQWSRO\PHUVQRWDYDLODEOHLQDQGWRUHÀHFWFKDQJHVLQ
FRPSRXQGLQJSUDFWLFH,QDGGLWLRQWRWKRVHSURSHUWLHVVWXGLHGIRUWKHDUWL¿FLDOZHDWKHULQJ
exposures, compression set and dynamic properties were also measured.

Order online at www.rubberworld.com/bookstore

FOLLOW US ON TWITTER @rubberworld 37


Characterizing rubber's resistance against
chip and cut behavior
E\ 5DGHN 6WRþHN 35/ 3RO\PHU 5HVHDUFK /DERUDWRU\ DQG tread compound candidates.
7RPDV%DWD8QLYHUVLW\&]HFK5HSXEOLF:LOOLDP90DUVDQG The CC phenomenon is complex, yet traditional CC test meth-
&KULVWRSKHU*5REHUWVRQ(QGXULFD//&DQG5HLQKROG.LS- ods for the rubber laboratory employ simple, non-instrumented
VFKROO&RHVIHOG*PE+ &R.**HUPDQ\ devices where sample weight loss is the only measurement (refs.
1-4). This article describes a new laboratory instrument for char-
Cutting and chipping of tread rubber is a significant concern for acterization of CC behavior which has several test conditions that
tires that are used in off-road or poor road conditions, where the can be independently controlled. It measures multiple force and
tires are in contact with gravel, rocks and uneven road surfaces. displacement data channels during testing of rubber specimens.
Some examples of cut and chip (CC) damage to tire treads are The testing principle and typical results for model rubber com-
illustrated in figure 1. Due to the usual difficulty in predicting CC pounds that are typical of tire tread applications will be discussed.
resistance of tire treads from laboratory testing of rubber com- In particular, the methodology which can predict actual CC rank-
pounds, it is often necessary to resort to expensive development ings for tires from laboratory testing of tread compounds will be
programs involving iterative tire building and field testing of new highlighted.

Experimental details
Figure 1 - examples of various extents of Polymers used in this study were natural rubber (NR; SMR CV
chip and cut damage to the treads of: TBR/ 60) and high cis butadiene rubber (BR; Buna CB 24 from Ar-
heavy truck tires (a) and (b); OTR/ lanxeo). The reinforcing filler was an N339 grade of carbon black
construction vehicle tire (c); and mud- (CB). All other ingredients were rubber grade chemicals. The
terrain light truck tire (d) rubber formulations are given in table 1.
Rubber compounds were prepared in two mixing stages. For
the first stage, all ingredients except CBS accelerator and sulfur
were mixed for five minutes in an internal mixer (SYD-2L from
Everplast, Taiwan) at 50 rpm with a chamber wall temperature of
(a) 80°C. The CBS and sulfur curatives were added in the second
mixing stage on a two-roll mill at a temperature of 60°C.
(c) Curing properties were determined by a moving die rheometer
(MDR 3000 Basic, MonTech, Germany) according to ASTM
6204 at 160°C. Rubber specimens with an outer diameter of 55
mm and thickness of 13 mm (see geometry shown in figure 2)
were cured in a heated press (LaBEcon 300, Fontijne Presses,
Netherlands) at 160°C according to the curing time t90 + 1 minute
(b) (d) per 1 mm of the thickness (13 minutes total added for specimen
thickness of 13 mm).
Laboratory chip and cut testing was performed on the rubber
specimens using an instrumented chip and cut analyzer (ref. 5)
Figure 2 - photograph of instrumented chip (ICCATM) manufactured by Coesfeld GmbH, Germany (figure
and cut analyzer (ICCA) showing expanded 2), and distributed in the Americas by Endurica LLC, USA. The
view of impacting device and sample (left)
and diagram of rubber sample geometry
with 55 mm outer diameter and 13 mm Table 1 - rubber formulations
thickness (right)
NR/BR 50CB NR/BR 65CB
NR 75 75
BR 25 25
CB (N339) 50 65
55

Zinc oxide 3 3
Ø

Ø Stearic acid 1 1
26
IPPD(a) 1.5 1.5
CBS(b) 2.5 2.5
Sulfur 1.7 1.7
(a) N-isopropyl-N’-phenyl-p-phenylenediamine
(b) N-cyclohexyl-2-benzothiazole sulfonamide

38 RUBBERWORLD.COM ‡ JANUARY 2018


Figure 3 - schematic of ICCA measuring Figure 5 - general graph showing multi-
principle, with: pneumatic actuator (1); two- channel data collection for one impact
axis load cell (2); holder plus impactor (3); loading cycle of ICCA measurement
and round rubber test sample (4)

Ff Normal force

Normal force, fn
Fn Z
Friction force

Force
ai

1 2 3 4 Time of sliding, ts
Time

Figure 4 - geometry of the stainless steel


impactor tool; the width of the impactor is ed rotation speed and striking the sample with a stainless steel
6.35 mm,which strikes the middle of the impactor at a given frequency. The impact is produced using a
13 mm thick rubber sample pneumatic cylinder, where the impact normal force, frequency
and contact (sliding) time with the rubber surface can all be sepa-
rately controlled. A schematic of the impacting device is shown in
9.61

figure 3, the impactor geometry is described in figure 4, and an


6.35 example of the data generated for each impact event is presented
.8 in figure 5. The types of parameter inputs and outputs, along with
R0
their ranges, are summarized in table 2, which emphasizes the
highly instrumented and flexible nature of the testing equipment.
60

One key characterization factor that is evaluated from the


°

16.55

multi-channel data acquisition is the chip and cut propensity, P.


19.05

The parameter P is determined from integrating the fluctuations in


friction force, related to roughness of the damaged surface, over a
.8 R5
Ra 0 number of impact cycles. The P value of tread compounds was
proven to be a very good predictor of actual tire cut and chip field
R1
.5

0.
8 test results for a variety of agricultural tires, truck and bus radial
R2

Ra 0.8
Ra (TBR) tires, and light truck tires. The details cannot be shared due
8 to confidentiality considerations with major tire manufacturers.
0.
Ra The cut and chip behavior as a function of number of impact

ICCA equipment and test-


ing approach will be fur- Table 2 - list of parameters for the instrumented chip and cut analyzer
ther described in the next (ICCA)
section. Samples were
tested at a rotation speed Parameter type
Parameter Range Unit Defined Measured Controlled Calculated
of 150 rpm, normal force ¥ ¥ ¥
Rotation speed, Ȧ 100 to 1,500 rpm
of 125 N, impact frequen- Impact frequency, f 0 to 10 Hz ¥ ¥ ¥
cy of 5 Hz, and sliding Number of impact cycles, n 0 to undefined - ¥ ¥ ¥
time of 30 ms for a varied Time of sliding, ts 20 to permanent ms ¥ ¥ ¥
number of cycles. Normal force, Fn 0 to 500 N  ¥ ¥ ¥
Friction force, Ff 0 to 900 N ¥
Resulting force, Fc Calculated N ¥
Results and discussion Depth of indentation, ai 0 to 20 mm ¥
The principle of measure- Friction distance, af Measured mm ¥
ment for the instrumented Normal energy, En Calculated J ¥
chip and cut analyzer in- Friction energy, Ef Calculated J ¥
Friction coefficient, cf Calculated - ¥
volves rotating the round ¥
Chip and cut propensity, P Calculated N/cycle
rubber sample at a select-

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Figure 6 - topology of the abraded surfaces Figure 7 - effect of number of impact cycles
for the NR/BR 65CB and NR/BR 50CB on P for the NR/BR 65CB and NR/BR 50CB
compounds after testing using loading compounds using conditions described in
conditions described in the text for the the text
indicated number of impact cycles
16
NR/BR 65CB
NR/BR 65CB NR/BR 50CB 14 NR/BR 50CB

Parameter P (N/cycles)
12
1,000 1,000
10
Number of impact cycles, n

2,500 2,500 8
5,000 5,000 6

10,000 4
2
15,000
0
20,000
0 10,000 20,000 30,000 40,000
30,000
Cycles, n
40,000

treads in service.
Abrasion of rubber involves both mechanical fracture and
cycles was compared for two blend compounds: NR/BR 50CB thermal-oxidative effects (aging/degradation) (ref. 6). Consider-
and NR/BR 65CB (see formulations in table 1). The results are ing the latter, impact-induced localized temperature increases of
presented in figures 6 and 7. The slope of the P versus n data the rubber during ICCA testing are of interest, and a study was
shows very distinct values for the two materials. A greater slope conducted to investigate this using a high speed, thermal imaging
is associated with less CC resistance. Inspection of the rubber camera. These preliminary results were shown during the presen-
specimen surfaces and the flat response of P with increasing num- tation of this paper at the 192nd Meeting of the Rubber Division,
ber of cycles for the NR/BR 65CB compound both show that no ACS, in October 2017.
significant chipping of rubber was evident for this material which In addition to cyclic impact, the ICCA can also be used in full
was reinforced with a significantly higher amount of carbon black contact mode as a friction and wear measurement device. This is
compared to the NR/BR 50CB compound, which showed clear an area of ongoing research with this flexible instrument.
CC damage.
The development of cutting patterns on the rubber surfaces, References
and the related chipping away of material that follows, show dis- 1. J. Beatty and B. Miksch, “A laboratory cutting and chipping
tinct characteristics that depend on normal load (not shown here), tester for evaluation of off-the-road and heavy duty tire treads,”
number of impact cycles, and especially the rubber formulation Rubber Chem. Technol. 55, 1,531 (1982).
(figure 6). Along with the P values, such differences in visual 2. C. Nah, B.W. Jo and S. Kaang, “Cut and chip resistance of
damage responses from cyclic impact reveal that the ICCA can NR-BR blend compounds,” J. Appl. Polym. Sci. 68, 1,537 (1998).
effectively distinguish the CC behavior of different rubber com- 3. M. Scherbakov and M.R. Gurvich, “A method of wear charac-
pounds. terization under cut, chip and chunk conditions,” J. Elastom.
Plast. 35, 73 (2003).
Conclusion 4. J.-H. Ma, Y.-X. Wang, L.-Q. Zhang and Y.-P. Wu, “Improvement
The instrumented chip and cut analyzer is a new test device for of cutting and chipping resistance of carbon black-filled styrene
the rubber laboratory that controls and records multiple applied butadiene rubber by addition of nanodispersed clay,” J. Appl.
loads and displacements during cyclic impact to mimic and quan- Polym. Sci. 125, 3,484 (2012).
tify the cut and chip damage experienced by tire tread compounds ((XFKOHU+0LFKDHO0*HKGH2.UDWLQD56WRþHN5
on rough terrain. The surface roughness characteristics of the Kipscholl and J.-M. Bunzel, “Wear of technical rubber materials
rubber specimens, created from the repetitive impacting process, under cyclic impact loading conditions,” Kautsch. Gummi
produce fluctuations in the friction force that are quantified using Kunstst. 69, 22 (2016).
the P parameter, thus allowing evaluation of the CC tendency of 6. A.N. Gent and C.T.R. Pulford, “Mechanisms of rubber abra-
rubber compounds in the laboratory to predict CC behavior of tire sion,” J. Appl. Polym. Sci. 28, 943 (1983).

Coming March 2018


Annual Custom Mixing & Custom Services Issue

40 RUBBERWORLD.COM ‡ JANUARY 2018


Independent Testing Laboratories Directory
time dependent tests including set, Technical service: Compound develop-
The following directory lists creep and stress relaxation, rebound ment, tire and rubber product testing,
independent testing laboratories and resilience and dynamic/thermo- formula reconstruction expertise, sour
serving the rubber industry, including mechanical; destructive tests including gas testing
address, contact person and types crack and cut growth, abrasion, fatigue
of technical service offered by each and heat buildup; durability testing Aspen Research Corp.
laboratory. including heat resistance (static), fluid 8401 Jefferson Highway
resistance and permeability, durability Maple Grove, MN 55369
including ozone resistance, weathering .......................................(651) 842-6100
R.D. Abbott Company, Inc. resistance and brittleness; electrical Fax: (651) 842-6199
16511 Carmenita Rd. properties including dissipation con- Website: www.aspenresearch.com
Cerritos, CA 90703 ........(562) 944-5354 stant, dielectric strength and dielectric Email: answers@aspenresearch.com
Fax: (562) 944-5374 factor; processing including cure rate Nathan Koenig, senior account man-
Website: www.rdabbott.com and extrudability; chemical anaylsis of ager
Email: info@rdabbott.com raw materials and rubber; spectropho- Technical service: Chemical analysis,
Rick Ziebell, vice president of technol- tometry, spectrometry and spectroscopy physical properties, heat and fluid resis-
ogy and innovation management including infrared, ultraviolet and visible, tance, failure analysis, product develop-
Technical service: Liquid additive manu- mass spectrometry, nuclear magnetic ment for elastomers and other polymer-
facturing (LAM) 3D printing; formula- resonance and flame emission/atomic ic materials, physical testing, material
tion development for silicone rubber, absorption; chromatography includ- characterization, product development
organic rubber, and rubber-to-substrate; ing gas and liquid; thermal analysis and failure analysis
material preparation (including lab including thermogravimetric, differential
scaled internal mixing, mill mixing, and thermal analysis and differential scan- Atlas Material Testing Technology
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testing (including testing for curing be- optical and electron 1500 Bishop Ct.
havior, processability, hardness, tensile, (See our ad on page 45) Mount Prospect, IL 60056
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density, die shrink, aging [in air and Alloy Extrusion Co. Fax: (773) 327-5787
fluids], dispersion [for squash molding], 4211 Karg Industrial Pkwy. Website: www.atlas-mts.com
immersion [in test fluids], compression Brimfield, OH 44240 ......(330) 677-4946 Email: atlas.info@ametek.com
set, and dynamic viscosity under shear Fax: (330) 677-4950 Stefani Levine, marketing services
and heat conditions); chemical analysis/ Website: www.alloyextrusion.com Technical service: Complete line of
testing for microscopy with digital field Email: info@alloyextrusion.com environmental and materials test-
analyses, direct film thickness, weight James G. Anthony, president ing instrumentation that can simulate
loss in volatile matter and total solids; Technical service: Complete develop- radiant energy, temperature, salt fog,
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repackaging environment, full line of physical testing
Alttran instruments
Akron Rubber Development 5285 Hudson Dr. Services offered: Natural and accelerat-
Laboratory, Inc. Hudson, OH 44236 ........(330) 650-2223 ed laboratory testing services, technical
2887 Gilchrist Rd. Fax: (330) 650-2215 service, training
Akron, OH 44305 ...........(330) 794-6600 Website: www.alttran.com
(866) 781-ARDL Email: innovation@alttran.com Bodycote plc - Macclesfield
Fax: (330) 794-6610 Carlee McCowin Springwood Court, Springwood Close
Website: www.ardl.com Technical service: Development and Tytherington Business Park
Email: answers@ardl.com testing capabilities include consulting, Macclesfield, Cheshire, United Kingdom
Jerry Leyden, president; Tim Samples, formulation development, lab scale SK10 2XF ............. +44 (0) 1625 505300
CEO; Tom Knowles, vice president mixing and physical property testing. Fax: +44 (0) 1625 505313
chemical services; Jim Drummond, We work with our customers to optimize Website: www.bodycote.com
manager physical testing; Ana Barbur, product performance. We use stan- Email: info@bodycote.com
manager chemical, pharmaceutical and dard test methods or develop our own J. Leidner, manager
microbiological services; Mac Wilborn, to simulate the conditions that rubber Technical service: Testing of mechanical
vice president business development; parts will see in end use applications properties, chemical analysis, com-
John Meser, manager ARDL engineer- (heat resistance, fluid resistance, QUV) pounding, evaluation of environmental
ing; Sean Djuricic, sales development aging, process development, failure
manager Argen Polymer LLC analysis
Technical service: ISO 9001-2008 17645 Telge Rd.
registered, A2LA accredited, indepen- Cypress, TX 77429 ........(330) 687-6388 Bowser-Morner, Inc.
dent testing, development and problem- (281) 719-8400 4518 Taylorsville Rd.
solving laboratory for all facets of the Website: www.argenpolymer.com Dayton, OH 45424 .........(937) 236-8805
rubber, plastics and latex industries. Email: joseph.incavo@argenpolymer. Fax: (937) 237-9947
Capabilities include physical testing com Website: www.bowser-morner.com
of rubber: stress/strain tests including Joseph Incavo, Ph.D., technical director Email: tryan@bowser-morner.com
tensile, tear, hardness and adhesion;

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Independent Testing Laboratories Directory
Tom Ryan, manager Wilson Palokkaran, technical director Electro Chemical Engineering
Technical service: Simulated envi- Technical service: Mold design, product 750 Broad St.
ronmental testing, chemical analysis, development, prototyping, FMEA stud- Emmaus, PA 18049 .......(800) 235-1885
mechanical and physical testing ies production, cost saving programs, (610) 965-9061
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Cameron out processes Website: www.electrochemical.net
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Houston, TX 77027 ........(713) 513-3300 DSET Laboratories Mike Bunner, president
Fax: (713) 513-3456 45601 N. 47th Ave. Technical service: Lab testing services
Website: www.c-a-m.com New River, AZ 85087-7042 including the chemical resistance cell
R. Scott Rowe, president and chief .......................................(623) 465-7356 test, bond and peel strength testing
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senior vice president Website: www.ametek.com Element Los Angeles
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ment testing at elevated pressures and John Wonders, customer/sales support Glendale, CA 91201 ......(818) 247-4106
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and liquid environments, life prediction Technical service: Outdoor (real-time) Website: www.element.com
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Sterling, VA 20165 .........(571) 434-1925 EAG Laboratories Element Materials Technology
Fax: (571) 434-1937 4747 Executive Dr., Ste. 700 662 Cromwell Ave.
Website: www.collaborativetesting.com San Diego, CA 92121 .... (877) 709 9526 St. Paul, MN 55114 ........(651) 645-3601
Email: rubber@cts-interlab.com Website: www.eag.com Fax: (651) 659-7348
Alexandria Moriarty, program analyst Email: info@eag.com Website: www.element.com
Technical service: Inter-laboratory test- Siddhartha C. Kadia, president; Carey Email: info.stpaul@element.com
ing programs; tests available include Lewis, senior vice president Charles Noall, president and CEO; Ari
tensile properties; hardness, Mooney Technical service: Materials analysis, Mckee-Sexton, marketing communica-
viscosity and vulcanization characteris- failure analysis, problem solving, foren- tions manager
tics (ODR and MDR) sic science in rubbers, plastics, non- Technical service: Laboratory testing
metallics and metal (seal) including: physical properties testing,
Dektron Scientific Instruments chemical analysis, environmental simu-
244 E. Third St. Eastern Laboratories, Inc. lation, etc.
Plainfield, NJ 07060.......(908) 226-1777 167 Albany St.
Fax: (908) 226-4973 Springfield, MA 01105 ...(413) 781-2540 Endurica, LLC
Website: www.dektroncorp.com Fax: (413) 733-9631 1219 West Main Cross, Ste. 201
Email: info@dektroncorp.com Website: www.elabs.com Findlay, OH 45840 .........(419) 957-0543
Miguel Vargas Email: elabs@elabs.com Website: www.endurica.com
Technical service: Diversified range of Geraldine Mikes Email: info@endurica.com
standard testing services Technical service: Materials charac- Will Mars
terization for polymers and plastics, Technical service: Elastomer fatigue
Delsen Testing Labs, Inc. extraction studies of medical devices analysis
1024 Grand Central Ave. and various plastic materials, product (See our ad on page 20)
Glendale, CA 91201 ......(818) 247-4106 deformulation, thermal decomposition
Fax: (818) 247-4537 Exova
Website: www.delsen.com Elastomer Research Testing B.V. 3883 E. Eagle Dr.
Email: info@delsen.com P.O. Box 2149, NL 7420 AC, Deventer Anaheim, CA 92807 ......(714) 630-3003
John Moylan, general manager Teugseweg 27, NL7418 AM, Deventer Fax: (714) 630-4443
Technical service: Mechanical, physical, The Netherlands ........... 31 570 624616 Website: www.exova.com
environmental, electrical and flammabil- Fax: 31 570 625702 Email: americas@exova.com
ity testing, polymer analysis Website: www.ertbv.com Mark Kokosinski
Email: info@ertbv.com Technical service: Mechanical, physi-
D.I.S. Enbi Seals Ireland Ltd. Dr. Ir. Kuno Dijkhuis cal, chemical, thermal, environmental
Clonminan Ind. Est. Technical service: Compound devel- exposure, qualification programs and
Portlaoise Co., Laois, Ireland 00 opment, troubleshooting, chemical material identifications
................................... +353 5786 21992 analysis, consultancy, education and
Fax: +353 5786 22322 training, multiclient projects prototyping, Experimental Services, Inc.
Website: www.diseuro.com interlaboratory testing, standard test 894 W. Waterloo Rd.
Email: info@diseuro.com materials Akron, OH 44314

42 RUBBERWORLD.COM ‡ JANUARY 2018


Independent Testing Laboratories Directory
............................ (330) 848-0059, ext. 1 analysis and testing of rubber and all MEI-Charlton, Inc. (MEIC)
Website: www.esilab.com polymeric products, including composi- 7220 N. Lombard St.
Email: kwinkler@esilab.com tions of rubber materials, all additives Portland, OR 97203 .......(503) 228-9663
Karl Winkler, president and thermal testing, ISO/IEC 17025 Fax: (503) 228-4065
Technical service: Independent A2LA certified laboratory Website: www.meic.com
accredited testing laboratory for auto- Email: business@meic.com
motive components, biomedical, railway Hauser GmbH Veronica Strong
and mechanical goods; specializes in Am Hartmayrgut 4-6 Technical service: Engineering and
static, dynamic and fatigue testing of A-4040 Linz, Austria science consulting, testing and forensic
suspension components and rubber- ........................... +43 (0) 732-732305-0 investigation services to rubber, plastic,
to-metal bonded products; material Fax: +43 (0)732-713113 composite, metal and paper based
development fatigue crack growth FCG Website: www.hauser.com products and industries. The services
propagation testing; block cycle and Email: office@hauser.com include, chemical, materials, mechani-
reat time testing of automotive bushings Kurt Ammon, marketing associate/ cal and physical testing, environmental
and mounts; static and dynamic charac- technical services exposure and root cause failure analy-
terization to 1,000 hz Technical service: Materials testing, sis investigations, product development
polymeric analysis and identification, R&D, testing products and materials to
Jesse Garant Metrology Center formulation analysis, EPA 9090, expert ASTM, ANSI, MIL-SPEC, etc., stan-
4610 Stecker St. testimony dards: pipes, o-rings, sheets, mem-
Dearborn, MI 48126 ......(313) 996-5840 branes, tires, utility items, pool slides,
(844) JGARANT Intertek Automotive Research floats, plumbing related, medical, auto
Website: jgarantmc.com 5404 Bandera Rd. related, aviation and railway related,
Email: sales@jgarantmc.com San Antonio, TX 78238 household and educational, paints and
Sara Malik ......................................(210) 523-4605 coatings, electric and electronic instru-
Technical service: This globally rec- Fax: (210) 684-6074 mentation, etc.
ognized part inspection company Website: www.ar.intertek-cb.com
provides NDT and metrology services Email: dean.schoppe@intertek.com Divisions:
using advanced imaging equipment; Dean Schoppe, senior project en- American Product Safety Company
industrial CT, digital radiography, 3D gineer; Randy Gay, senior project (APS)
scanning services allow manufactur- engineer; Brent Ackles, senior project 7220 N. Lombard St.
ers to make qualified decisions at key engineer Portland, OR 97203 .......(503) 228-9665
stages throughout a part’s lifecycle, Technical service: Materials testing Fax: (503) 228-4065
including: pre-production, production, Website: www.meic.com
failure investigation, sorting and reverse In USA, Inc. Email: business@meic.com
engineering 100 Morse St. Raj Patel
Norwood, MA 02062 .....(781) 444-2929 Technical services: Field evaluation
Gasmet Technologies Fax: (781) 444-9229 of electrical instruments, electrcial
Oy, Pulttitie 8 A Website: www.inusacorp.com instrument testing, safety testing, safety
FI-00880 Helsinki, Email: info@inusacorp.com audits. Electrical and electronic product
Finland ..................... +358 9 7590 0400 Adriana Alcorta development support and testing, UL
Website: www.gasmet.com Technical service: Provide ozone test inspections, safety evalaution, red tag
Email: contact@gasmet.fi chambers to materials testing labs that and product labeling
test rubber using ozone
Divisions: MonTech USA
Gasmet Technologies Inc. List AG 1280 S. Williams Dr.
.......................................(866) 685-0050 Berstelstrasse 24 Columbia City, IN 46725
Email: sales@gasmet.com CH-4422 Arisdorf .......................................(800) 552-5115
Switzerland .............. +41 61 815 30 00 Fax: (260) 244-4158
Gasmet Technologies (Asia) Ltd. Fax: +41 61 815 30 00 Website: www.montechusa.com
..................................... +852 3568 7586 Klaus List, owner and chairman of the Email: info@montechusa.com
Email: sales@gasmet.com.hk board Richard Bagan
Technical service: Laboratory system Technical services: Rubber testing
Green Globe Laboratories is used to conduct feasibility studies to equipment, calibration, maintenance,
1860 Arthur Dr. quickly determine how List technology repair
West Chicago, IL 60185 performs in processes such as reac- (See our ad on page 19)
.......................................(630) 231-0680 tions, drying, polymerization, devola-
Fax: (630) 957-4394 tilization and mixing. The system is Musco Engineering Associates
Website: www.therightstuff.com precisely scaled for a smaller footprint, 375 Morgan Ln., Unit 307
Email: rajan@therightstuff.com easy set up and intuitive operation. It West Haven, CT 06516
Rajan Muthiah also allows developers to conduct their .......................................(203) 932-1901
Technical service: Complete chemical research on materials in the concen- Fax: (203) 931-1550
analytical services for compositional trated phase, using little or no solvents. Website: www.muscoengineering.com

FOLLOW US ON TWITTER @rubberworld 43


Independent Testing Laboratories Directory
Email: admin@muscoengineering.com materials and sealings, offer technical Precision Testing Laboratories, LLC
Michael V. Musco seminaries, consulting and have a great 313 Hill Ave.
Technical service: Power distribution, experience in failure analyses of seal- Nashville, TN 37210 ......(615) 254-3401
controls and system integration, plant ings and especially o-rings Fax: (615) 254-3488
and facility design, start-up and com- Website: www.precisiontesting.com
mission assistance, code review and Pelmor Laboratories, Inc. Email: vpsales@precisiontesting.com
evaluation, pre-OSHA inspection 401 Lafayette St. Suzanne Piispanen, COO; John Piis-
Newtown, PA 18940.......(800) 772-6969 panen, director of business develop-
Nevada Automotive Test Center, a di- Fax: (215) 968-3676 ment
vision of Hodges Transportation, Inc. Website: www.pelmor.com
P.O. Box 234 Email: sales@pelmor.com Princeton Polymer Labs
Carson City, NV 89702 James Ross, president 521 Lehigh Ave.
.......................................(775) 629-2000 Technical service: ASTM testing; Union, NJ 07083 ............(908) 687-7033
Fax: (775) 629-2029 formula development, research and ap- Fax: (908) 687-1147
Website: www.natc-ht.com plication for polymers; consultation Website: www.princetonpolymer.com
Email: info@natc-ht.com Email: info@princetonpolymer.com
Henry C. Hodges, Jr. Bill Peltzman & Assoc., Inc. P. Wachtel, president
Technical service: Engineering re- 7157 S. Owens St. Technical service: Compounding, test-
search, testing, development, traction Littleton, CO 80127........(303) 933-0317 ing and synthesis
and winter performance, wear and dura- Fax: (303) 933-7089
bility; thermal profile, ride and handling, Website: www.peltzmanandassociates. Q-Lab Corporation
real time force and moment measure- com 800 Canterbury Rd.
ments, virtual proving ground including Email: bill@peltzmanandassociates.com Cleveland, OH 44145 ....(440) 835-8700
computer modeling, simulation, road Bill Peltzman, president Fax: (440) 835-8738
profiling and validation Technical service: Textile treating, Website: www.q-lab.com
RFL adhesives, process development, Email: info@q-lab.com
NSL Analytical Services, Inc. contamination control and resolution, James Gauntner, sales manager
4450 Cranwood Pkwy. surface energy analysis Technical service: weathering, lightfast-
Cleveland, OH 44128 ....(877) 560-3992 ness and corrosion contact testing
.......................................(216) 438-5200 Phoenix National Laboratories, Inc.
Fax: (216) 438-5050 2837 E. Chambers St. RCMA Americas, Inc.
Website: www.NSLanalytical.com Phoenix, AZ 85040 ........(602) 431-8887 1507 Boettler Rd.
Email: nsl@NSLanalytical.com Fax: (602) 431-8889 Uniontown, OH 44685 ...(330) 896-5900
Larry Somrack, president Website: www.pnltest.com Fax: (330) 896-9943
Technical service: Advanced materials Email: pnl@pnltest.com Website: www.rcma.com
and polymer testing for multiple verticals Alex Zuran III, president Email: rodney.armstrong@rcma.com
including the healthcare, aerospace and Technical service: Testing and inspec- Rodney Armstrong, laboratory manager
opthalmic industries; chemists and en- tion services Technical service: Third party testing
gineers are trained in elemental and or- and compound development for asphalt
ganic chemical analysis, inorganic and Polymer Diagnostics Inc. roofing and paving systems, adhesives,
organic analysis, SEM analysis w/EDS, 33587 Walker Rd. coatings, natural latex, rubber and
thermal analysis; clients appreciate the Avon Lake, OH 44012....(800) 438-2335 plastics
fast turnaround time and the technology Fax: (440) 930-1644
we continually invest in to produce ac- Website: www.polymerdiagnostics.com Rubber Consultants
curate, reliable results; nearly 70 years, Email: info@polymerdiagnostics.com Brickendonbury
we have provided the highest standards Thomas Hughes, senior vice president Hertford, U.K. SG13 8NL
of product quality from design to launch Technical service: Polymers/rubber .............................. + 44 (0)1992 554657
by providing trusted materials testing Fax: +44 (0)1992 504248
results; learn how NSL can work with Polymer Solutions Incorporated Website: www.rubberconsultants.com
you to solve your product performance 135 Technology Dr. Email: info@rubberconsultants.com
challenges Christiansburg, VA 24073 David Cawthra and Gail Reader, market
.......................................(877) 961-4341 development and promotion
O-Ring Prüflabor Richter GmbH Website: www.polymersolutions.com Technical service: Analytical, biotech-
Kleinbottwarer Str. 1 Email: george.cheynet@polymersolu- nology, bioinformatics, rubber in engi-
D-71723 Großbottwar tions.com neering, prototype design and manu-
Germany ................... +49 7148 16602-0 George Cheynet facturing, rubber technology, contract
Fax: +49 7148 16602-299 Technical service: Polymer solutions research, physical testing, tire testing
Website: www.o-ring-prueflabor.de/en/ is an independent testing lab that is
home CGMP compliant, FDA registered, DEA Rutherford Research
Email: info@o-ring-prueflabor.de licensed and ISO 17025 certified. We 89 Prospect Place
Bernhard Richter, managing director offer chemical analysis, physical testing, Rutherford, NJ 07070 ....(201) 933-2711
Technical service: We test rubber consultation and R&D services Website: www.rutherford-research.ca

44 RUBBERWORLD.COM ‡ JANUARY 2018


Independent Testing Laboratories Directory
Email: calgary@rutherford-research.ca wheel, cut-growth, rolling resistance, including chemical analysis, fungus
William Rutherford, owner high speed; tire strength, bead unseat- resistance, toxicity (NSF 61)
Technical service: Research and de- ing, load/deflection, footprints, profiles,
velopment, design, testing and analy- hydrostatic burst, sections, cord pulls; UL Verification Services
sis, consulting, electrical and physical complete in-house photographic/video; 1559 King St.
measurements, failure analysis, testing forensic testing, accident reconstruc- Enfield, CT 06082 ..........(860) 835-2085
equipment, conductive rubber and tion; failure analysis, consultation; Fax: (860) 749-7533
expert testimony non-destructive testing including Website: www.ul.com
x-ray, shearography; designing and Email: paul.o.moore@ul.com
SGS U.S. Testing Company Inc. manufacturing of tire and wheel testing Paul Moore
291 Fairfield Ave. machinery, tire sectioning equipment, Technical service: Quality assurance
Fairfield, NJ 07004.........(973) 575-5252 computerized controls; test air springs, and testing services; materials selec-
Fax: (973) 575-7175 marshmallow springs, engine mounts, tion/evaluation
Website: www.us.sgs.com/cts tire valves, tire repair materials, seal-
Email: marketing.cts.us@sgs.com ants, filling materials VTEC Laboratories Inc.
Chris Kirk, CEO 212 Manida St.
Technical service: Mechanical, electri- Truesdail Laboratories, Inc. Bronx, NY 10474 ...........(718) 542-8248
cal, thermal and flammability properties 3337 Michelson Dr. Fax: (718) 542-8759
testing of all kinds of elastomers, plas- Irvine, CA 92612 ............(714) 730-6239 Website: www.vteclabs.com
tics, metal, wood and stone, per ASTM, Fax: (714) 730-6462 Email: neil@vteclabs.com
ANSI, federal and military specifications Website: www.truesdail.com Neil Schultz
Email: nhester@truesdail.com Technical service: Commercial testing
Shrader Analytical & Consulting Norman Hester, chief science officer and research, testing: physical, struc-
Laboratories Inc. Technical service: Provide a wide tural, flammability, combustion, toxicity,
440 Burroughs St. variety of materials testing properties, weathering electrical, mechanical
Ste. 340
Detroit, MI 48202 ...........(313) 894-4440
Fax: (313) 894-4489
Website: www.shraderlabs.com
Email: sales@shraderlabs.com
Philip Shrader
Technical service: Chemical analysis by
mass spectrometry, gas chromatogra- Independent Testing, Development and Consulting
phy/mass spectrometry, liquid chroma-
tography/mass spectrometry
From the Polymer Experts You Know
and Have Trusted Since 1962
Smithers Rapra
425 W. Market St.
Akron, OH 44303 ............(330) 762-7441
Fax: (330) 762-7447
Rubber. Plastic. Latex.
Website: www.smithersrapra.com
Nat Leonard, president
Technical service: Full service in rubber Rubber. Plastic. Latex.
from testing to consulting; compound de- :KHWKHU\RXQHHGDVLQJOHWHVWPHWKRGRUDIXOOSURJUDPRIWHVWVDQG
velopment, analytical, physical/mechani- FRQVXOWDWLRQWRSHUIHFW\RXUSURGXFWZHèUHKHUHWRKHOSDQGFDQSURYLGH\RX
cal product analysis, failure analysis and ZLWKDTXRWHWKDWèVFXVWRPL]HGWR\RXUPDWHULDOWHVWLQJQHHGV
process development
(See our ad on page 77) ï&KHPLFDO$QDO\VLVDQG7HVWLQJ ï$GKHVLYHV&RDWLQJV7HVWLQJ
ï3K\VLFDO0HFKDQLFDO7HVWLQJ ï0LFURVFRS\
Standards Testing Labs ï&RPSRXQG'HYHORSPHQW ï)DLOXUH$QDO\VLV
1845 Harsh Ave., S.E. ï)RUPXOD5HFRQVWUXFWLRQ ï0L[LQJDQG0ROGLQJ
Massillon, OH 44648 .....(330) 833-8548 ï'\QDPLF7HVWLQJDQG(QJLQHHULQJ6HUYLFHV ï1RQ6WDQGDUG7HVW'HYHORSPHQW
.......................................(800) 833-8547 ï3KDUPDFHXWLFDODQG0LFURELRORJLFDO6HUYLFHV ï&RQVXOWLQJ
Fax: (330) 833-7902
Website: www.stllabs.com
Email: sales@stllabs.com Contact Us Today!
Cheryl Schnuth, vp marketing/technical
sales
Technical service: Complete tire testing, 9LVLWZZZDUGOFRPIRURXUZLGHUDQJHRISUREOHPVROYLQJFDSDELOLWLHV
Akron Rubber Development Laboratory, Inc.
including resiliometer, endurance, tread Toll Free (866) 781-ARDL Worldwide (330) 794-6600
separation, steer/camber angle, cleated answers@ardl.com

FOLLOW US ON TWITTER @rubberworld 45


Independent Testing Laboratories Directory
The following grid lists the types of Physical testing of rubber
testing offered by independent testing
laboratories. Tests for physical testing Stress/strain Time-dependent Destructive Durability
tests tests tests
of rubber include stress/strain tests;
time-dependent tests; destructive
tests; durability; electrical properties;
and processing. Tests for chemical
analysis of raw materials and rubber

Dynamic/thermomechanical
Creep and stress relaxation
are broken down into spectrophoto-

Rebound and resilience

Heat resistance (static)


Crack and cut growth
metry, spectrometry and spectrosco-
py; chromatography; thermal analysis;

Fluid resistance
Heat build-up

Permeability
and microscopy. Each of these subdi-

Hardness

Adhesion

Abrasion
visions is further broken down into the

Fatigue
Tensile

specific type of tests.


Tear

Set
R.D. Abbott Company, Inc. s s s s s s s s s s s s
Akron Rubber Development Lab, Inc. s s s s s s s
Alloy Extrusion Co. s s
Alttran s s s s s s s s s
Aspen Research Corp. s s s s s s s s
Atlas Material Testing Technology LLC

Bodycote plc - Macclesfield s s s s s s s s


Bowser-Morner, Inc. s s s s s s s
Cameron s s s s s s s s
Collaborative Testing Services, Inc. s s
Dektron Scientific Instruments s s s s s s s s s s s s s s
Delsen Testing Labs, Inc. s s s s s s s
D.I.S. Enbi Seals Ireland Ltd.

DSET Laboratories
EAG Labortories s s s s s s s s s
Eastern Laboratories, Inc. s s s s s s s s
Elastomer Research Testing B.V. s s s s s s s s s s s
Element Los Angeles s s
Element Materials Technology s s s s s s s s
Endurica, LLC s s s s s s
Experimental Services, Inc. s s s s s s s s s s
Green Globe Laboratories

Hauser GmbH s s s s s s s
Intertek Automotive Research s s s s s s s
In USA, Inc.

MEI-Charlton, Inc. s s s s s s s s s s s
MonTech

46 RUBBERWORLD.COM ‡ JANUARY 2018


Independent Testing Laboratories Directory
Physical testing of rubber Chemical analysis of raw materials and rubber

Durability Electrical Process- Spectrophotometry, spec- Chroma- Thermal Micro-


properties ing trometry and spectroscopy tography analysis scopy

Nuclear magnetic resonance

Differential thermal anaylsis


Flame emission/atomic
Weathering resistance

Ultraviolet and visible

Differential scanning
Dissipation constant

Mass spectrometry

Thermogravimetric
Dielectric strength
Ozone resistance

Dielectric factor

Extrudability

calorimetry
absorption
Brittleness

Cure rate

Electron
Infrared

Optical
Liquid
Gas
s s
s s s s s s s s s s s s s s s s s s s s
s s
s s s s s
s s s s s s s s s s s s s s s s s s
s s s

s s
s
s

s s s s s s s s
s s
s
s

s s s s s s

s s s s s
s

s s s s s s s
s s s s s s s s s s s
s s s s s s
s s s

s s s

FOLLOW US ON TWITTER @rubberworld 47


Independent Testing Laboratories Directory
The following grid lists the types of Physical testing of rubber
testing offered by independent testing
laboratories. Tests for physical testing Stress/strain Time-dependent Destructive Durability
tests tests tests
of rubber include stress/strain tests;
time-dependent tests; destructive
tests; durability; electrical properties;
and processing. Tests for chemical
analysis of raw materials and rubber

Dynamic/thermomechanical
Creep and stress relaxation
are broken down into spectrophoto-

Rebound and resilience

Heat resistance (static)


Crack and cut growth
metry, spectrometry and spectrosco-
py; chromatography; thermal analysis;

Fluid resistance
Heat build-up

Permeability
and microscopy. Each of these subdi-

Hardness

Adhesion

Abrasion
visions is further broken down into the

Fatigue
Tensile

specific type of tests.


Tear

Set
NSL Analytical Services s s s s s s s s s s s
O-Ring Prüflabor Richter GmbH s s s s s s s s s
Bill Peltzman and Assoc., Inc.

Phoenix National Laboratories, Inc. s s s s s s s s


Polymer Diagnostics Inc. s s s s s s
Polymer Solutions Inc. s s s
Precision Testing Laboratories, Inc. s s s s s s s s s s
Princeton Polymer Labs s s s s s
RCMA Americas, Inc. - Synthetic Division s s s s s s s s s
Rubber Consultants s s s s s s s s s s s s s s s
Rutherford Research

SGS U.S. Testing Company, Inc. s s s s s s s s s s s


Shrader Analytical and Consulting Labs s s s s s s s s s s s s
Smithers Rapra s s s s s s s s s s s s s s s
Standards Testing Labs s s s s s s s s s
Truesdail Laboratories, Inc.

UL Verification Services s s s s s s s s
VTEC Laboratories Inc. s s s s s s s s s s s s s s s
Western Technologies Inc. s s s s s

Extrusion Dies for


Plastics and
Rubber
Adhesion and
Adhesives
Technology
Indispe
Author: Michaeli, W.
Copyright: 2003
ISBN: 9781569903490
Author: Pocius, A.
Copyright: 2012
ISBN: 978-1-56990-511-1
Referenc
www.rubberworld
Hardcover: 362 pages Hardcover: 370 pages

48 RUBBERWORLD.COM ‡ JANUARY 2018


Independent Testing Laboratories Directory
Physical testing of rubber Chemical analysis of raw materials and rubber

Durability Electrical prop- Process- Spectrophotometry, spec- Chroma- Thermal Micro-


erties ing trometry and spectroscopy tography analysis scopy

Nuclear magnetic resonance

Differential thermal anaylsis


Flame emission/atomic
Weathering resistance

Ultraviolet and visible

Differential scanning
Dissipation constant

Mass spectrometry

Thermogravimetric
Dielectric strength
Ozone resistance

Dielectric factor

Extrudability

calorimetry
absorption
Brittleness

Cure rate

Electron
Infrared

Optical
Liquid
Gas
s s s s s s s s s s
s s s s s s s s s s
s s s s s s s s s s s
s s

s
s
s s s s
s s s s
s
s s

s s s s s s s s s s s s
s s s s s s s s s s s s s s s s s
s s s
s s s s s s s
s s s s s s s s s s
s s s s s s s s s s s s s s s s

ensable Understanding
Thermoplastic
Elastomers
Mixing of Rubber
Compounds
Author: Limper, A. Copy-

ce Tools
d.com/bookstore
Author: Holden, G.
Copyright: 2000 ISBN:
9781569902899
Softcover: 110 pages
right: 2012
ISBN: 9781569904589
Hardcover: 239 pages

FOLLOW US ON TWITTER @rubberworld 49


Instrumentation, Test
Test Equipment
Equipment Suppliers
Suppliers
Akron Special Machinery, Inc. Ametek Measurement & Calibration
The following directory lists suppliers of 2740 Cory Ave. Technologies Division
instrumentation and test equipment to Akron, 44314.................... (330) 753-1077 8600 Somerset Dr.
the rubber industry, with address, con- Fax: (330) 753-7308 Largo, FL 33773...................(800) 527-9999
tact person, types of instrumentation, Website: www.polinggroup.com Fax: (727) 539-6882
test equipment and services offered. Email: sales@polinggroup.com Website: www.chatillon.com
David L. Poling, president Email: chatillon.fl-lar@ametek.com
Instrumentation: Instruments for uniformi- Dave Hermance, vice president
R.D. Abbott Company, Inc. ty testing, runout testing, sidewall testing Instrumentation: Tensile testers
16511 Carmenita Rd. and grinding, tire testing Services offered: Technical services, train-
Cerritos, CA 90703 ..............(562) 944-5354 ing, software programs
Fax: (562) 944-5374 Alpha Technologies
Website: www.rdabbott.com 6279 Hudson Crossing Pkwy, #200 Ametek U.S. Gauge
Email: info@rdabbott.com Hudson, OH 44236 ..........(330) 745-1641 205 Keith Valley Rd.
Rick Ziebell, vice president of technology Fax: (330) 848-7326 Horsham, PA 19044 ............(215) 293-4100
and innovation management Website: www.alpha-technologies.com Fax: (215) 323-9450
Instrumentation: Computers, controllers, Email: alphasales@alpha-technologies. Website: www.ametekusg.com/products/
curemeters/rheometers, densimeters, com gauges.cfm
durometers, laboratory equipment (miscel- Melissa Kollar, global marketing manager Email: usg@ametek.com
laneous), measuring equipment, monitors, Instrumentation: Design and manufactur- Instrumentation: Process measurement
physical testing equipment, presses, soft- ing of instruments and software. Advance technology, pneumatic controllers, elec-
ware systems, testers and testing equip- precision rubber and elastomeric materi- tronic process transmitters, calibration
ment, density testers, hardness testers, als analysis for production optimization equipment
plasticity testers, processability testers, and product compliance solutions. Alpha Services offered: Technical service, training
specific gravity testers, viscometers Technologies, a Roper Technologies
company, introduced the world’s first Leverett A. Anderson Co.
Acrolab Ltd.
rubber rheometer in 1964 and since has 1245 S. Cleveland-Massillon Rd., Ste. 2
7475 Tranby Ave.
been dedicated to working closely with Copley, OH 44321 ...............(330) 670-1363
Windsor, Ontario, Canada N8S 2B7
clients and industries to improve and Fax: (330) 670-9450
...............................................(519) 944-5900
enable performance, value and safety to Website: www.leverettanderson.com
Fax: (800) 465-9674
consumers. ISO 9001-registered and ISO Email: sales@leverettanderson.com
Website: www.acrolab.com
17025-accredited, Alpha Technologies’ William S. Cole, president
Email: jhodgins@acrolab.com
instruments measure the dynamic, physi- Instrumentation: Materials testing equip-
John Hodgins, chief executive officer
cal and processability characteristics of ment for rubber and plastics
Instrumentation: Heat transfer technology
rubber and polymers Services offered: Sales, service including
Acu-Gage Systems calibration design and fabrication or special
12 Park Ave. Altman Manufacturing Co. testing equipment
Hudson, NH 03051 ..............(603) 622-2481 1990 Ohio St.
(800) 422-2283 Lisle, IL 60532 .................. (630) 963-0031 Applied Test Systems, Inc.
Fax: (603) 626-1277 Fax: (630) 963-0089 154 East Brook Ln.
Website: www.acu-gage.com Website: www.altmanmfg.com Butler, PA 16002 ..................(724) 283-1212
Email: info@acu-gage.com Email: brian@altmanmfg.com (800) 441-0215
John A. Kane, president Brian Altman Fax: (724) 283-6570
Instrumentation: Acu-Gage I single axis Services offered: Testing molded parts Website: www.atspa.com
linear measuring machine in sizes ranging for cracking, missing rubber, pressure Email: sales@atspa.com
from 12” to 120”; Acu-Gage II, two axis testing, metal insert detection, size and Greg Osborne, sales manager
coordinate measuring machine with base air flow Instrumentation: Creep/stress rupture test-
sizes of 12” x 12” to 48” x 96”, Z-axis also ing machines, universal testing machines,
available Ames Inc., B.C. pressure test systems, fatigue testers,
1644 Concord St furnaces and ovens for testing and process-
Admet Inc. Framingham, MA 01701 ing, elastomeric extensometers, special test
51 Morgan Dr. .......................................... (781) 893-0095 equipment
Norwood, MA 02062............(781) 769-0850 (800) 438-4249 Services offered: Technical service, calibra-
...............................................(800) 667-3220 Fax: (781) 647-3356 tion, repair
Fax: (781) 769-0884 Website: www.bcames.com
Website: www.admet.com Email: info@bcames.com Aqua Measure Instrument Company
Email: sales@admet.com Francis Gardner, president 9567 Arrow Route, Ste. E
Scott Carroll Instrumentation: For thickness measure- Rancho Cucamonga, CA 97130
Instrumentation: Elecromechanical and hy- ment - dial and digital bench compara- ...............................................(800) 966-4788
draulic universal testing frames for tension, tors, handheld micrometers, non-contact (909) 941-7776
compression and torsion testing; digital AccuFlow air gaging for in-process and Fax: (909) 941-6444
indicating systems for tension, compression bench; electronic read-out available. Website: www.aquameasure.com
and torsion testing Services offered: Application engineering Email: sales@aquameasure.com

50 RUBBERWORLD.COM ‡ JANUARY 2018


Instrumentation, Test Equipment Suppliers
Steven Brunasso, CEO Atlas Material Testing Technology, LLC Dayton, OH 45424 ...............(937) 233-9935
Instrumentation: Analysis equipment, gaug- 1500 Bishop Ct. Fax: (937) 233-7284
es, laboratory equipment (miscellaneous), Mount Prospect, IL 60056 Website: www.ndc.com/betalasermike
measuring equipment, meters and moisture ...............................................(773) 327-4520 Email: sales@betalasermike.com
meters, testers and testing equipment Fax: (773) 327-5787 Jay Luis, marketing communications
Website: www.atlas-mts.com manager
Armstrong International Email: atlas.info@ametek.com Instrumentation: Integrated process control
816 Maple St. Stefani Levine, marketing services systems using a wide range of non-contact
Three Rivers, MI 49093 .......(269) 279-3603 Instrumentation: Complete line of environ- measurement technologies designed to
Fax: (269) 278-6555 mental and materials testing instrumen- improve product quality and reduce manu-
Website: www.armstronginternational.com tation that can simulate radiant energy, facturing costs. These systems provide both
Email: marketing@armstronginternational. temperature, salt fog, moisture, other in-process dimensional monitoring, control
com components of a natural environment, full and sample inspection of rubber and plastic
Denise DeVries, North American marketing line of physical testing instruments. round, cylindrical and tubular products. Our
manager Services offered: Technical service, training systems offer a number of advantages over
Instrumentation: Steam, air and hot water contact and other non-contact gauging sys-
products Automation Products, Inc. - Dynatrol tems. Our technologies and brands include
Services offered: Energy auditing that Division InControl for process control, AccuScan
identifies areas of utility system inefficiency, 3030 Maxroy St. for laser scanning diameter measurement,
engineering design for utility project im- Houston, TX 77008-6294 UltraScan for ultrasonic wall thickness and
provements, complete utility operations and ...............................................(713) 869-0361 concentricity measurement, BenchMike for
maintenance responsibilities, turnkey instal- (800) 231-2062 off-line sample inspection and LaserSpeed
Fax: (713) 869-7332 for non-contact length and speed measure-
lation, project management, financing for
Website: www.dynatrolusa.com ment.
utility upgrade projects, measurement and
Email: sales@dynatrolusa.com Services offered: Dimensional monitoring,
verification of energy projects, complete
Instrumentation: Equipment which mea- diameter measurement, thickness mea-
steam system training
sures and controls density, specific gravity, surement, length and speed measurement
percent solids, percent concentration,
ASM-Hasbach viscosity and level detection C. W. Brabender Instruments
2740 Cory Ave. 50 East Wesley St.
Akron, OH 44314 .................(330) 753-1077 Basler Vision South Hackensack, NJ 07606
(614) 505-0289 855 Springdale Dr., Ste. 203 ...............................................(201) 343-8425
Fax: (330) 753-7308 Exton, PA 19341 ..................(610) 280-0171 Fax: (201) 343-0608
Website: www.polinggroup.com Fax: (610) 280-7608 Website: www.cwbrabender.com
Email: sales@polinggroup.com Website: www.baslerweb.com Email: cwbi@cwbrabender.com
David L. Poling, president; Alexander Has- Email: info@baslerweb.com Richard F. Thoma, president
bach, vice president Instrumentation: Inspection systems, Instrumentation: Laboratory testing equip-
Instrumentation: Analysis equipment, laboratory equipment (miscellaneous), ment for rubber testing, including process-
inspection systems, laboratory equipment measuring equipment ability studies, dispersion, mixing, cure and
(miscellaneous), measuring equipment, density for R&D and QC
testers and testing equipment, burst testers, Benz Materials Testing Instruments Services offered: Testing laboratory
fatigue testers, high speed uniformity tes- 73 Maplehurst Ave.
ters, impact testers, nondestructive testers, Providence, RI 02908 ..........(401) 331-5650 Brandywine Technology Sales
rolling resistance testers, tire testers, tire Fax: (401) 331-5685 1379 Dilworthtown Crossing #139
endurance testers and universal testers Website: www.benztesters.com West Chester, PA 19382
Services offered: Durability testing, pas- Email: engineering@benztesters.com ...............................................(610) 761-8918
senger and truck tires, equipment design, Ted Benz, president Email: mjt@brandywineonline.com
nondestructive testing, research and Instrumentation: TR testers, abrasion, test Michael J. Trojan, president
development tube aging ovens, burst testers, plasto- Instrumentation: Densimeters, inspection
meters, rheometers, durometers, visco- systems, measuring equipment, ovens,
Asylum Research, an Oxford meters, tensile testers, test dies, test molds, x-ray inspection machines
Instruments Company laboratory ovens, hardness, flexing, fatigue,
6310 Hollister Ave. impact, lab presses, specific gravity testers, Brookhaven Instruments Corporation
Santa Barbara, CA 93117 test tubes, glassware, test fixtures, grips 750 Blue Point Rd.
...............................................(805) 696-6466 Services offered: Technical service, training, Holtsville, NY 11742 ............(631) 758-3200
(888) 472-2795 software programs, repair and rebuilding Fax: (631) 758-3255
Fax: (805) 696-6444 testing instruments and lab information Website: www.brookhaveninstruments.com
Website: www.oxford-instruments.com/AFM management systems Email: info@brookhaveninstruments.com
Email: afm.info@oxinst.com (See our ads on pages 81 and 86) Joe Pozzolano, general manager
Ben Ohler, director of marketing Instrumentation: Particle size measurement
Instrumentation: Atomic force microscopes, Beta LaserMike Products utilizing laser light scattering, disc centrifu-
scanning probe microscopes, AFM probes/ (An NDC Technologies Brand) gation; for zeta potential analysis by particle
cantilevers, nanomechanical properties 8001 Technology Blvd. electrophoresis; applications include pig-

FOLLOW US ON TWITTER @rubberworld 51


Instrumentation, Test Equipment Suppliers
ments, carbon blacks Fax: (913) 492-1483 CPM Wolverine Proctor, LLC
Services offered: Technical support Website: www.instruments.com 251 Gibraltar Rd.
Email: info@instruments.com Horsham, PA 19044 ........... (215) 443-5200
Carver Inc. Chris Herring, president Fax: (215) 443-5206
1569 Morris St. Instrumentation: Temperature instrumenta- Website: www.cpmwolverineproctor.com
Wabash, IN 46992-0544 tion (alarms, monitors, controllers, etc.) Email: sales@cpmwolverineproctor.com
...............................................(260) 563-7577 Services offered: Repairing company P. Zagorzycki, technical director; C.
Fax: (260) 563-7265 equipment Schnitzer, advertising manager; F.C. Keill,
Website: www.carverpress.com lab manager; B. Thomson, sales manager
Email: carverpress@corpemail.com Corporate Consulting, Service & Instrumentation: Dryers and extruders
David Singer, sales and marketing man- Instruments, Inc.
ager University Park Creative Coatings Corporation
Instrumentation: Laboratory equipment and Akron, OH 44304-1909 .......(330) 376-3600 One Chestnut St., Ste. 4Z (03060)
dies (800) 742-8535 Nashua, NH 03061-1165
Fax: (330) 376-8500 ...............................................(603) 791-0137
CDS Analytical, Inc. Website: www.ccsi-inc.com Fax: (603) 791-0209
465 Limestone Rd. Email: sales.department@ccsi-inc.com Email: flocking@aol.com
Oxford, PA 19363-0277 David Warner, president; Michael Kent Robert P. Borowski, president
...............................................(610) 932-3636 Warner, executive vice president Instrumentation: Dryers, grinders, labora-
(800) 541-6593 Instrumentation: ISO/IEC 17025 calibra- tory equipment (miscellaneous), ovens, tes-
Fax: (610) 932-4158 tion and certifications, durometer hard- ters and testing equipment, testers abrasion
Website: www.cdsanalytical.com ness testers (Shore, Wallace, PTC, Rex, Services offered: Equipment design,
Gary Deger, director of sales and marketing and others), durometer operating stands, general cutting, mechanical cutting, drying
Instrumentation: Analysis equipment, durometer test blocks, Mooney viscom- of rubber, extruding and vulcanizing extru-
environmental chambers, physical testing eters, moving die rheometers, oscillating sions, fabricating, grinding, winding, mold
equipment, temperature measuring de- disk rheometers, tensile/compression making, splicing, 3M tape, flocking, laminat-
vices, testers and testing equipment testers, compression set fixtures, ASTM/ ing, special services
Services offered: Manufacturing ISO specimen cutting dies and specimen
molds, custom rubber molds, laboratory Custom Scientific Instruments, Inc.
Cober, Inc. bale cutters, rubber cutters/trimmers, Atom 1125 Conroy Place
30 Moffit St. swing arm clicker presses, ElasTek ‘mini Forks Township (Easton), PA 18040
Stratford, CT 06615 .............(203) 855-8755 clicker’ presses, ElasTek DeMattia flex ...............................................(610) 923-6500
Fax: (203) 855-7511 testers, ElasTek fully automatic density/ Fax: (610) 923-6543
Website: www.cober.com specific gravity testers, rubber buffers, Website: www.csi-instruments.com
Email: sales@cober.com rubber grinders, environmental chambers, Email: info@csi-instruments.com
Matthew Krieger laboratory ovens, heated mold presses, Segundo Vargas, vice president engineer-
Instrumentation: Microwave receptivity test- Taber abrasion testers, BarCol hardness ing
ing, microwave curing ovens testers, Ross flex testers, Scott flex testers,
Services offered: Technical service for Taber stiffness testers, Mullen burst testers, Davis Instruments
microwave technology ElasTek ASTM D865 aging block ovens, 625 East Bunker Ct.
(See our ad on page 86) OREC ozone chambers, OREC ozone Vernon Hills, IL 60061-1844
monitors, low temperature retraction (TR ...............................................(847) 327-2000
Commercial Timesharing, Inc. (CTI) test) and brittleness point testers, ASTM (800) 358-5525
2740 Cory Ave. D2632 vertical rebound testers (ElasTek re- Fax: (800) 433-9971
Akron, OH 44314 .................(330) 644-3059 siliometers), ElasTek Williams’ parallel plate Website: www.davis.com
Fax: (330) 644-8110 plastometers, Brinell, Vickers and Rockwell Email: info@davis.com
Website: www.comtime.com hardness testers Instrumentation: Hardness testers and
Email: sales@comtime.com Services offered: ISO/IEC 17025 calibration durometers
Ronald Symens, president and certifications (A2LA) service and repair
Instrumentation: Analysis equipment, of: durometer hardness testers, Mooney Davis-Standard, LLC
computers, controllers, inspection sys- viscometers, all rheometers, tensile testers, 1 Extrusion Dr.
tems, physical testing equipment, software thickness gauges, micrometers, calipers, Pawcatuck, CT 06379 .........(860) 599-1010
systems, testers and testing equipment, tire cutting dies, molds, resilience testers, Fax: (860) 599-6258
laser measurement systems
compression testers, plastometers, scales Website: www.davis-standard.com
Services offered: Computer services, cost
and balances, abraders, mass and weights, Email: info@davis-standard.com
control, reduction, and studies, data ware-
gauge blocks, Brookfield viscometers, Robert Preston, CEO
housing, business intelligence, engineers,
dimensional measurement tools, tachom- Instrumentation: Laboratory equipment
physical testing, plant management, pro-
eters, laboratory ovens (E145 and D7969),
duction control, test method development
air flow, thermocouples and thermometers, Dektron Scientific Instruments
ozone chambers, ozone monitors (NIST 244 East Third St.
Computer Instruments Inc.
direct traceability), and time measurement Plainfield, NJ 07060.............(908) 226-1777
10591 Widmer Rd.
instruments Fax: (908) 226-4973
Lenexa, KS 66215 ...............(888) 451-0851
(913) 492-1888 (See our ad on page 83) Website: www.dektroncorp.com

52 RUBBERWORLD.COM ‡ JANUARY 2018


Instrumentation, Test Equipment Suppliers
Email: info@dektroncorp.com Taiwan ..................................886-4-8761635 Sal Negro, manufacturing executive
Miguel Vargas, manager Fax: 886 4-8761637 Instrumentation: Laboratory equipment
Instrumentation: Test equipment for materi- Website: www.ektrontek.com
als Email: ektronco@ms48.hinet.net Emerson Apparatus, Inc.
Services offered: Applications assistance Zhang Yaodong, president 59 Sanford Dr.
for testing of materials; service and repair of Instrumentation: Flexing machines, ozone Gorham, ME 04038 .............(800) 445-1055
test equipment testers, rheometers, tensile testers, tire Fax: (207) 856-1117
testers, viscometers, vibration simulator Website: www.emersonapparatus.com
Despatch Industries Email: sales@emersonapparatus.com
8860 207th St. Elastocon AB Connie Upson, vice president, sales and
Minneapolis, MN 55044 Tvinnargatan 25 marketing
...............................................(952) 469-5424 Bramhult, Sweden .........0046 33 - 22 56 30 Instrumentation: Rubber buffing machines,
(800) 726-0110 Website: elastocon.com foam endurance tester, ASTM 1055 load
Fax: 952 469-4513 Email: info@elastocon.se deflection tester
Website: www.despatch.com Göran Spetz, marketing and sales manager Services offered: Technical service, training
Email: info@despatch.com Instrumentation: Instruments for testing
Roger Dullinger, marketing with precision, stress relaxation systems, Emery Winslow Scale Company
Instrumentation: Environmental test cham- aging ovens, specimen preparation, low 73 Cogwheel Ln.
bers, curing, testing ovens temperature test, LTCS, freezers, automatic Seymour, CT 06483-3919
Services offered: Technical service, training Gehman, TR and brittleness tester, wind- ...............................................(203) 881-9333
screen fogging, electrical tests, computer- Fax: (203) 881-9477
Dewes Gumbs Die & Presses ized testing, automatic creep and relaxation Website: www.emerywinslow.com
38-33 24th St. test, hot set test, software and more Email: homeoffice@emerywinslow.com
Long Island City, NY 11101 Services offered: Testing services, lifetime William K. Fischer, president; Rudi P.
...............................................(718) 784-9756 estimations, accredited calibration, semi- Baisch, vice president, sales and marketing;
Fax: (718) 784-9755 nars and educations, both in our facilities David M. Young, sales manager Instru-
Website: www.dewes-gumbs.com and at your site mentation: Load cells, scales and weighing
Email: info@dewes-gumbs.com (See our ad on page 82) systems
Robert Salerni, president
Instrumentation: Specimen cutting dies, Electronic Development Labs, Inc. Endurica, LLC
dies for ASTM, DIN, JAP, TAPPY and test- 244 Oakland Dr. 1219 West Main Cross, Ste. 201
ing equipment Danville, VA 24540 ...............(434) 799-0807 Findlay, OH 45840 ...............(419) 957-0543
Services offered: Reconditioning and recali- Fax: (434) 799-0847 Website: www.endurica.com
bration of test dies and molds Website: www.edl-inc.com Email: info@endurica.com
Email: sales@edl-inc.com William Mars, president
Dillon Danielle Smith Instrumentation: Intrinsic strength analyser,
1000 Armstrong Dr. Instrumentation: Pyrometers, calibrators, tear and fatigue analyzer and chip and cut
Fairmont, MN 56031............(507) 238-8796 sensors analyzer; Endurica Solutions in your own
Fax: (507) 238-8258 Services offered: Calibration services lab using our protocols running on Coesfeld
Website: www.dillon-force.com instruments
Email: info@dillion-force.com Electro Standards Laboratories Services offered: Simulation software that
Robin Rogge, marketing 36 Western Industrial Dr. analyzes the fatigue performance of elasto-
Instrumentation: Testing systems, com- Cranston, RI 02921 .............(401) 943-1164 mers under real world service conditions
puter controlled to manual systems, force Fax: (401) 946-5790 (See our ad on page 20)
guages, load cells, software Website: www.electrostandards.com
Services offered: Sales, service and techni- Email: eslab@electrostandards.com Epic, Inc.
cal assistance Jeanette Gouin, marketing manager 403 Fort Salonga Rd.
Instrumentation: Controllers, laboratory Northport, NY 11768
Eagle Polymer Equipment equipment (miscellaneous), measuring ...............................................(631) 239-1668
P.O. Box 1271 equipment, testers and testing equipment, Fax: (631) 261-0765
Akron, OH 44309 .................(330) 706-0552 burst testers, compression testers, cord Website: www.epictachometers.com
Fax: (330) 706-0546 tensile testers, creep rupture testers, fatigue Email: epictachometers@optimum.net
Website: www.polymerequipment.com testers, shear testers, tear tensile testers, Greg Letica, chairman/president
Email: info@polymerequipment.com tensile strength testers, universal testers Instrumentation: Tachometers
Tim Samples, president
Instrumentation: Curemeters/rheometers, Electro-Steam Generator Corporation Equitech Int’l Corporation
environmental chambers, measuring 50 Indel Ave. 903 Main St., South
equipment, physical testing equipment, Rancocas, NJ 08073-0438 New Ellenton, SC 29809 .....(706) 364-6060
scales, test chambers, tensile tear testers, ...............................................(609) 288-9071 Website: www.equitechintl.com
viscometers (866) 617-0764 Email: rfloyd@equitechintl.com
Fax: (609) 288-9078 Ron Floyd, president and CEO
Ektron Tek Co., Ltd. Website: www.electrosteam.com Instrumentation: Probes, chemical process
Tien-Chung Chang-Hwa 520 Email: sales@electrosteam.com analyzer and spectrometers

FOLLOW US ON TWITTER @rubberworld 53


Instrumentation, Test Equipment Suppliers
Erhardt + Leimer, GmbH surement system for an entire bale of Email: sales@grecon-us.com
350 Tucapau Rd. synthetic rubber Terry Franklin, sales
Duncan, SC 29334 ..............(864) 486-3000 Services offered: Nondestructive testing, Instrumentation: GreCon spark detection
Fax: (864) 486-3011 physical testing, production control and extinguishing systems are a preven-
Website: www.erhardt-leimer.com tative measure against combustible dust
Email: wneumann@erhardt-leimer.com French Oil Mill Machinery Co. fires and explosions
Werner Neumann, division manager 1035 W. Greene St.
Piqua, OH 45356-0920 Grieve Corporation
Exakt Technologies, Inc. ......................................... (937) 773-3420 500 Hart Rd.
7002 N. Broadway Ext. Fax: (937) 773-3424 Round Lake, IL 60073 ..... (847) 546-8225
Oklahoma City, OK 73116-9006 Website: www.frenchoil.com Fax: (847) 546-9210
...............................................(800) 866-7172 Email: sales@frenchoil.com Website: www.grievecorp.com
(405) 848-5800 Daniel P. French, chairman and CEO; Email: sales@grievecorp.com
Fax: (405) 848-7701 March Archey, polymer sales; Alex Lee, Frank Calabrese, sales manager
Website: www.exaktusa.com polymer sales; Jason McDaniel, COO Instrumentation: Ovens and furnaces
Email: info@exaktusa.com and president; Doug Smith, hydraulic
Linda E. Durbin, president and CEO sales; Dave Sledz, hydraulic and mixer Hamamatsu Corporation
Instrumentation: Laboratory cutting sys- sales; Dennis Ashurst, aftermarket sales 360 Foothill Rd.
tems, grinding systems, three-roll mills Instrumentation: Laboratory compres- Bridgewater, NJ 08807
sion and transfer hydraulic presses and ......................................... (908) 231-0960
Exova mixers Fax: (908) 231-1218
2395 Speakman Dr. Website: www.usa.hamamatsu.com
Mississauga, Ontario, Canada L5K 1B3 Gasmet Technologies Email: usa@hamamatsu.com
...............................................(905) 822-4111 Oy, Pulttitie 8 A, FI-00880 Helsinki, Yakov Bulayev, product manager
Fax: (905) 823-1446 Finland ..........................358 9 7590 0400 Instrumentation: Detectors, imaging de-
Website: www.exova.com Website: www.gasmet.com vices, cameras, light sources, photomulti-
Email: americas@exova.com Email: contact@gasmet.fi plier tubes, light sources, imaging tubes,
John McNeill, general manager Instrumentation: Gas monitoring instru- opto-semiconductor, imaging and analyz-
Instrumentation: Aging apparatus, analysis ments and systems ing system, x-ray inspection machines
equipment, baths, chemical analysis, com-
puters, curemeters/rheometers, densim- Divisions: Hardy Process Solutions
eters, dies, durometers, gauges, inspection Gasmet Ansyco GmbH 9440 Carroll Park Dr.
systems. .......................................+49 721 626 560 San Diego, CA 92121 ..... (858) 278-2900
Website: www.gasmet.de Website: www.hardysolutions.com
Experimental Services, Inc. Email: info@ansyco.de Email: hardyinfo@hardysolutions.com
894 W. Waterloo Rd. Rodger Jeffery, director of marketing and
Akron, OH 44314 .................(330) 848-0059 Goettfert product development
Website: www.esilab.com 488 Lakeshore Pkwy. Instrumentation: Scales
Email: kwinkler@esilab.com Rock Hill, SC 29730 ........ (803) 324-3883
Karl Winkler, president Fax: (803) 324-3993 Harris Instruments Corp.
Instrumentation: Used equipment, actua- Website: www.goettfert.com 155 Johnson Dr.
tors, manifolds Email: info@goettfert.com Delaware, OH 43015....... (740) 369-3580
Tim Haake, general manager Fax: (740) 369-2653
Facts, Inc. Instrumentation: Rheometers, rheovulka- Website: www.harris-instrument.com
2737 Front St. meter, curemeters and extruders Email: info@harris-instrument.com
Cuyahoga Falls, OH 44221 Joe Lieser, sales manager
...............................................(330) 928-2332 Gomaplast Machinery, Inc. Instrumentation: Non-contact measure-
Fax: (330) 928-3018 2424 Long Rd.
ment sensors, control systems, digital
Website: www.facts-inc.com Wooster, OH 44691......... (330) 263-7845
process control systems
Email: tfisher@facts-inc.com Fax: (330) 263-7846
Services offered: Monitor and control of
Tim Fisher, owner Website: www.gomaplast.com
extruded dimension for size control and
Instrumentation: Computers, controllers, Email: sales@gomaplast.com
measurement of shrinkage, inspection
gauges, measuring equipment, monitors Marcelo S. Hildebrandt, president
for holes
Instrumentation: Tensile testers, rheom-
Forte Technology, Inc. eters, lab ovens, lab presses, lab mixers,
HF Rubber Machinery, Inc.
58 Norfolk Ave. viscometers and scales
1701 Northwest Topeka Blvd.
South Easton, MA 02375 (See our ad on page 21)
Topeka, KS 66608........... (785) 235-2336
...............................................(508) 297-2363
Fax: (508) 297-2314 GreCon, Inc. Fax: (785) 235-1331
Website: www.forte-tec.com 15875 SW 74th Ave. Website: www.hfrmusa.com
Email: info@forte-tec.com Tigard, OR 97224 ........... (503) 641-7731 Email: mixing@hf-group.com
Patricia R. White, president Fax: (503) 641-7508 Paul White, executive VP operations
Instrumentation: Electronic moisture mea- Website: www.grecon-us.com Instrumentation: Laboratory equipment

54 RUBBERWORLD.COM ‡ JANUARY 2018


Instrumentation, Test Equipment Suppliers
Hitec Sensor Developments, Inc. Imada, Inc. microscopy, stress and strain, salt fog
537 Great Rd. 3100 Dundee Rd., Ste. 707 Services offered: Sales and calibration of
Littleton, MA 01460 .............. (978) 742 9032 Northbrook, IL 60062...........(847) 562-0834 test instrumentation
Fax: (978) 742 9033 Fax: (847) 562-0839
Website: www.hitecsensors.com Website: www.imada.com Instron Corporation
.............................. sales@hitecsensors.com Email: imada@imada.com 825 University Ave.
Tim Cetto, vice president Bob Hashioka, marketing manager Norwood, MA 02062............(781) 828-2500
Instrumentation: Rolling resistance load Instrumentation: For tension, compression, (800) 877 6674
cells, multi-axis load cells peel, adhesion; mechanical and digital force Website: www.instron.com
Services offered: ISO-17025 accredited gauges, manual and motorized test stands, Email: marcom@instron.com
calibration SPC software and special attachments up Kaleigh Durkin, events and media specialist
to 4,400 lbf.; ISO 9001 and ISO/IEC 17025 Instrumentation: Universal tension and
Hoto Instruments accredited compression testing machines, servo-
3100 Dundee Rd., Ste. 707 hydraulic machines for determining the
Northbrook, IL 60062...........(847) 564-2260 Imass, Inc. dynamic properties of elastomers, grips, ex-
(866) 527-4666 P.O. Box 134 tensometers and environmental chambers
Fax: (847) 564-2095 Accord, MA 02018-0134 Services offered: Technical service, training,
Website: www.hoto-instruments.com ...............................................(781) 834-3063 software programs, load and extensometer
Email: info@hoto-instruments.com Fax: (781) 834-3064 verification traceable to NIST
Bob Hashioka, marketing manager Website: www.imass.com
Instrumentation: Asker digital and analog Email: sales@imass.com ISRA Surface Vision
durometers; hand-held, auto loading and Eleanor Fusoni, advertising manager 4470 Peachtree Lakes Dr.
automatic micro durometers for measuring Instrumentation: Materials testing instru- Duluth, GA 30096 ................(770) 449-7776
hardness and characteristics of various rub- ments Fax: (770) 449-0399
ber, elastomers, plastics, sponges urethane
Website: www.lisravision.com
foam and polystyrene foam
Impakt Email: info.surface@isravision.com
Services offered: Calibration services
5721 Dragon Way Maureen Macken, marketing manager
(See our ad on page 87)
Cinncinnati, OH 45227 Instrumentation: Quality control systems;
...............................................(513) 271-9191 inspection and measurement, web inspec-
Hudson Cutting Solutions, a division of
IPSUMM, Inc. Fax: (513) 271-5120 tion system
8810 Place Ray-Lawson Website: impaktusa.com Services offered: Turnkey systems including
Anjou, Quebec, Canada H1J 1Z2 Email: sales@impaktusa.com training, installation, maintenance and sup-
...............................................(603) 570-4090 Bruce Freeman port worldwide
Website: www.hudsoncutting.com Instrumentation: Laboratory specimen
Email: dlees@hudsoncutting.com cutters, laboratory cutting presses, sample J&L Tool & Machine, Inc.
David Lees, sales molds 1441 Miller Ave.
Instrumentation: Fortuna rubber splitting Services offered: Sharpening and certifica- Shelbyville, IN 46176 ...........(317) 398-6281
and skiving machines. Hudson swing beam tion of laboratory specimen cutters Fax: (317) 392-4267
cutting presses for laboratory ASTM speci- Website: www.jltool.com
men preparation Indusco Email: bob@jltool.com
3611 Keystone Ave. Bob Landwerlen, president
Hydramotion Ltd. Nashville, TN 37211.............(615) 833-0666 Instrumentation: JL 5000 SPL flow com-
1 York Rd. Business Park Fax: (615) 834-8722 parator
Malton, North Yorkshire, U.K. YO17 6YA Website: www.induscousa.com
...........................................+44 1653-600294 Donny Fetzer, sales manager JCR Automation, Inc.
Fax: +44 1653-693446 Instrumentation: Fatigue, tear, tensile 1426 S. Ryan Rd.
Website: www.hydramotion.com testing; instrumentation for testing of raw New Haven, IN 46774 .........(260) 493-6606
Email: sales@hydramotion.com materials, vulcanized and unvulcanized Fax: (260) 749-4782
Danny Morbey, operations manager rubber testing Website: www.jcrautomation.com
Instrumentation: Process viscometers, por- Email: sales@jcrautomation.com
table and laboratory viscometers, viscosity Indy Tech Lab Equipment Inc. Rick Johnson, general manager
measuring instrumentation, online viscosity 27 Legend Ct. Instrumentation: PVT (pressure-vibration-
analyzers, viscosity meters Ancaster, Ontario, Canada L9K 1P3 thermal) coolant hose durability tester
...............................................(905) 512-7751 Services offered: Design and build test
IKA Works, Inc. Fax: (905) 304-2110 equipment for component durability, audit
2635 Northchase Pkwy., SE Website: www.indytechlab.com and functional tests; leak and burst testing
Wilmington, NC 28405 ........(910) 452-7059 Email: sales@indytechlab.com equipment with data acquisition capability
(800) 733-3037 Brian Williams
Fax: (910) 452-7693 Instrumentation: Indy offers a wide range J.D. & Company
Email: sales@ika.net of used and reconditioned test instruments P.O. Box 818
Bob Anderson, operations manager and devices: Izod charpy impact, hardness, 1708 Hal Ave.
Instrumentation: Laboratory equipment tensile, tear, density, tack, micrometer, Cleburne, TX 76033........... (817) 645-5644

FOLLOW US ON TWITTER @rubberworld 55


Instrumentation, Test Equipment Suppliers
Fax: (817) 645-9180 endurance testers, tire laser measurement Email: contact@lmi3d.com
Email: jdcustommix@sbcglobal.net systems, tire durability testers, inside drum Len Chamberlain, vice president, sales
R. Joe Dunnam, CEO; Amy Hiett, president; testers (durability/fatigue), treadwear tester, Instrumentation: Over 44 non-contact laser-
Deborah Baker, vice president 10 tire tester, side force testing machine, based measurement sensors for a variety
Instrumentation: Curemeters, rheometers, tread pressure distribution testing machine, of on and off line applications; these include
laboratory equipment, testers - specific bead expansion tester, road surface motion radial runout at full production speed; profil-
gravity observation machine, traction-BUS testing ing green and high silicone content rubber;
Services offered: Consulting services, machine, bump run-over testing machine, tire sidewall and inspection, thickness
general, formula and/or compound develop- plunge testing machine control of calendered rubber; splice width
ment, management consulting detection; treadwear analysis; extrusion
The Lanly Company profiling and profiling sidewall bulge and
J.M. Machinery 26201 Tungsten Rd. dent, and many others
P.O. Box 378 Cleveland, OH 44132 ........ (216) 731-1115 Services offered: Installation, training and
Wadsworth, OH 44282 ........(330) 825-2400 Fax: (216) 731-7900 support services; OEM capability
Fax: (330) 825-0569 Email: sales@lanly.com
Website: www.jmmachinery.com Website: www.lanly.com Lydon Oven Company
Email: dyer@jmmachinery.com Dennis W. Hill, president; Ed Chapman, P.O. Box 708
Michael Dyer, president applications engineering manager Hackensack, NJ 07602-0708
Instrumentation: Autoclaves, calenders, Instrumentation: Ovens ...............................................(201) 343-4334
extruders, laboratory equipment (miscella- Fax: (201) 343-7335
neous), mills, mixers, presses, compression Leica Microsystems Inc. Website: www.lydonoven.com
testers, cord tensile testers, specific gravity 1700 Leider Ln. Email: info@lydonoven.com
testers, tear tensile testers, tensile strength Buffalo Grove, IL 60089 Timothy McBride, president
testers, viscometers ...............................................(800) 248-0123 Instrumentation: Ovens
Fax: (847) 236-3009
Keithley Instruments, Inc. Website: www.leica-microsystems.com Maag Automatik Inc.
28775 Aurora Rd. Email: info@leica-microsystems.com 1500 Continental Blvd.
Solon, OH 44139 .................(440) 248-0400 Markus Lusser, president Charlotte, NC 28273............(704) 716-9000
Fax: (915) 852-4084 Instrumentation: Microscopes, measuring Fax: (704) 716-9001
Website: www.keithley.com equipment, microphotographic equipment, Website: www.maag.com
Email: info@keithley.com microtomes Email: maagamericas@maag.com
Linda Rae, president Services offered: Technical service, training Phil Shoemaker, general manager
Instrumentation: Data systems (includes Instrumentation: Dies, dryers, mixers, tem-
acquistion systems), electronic instrumen- Limpro Equipment & Services Inc. perature measuring devices
tation, recorders and indicators (includes 19 Sun Ter. Services offered: Pelletizing, processing,
chart, event and production, round and/or Laguna Niguel, CA 92677 reclaiming and recycling
strip chart records), temperature controllers, ...............................................(949) 636-3840
controls, systems Website: www.limprotech.com Malcam, Ltd.
Email: roger@limprotech.com 27th Habarzel St.
KLA-Tencor Roger Kuntz, CEO Tel Aviv, Israel 6971039
One Technology Dr. Instrumentation: Lab production systems, .............................................+972-3-6485664
Milpitas, CA 95035...............(408) 875-3000 mix meter and dispensing systems, liquid Fax: +972-3-6488335
Fax: (408) 875-4144 injection molding machines Website: www.malcam.com
Website: www.kla-tencor.com Email: info@malcam.com
Email: customer.parts@kla-tencor.com C.A. Litzler Co., Inc. Udi S. Moshe, sales director, sales and
Rick Wallace, CEO 4800 W. 160th St. marketing department
Instrumentation: Xi-100 IFM Cleveland, OH 44135-2689 Instrumentation: Analysis equipment,
Services offered: Carbon black dispersion ...............................................(216) 267-8020 measuring equipment, meters and moisture
index measurement Fax: (216) 267-9856 meters, density testers, high speed unifor-
Website: www.calitzler.com mity testers
Kokusai, Inc. Email: sales@calitzler.com
5333 W. 79th St. James H. Rogers, vice president, sales Malvern Instruments, Inc.
Indianapolis, IN 46268 .........(317) 704-9922 Instrumentation: Computreater 2000 single 117 Flanders Rd.
Fax: (317) 704-9921 end cord treating lab machine Westborough, MA 01581-1042
Website: www.kokusaiusa.com Services offered: Field service ...............................................(508) 768-6400
Email: sales@kokusaiusa.com Fax: (508) 768-6403
John Funcheon, president, Kokusai LMI Technologies Website: www.malverninstruments.com
Instrumentation: Bead seaters, dynamome- 9200 Glenlyon Pkwy. Email: sales.us@malvern.com
ters, laboratory equipment (miscellaneous), Burnaby, BC, Canada V5J 5J8 Randy Byrne, sales and marketing
measuring equipment, fatigue testers, high ............................................... (604) 636 1011 Instrumentation: Instrumentation for dynam-
speed uniformity testers, rolling resistance Fax: (604) 516 8368 ic/thermomechanical and processability
testers, tear tensile testers, tire testers, tire Website: www.lmi3d.com testing

56 RUBBERWORLD.COM ‡ JANUARY 2018


Instrumentation, Test Equipment Suppliers
Manufacturers Supplies Co. Website: www.metravib.com automatic dimensional measurement of
4220 Rider Trail N. Email: stephanie.briand@acoemgroup. o-rings, gaskets, etc.
Earth City, MO 63045.........(314) 770-0880 com
Fax: (314) 770-0990 Hugues Baurier, head of DMA department MonTech USA
Website: www.mfgsup.com Instrumentation: Dynamic mechanical 1280 S. Williams Dr.
Email: information@mfgsup.com analyzers for rubber compounds Columbia City, IN 46725
Robert D. Goellner, president Services offered: Training courses .............................................. (260) 244-5115
Instrumentation: Equipment for lab testing Fax: (260) 244-4158
clickers for dumbbell cutting; skiving equip- Mettler-Toledo, Inc. Website: www.montechusa.com
ment for ply splitting; bandknife splitters for 1900 Polaris Pkwy. Email: info@montechusa.com
splitting for layer analysis Columbus, OH 43240 ............(800) Mettler Richard Bagan
Services offered: Service and installation Fax: (614) 438-4518 Instrumentation: Rubber process analyzers,
of company equipment Website: www.mt.com/us rheometers, Mooney viscometers,
Email: labinsidesales@mt.com hardness/density testers, filler dispersion
Mast/Keystone Michael Zemo, marketing testers, sample cutters, legacy equipment
2200 Dickerson Rd. Instrumentation: Dynamic mechanical upgrades, parts, analysis software
Reno, NV 89503 .................(510) 931-7747 analyzers, thermomechanical analyzers, Services offered: Rubber testing equip-
Fax: (775) 324-5375 differential scanning, calorimeters, thermo- ment, calibration, maintenance, repair
Website: www.mastdev.com gravimetric analyzers, balances (See our ad on page 19)
Email: sales@mastdev.com
Thomas Hall, marketing director; Gifford Micromeritics Instrument Corporation MTI Instruments, Inc
Mast, president 4356 Communications Dr. 325 Washington Ave. Ext.
Instrumentation: Ozone test chamber, Norcross, GA 30093...........(770) 662-3633 Albany, NY 12205-5505 ......(518) 218-2550
monitors Fax: (770) 662-3696 (800) 342-2203
Website: www.micromeritics.com Fax: (518) 218-2506
McGill AirPressure, LLC Email: ussales@micromeritics.com Website: www.mtiinstruments.com
1777 Refugee Rd. Preston Hendrix, president; Jeff Sher- Email: sales@mtiinstruments.com
Columbus, OH 43207 ........(614) 829-1200 man, vice president, sales and business Kevin G. Lynch, chief executive officer
Fax: (614) 445-8759 development; Ray Lombardi, marketing Instrumentation: Quality control inspection
Website: www.mcgillairpressure.com manager products, sensors, amplifiers using fiber
Email: sales@mcgillairpressure.com Instrumentation: Analysis equipment, optic, capacitance, laser technologies, for
Jared McGill, sales manager physical testing equipment, porosity detec- displacement vibration, runout , thickness
Instrumentation: Autoclaves, dryers tors, density testers, specific gravity testers and surgace condition

Meeco Inc. Micro-Poise Measurement Systems, LLC MTS Systems Corp


250 Titus Ave. 555 Mondial Pkwy. 14000 Technology Dr.
Warrington, PA 18976 ........(215) 343-6600 Streetsboro, OH 44241-4510 Eden Prarie, MN 55344-2290
Fax: (215) 343-4194 ............................................ (330) 541-9100 ...............................................(800) 328-2255
Website: www.meeco.com Fax: (330) 541-9111 Fax: (925) 937-4515
Email: sales@meeco.com Website: www.micropoise.com Website: www.mts.com
Rob Leiter, marketing Email: micropoise.techsupport@ametek. Email: info@mts.com
Instrumentation: Electrolytic moisture ana- com Dr. Jeffrey A. Graves, president
lyzers, electronic measuring instruments to Les Gyori, vice president sales and Instrumentation: Test systems to measure
detect trace moisture in gases and solids service the dynamic properties of elastomeric
Services offered: Technical service Instrumentation: Analysis equipment, materials and components
inspection systems, measuring equipment, Services offered: Technical consulting
Mesabi Control Engineering, Ltd. physical testing equipment, software sys- service, training, software programs
1350 Arcade St. tems, testers and testing equipment, test-
St. Paul, MN 55106 ............(651) 771-1890 ers - tire, tire laser measurement systems, Nanotronics Imaging
Fax: (651) 771-0437 x-ray inspection machines 2251 Front St., Ste. 109-111
Website: www.mesabicontrol.com Services offered: Non-destructive testing, Cuyahoga Falls, OH 44221
Email: mesabi@mesabicontrol.com physical testing, test method development ...............................................(330) 926-9809
John Beaudoin, president (See our ad on page 6) Website: www.nanotronicsimaging.com
Instrumentation: Computers, controllers, Email: info@nanotronicsimaging.com
measuring equipment, monitors, scales, Micro-Vu Corp. Matthew Putman, CEO; John Putman,
software systems, special services, tem- 7909 Conde Ln. president and chief technology officer
perature measuring devices Windsor, CA 95492 ............(707) 838-6272 Instrumentation: Nanoscale imaging and
Fax: (707) 838-3985 inspection systems, rapid topography
Metravib Website: www.microvu.com measurements
200 Chemin Des Ormeaux Email: sales@microvu.com
Limonest Cedex F-69578 Greg Chatfield, marketing/sales manager NDC Infrared Engineering Inc.
France ............................ +33 472 52 48 00 Instrumentation: Automated video co- 5314 North Irwindale Ave.
Fax: +33 4 72 52 47 47 ordinate measuring machines providing Irwindale, CA 91706 ............(626) 939-3887

FOLLOW US ON TWITTER @rubberworld 57


Instrumentation, Test Equipment Suppliers
Fax: (626) 939-3870 Nikon Inc., Instrument Group Email: info@olympusndt.com
Website: www.ndc.com 1300 Walt Whitman Rd. Nacho Abia, president
Email: enquiries@ndc.com Melville, NY 11747............ (973) 966-1100 Instrumentation: Thickness gauges, flaw
David Wambold, vice president Fax: (631) 547-4025 detectors, transducers, automated sys-
Instrumentation: On-line thickness gaug- Website: www.nikoninstruments.com tems, instrumentation
ing, contact systems for the rubber and Cynthia Flynn, sales manager Services offered: Applications lab, training
calendered products industry; systems Instrumentation: Profile projectors, video
range from simple single-point measure- measuring systems, microscopes Ontario Die International
ments to complete scanning systems Services offered: Technical service, train- 235 Gage Ave.
ing, software programs Kitchener, Ontario, Canada N2M 2C9
NELA Vision Systems ........................................... (519) 745-1002
610 Whitetail Blvd. Nishiyama Corporation of America Fax: (519) 745-0051
River Falls, WI 54022 .........(888) 407-4808 Division: Nishiyama Corp. Japan Website: www.ontariodie.com
(715) 425-1900 111 Great Neck Rd., Ste. 301 Email: kitchener@ontariodie.com
Fax: (715) 425-1901 Great Neck, NY 11021 ....(516) 466-7570 Gary Levene, president
Website: www.nela-usa.com Fax: (516) 466-7572 Instrumentation: Laboratory specimen
Email: info@nela-usa.com Email: rxue@nishiyama-usa.com cutters, laboratory cutting presses, sample
Katharina Gruber, marketing manager Website: www.nishiyama.co.jp molds
Instrumentation: Fully automatic inspection Takumi Kawabe, vice president, sales Services offered: Sharpening and certifi-
systems and marketing; Raymond Xue, customer cation of laboratory specimen cutters
service manager
Netzsch Instruments North America, Instrumentation: Measuring diaphragms Ontario Die International (USA) Inc.
LLC for gas meters 2735 20th St.
129 Middlesex Turnpike Port Huron, MI 48060 ...... (810) 987-5060
Burlington, MA 01803 ....... (781) 272-5353 OAI (Optical Associates Inc.) Fax: (810) 987-3688
Fax: (781) 272-5225 685 River Oaks Pkwy. Website: www.ontariodie.com
Website: www.netzsch.com San Jose, CA 95134 ........ (408) 232-0600 Email: porthuron@ontariodie.com
Email: nib-sales@netzsch.com Fax: (408) 433-9904 Instrumentation: Laboratory specimen
Dave Shepard, sales manager Website: www.oainet.com cutters, laboratory cutting presses, sample
Instrumentation: Analysis equipment, Email: sales@oainet.com molds
curemeters/rheometers, testers and test- Nat Weil
ing equipment - thermal analysis and ther- Instrumentation: UV radiometers, cureme- Orec Ozone Chambers and Monitors
mal properties measurement instruments ters University Park
and testing services; featuring the new Akron, OH 44304 .............. (330) 376-3600
highest-force dynamic mechanical (DMA/ ODC Tooling and Molds (800) 742-8535
DMTA) testing instruments; Netzsch-Gabo 119 Roger St. Fax: (330) 376-8500
Eplexor and Qualimeter flexometers for Waterloo, Ontario, Canada N2J 3Z6 Website: www.orecozone.net
measurement of thermal fatigue of rub- ........................................... (519) 576-8950 Email: info@ccsi-inc.com
ber, testing instruments for measurement Fax: (519) 576-3670 Michael Kent Warner, executive vice presi-
of the dynamic durometer hardness or Website: www.odctooling.com dent; David Warner, president
adhesive properties (autohesion) such as Email: sales@odctooling.com Instrumentation: Ozone test chambers
rubber compounds before vulcanization; Ronald Levene, CEO/president providing continuous ozone measure-
thermal analyzers for polymer analysis Instrumentation: Controllers, dies, press- ment control and data aquisition; A2LA-
including DSC, TGA, STA (DSC-TGA) and es, testers and testing equipment, testers 17025 calibrations NIST primary monitor
TMA with coupling to FTIR, MS and GC- tear tensile, testers tensile strength standards
MS for analysis of evolved gases; thermal Services offered: Instrumentation: Durom-
conductivity by guarded hot plate and the OHMIC Intruments
eter hardness testers, curemeter (ODR),
laser flash method 508 August St.
Mooney viscometer, Rheomaster data
Services offered: Contract testing services Easton, MD 21601............ (410) 820-5111
systems for Mooney and rheometers,
Fax: (410) 822-9633
ASTM dies, molds, cutters, the XDR
Newage Testing Instruments, Inc., An Website: www.ohmicinstruments.com
Mooney viscometer, XDR-MDR moving
Ametek Company Email: ohmic@ohmicinstruments.com
die rheometer, Orec ozone chambers and
820 Pennsylvania Blvd. Ed Donovan
monitor calibration, low temperature TR
Feasterville, PA 19053 ...... (215)-355-6900 Instrumentation: Dew point monitors and
test and brittleness point tester, ASTM
Fax: (215)-354-1803 controllers, absolute humidity transmitters
cutting dies.
Website: www.hardnesstesters.com Services offered: Servicing and calibration
Services offered: Certified calibration/ser-
Email: newage.info@ametek.com of all “Ohmic” manufactured equipment
vice/repair of durometer hardness testers,
Rick Wismer, sales manager
Instrumentation: Hardness testers for Olympus - NDT Mooney viscometers, all rheometers
IRHD and durometer scales in both regu- 48 Ward Ave. and recorders, tensile testers, thickness
lar and micro, built in SPC, RS232 output, Waltham, MA 02453 ......... (800) 225-8330 gauges, A2LA certified calibration lab and
fully automated for reduced operator (781) 419-3900 ISO 9002 and 17025 registered
influence Website: www.olympusndt.com (See our ad on page 83)

58 RUBBERWORLD.COM ‡ JANUARY 2018


Instrumentation, Test Equipment Suppliers
Oxford Instruments Fax: (330) 633-6367 Services offered: Service and calibration of
300 Baker Ave. Website: www.polymermachineryco.com rubber testing
Concord, MA 01742-2124 Email: jchiofolo@polymermachineryco.com
...............................................(800) 447-4717 Jim Chiofolo, sales Princo Instruments, Inc.
(978) 369-9933 Instrumentation: Rheometer, viscometer, 1020 Industrial Blvd.
Fax: (978) 369-8287 testers; fatigue, dynamic, flex-cracking, Southhampton, PA 18966
Website: www.oxford-intruments.com ozone chamber, aging oven, tire plunger, air ...............................................(215) 355-1500
Email: industrial@oxinst.com permeability, oil bath, carbon black disper- Fax: (215) 355-7766
Chris Horvath, director of sales and market- sion, electronic tensile, tensile strength, Website: www.princoinstruments.com
ing, XRF products, Americas abrasion resistance; electronic densimeter, Email: info@princoinstruments.com
Instrumentation: EDXRF, WDXRF, MDXRF tire cutting machine, constant temperature Paul Wasser, president
and HHXRF and humidity chamber Instrumentation: Level controls. level trans-
mitters, thermometers and thermostats
Pacific Transducer Corp. - PTC Polymer Testing Instruments Services offered: Technical service
Instruments 74 Patton Ave.
2301 Federal Ave. Asheville, NC 28801 ............(828) 252-1326 Prosco, Inc.
Los Angeles, CA 90064 ......(310) 478-1134 Website: www.polymer-testing.com 450 Keller Dr., Unit C
Fax: (310) 312-0826 Email: andy@polymer-testing.com Park City, IL 60085...............(847) 336-1323
Website: www.ptc1.com Andy Sluder, sales and service manager Fax: (847) 336-1390
Email: sales@ptc1.com Instrumentation: Rheometer and viscom- Website: www.prosco-inc.com
John S. Marcus, president eter rebuilds Email: contact@prosco-inc.com
Instrumentation: Durometers, microscopes, Peter Kubala, sales manager
temperature measuring devices, hardness PPD Group Instrumentation: Grinders, laser inspection
testers, tester stands 325 Principale N. systems
Waterville, Quebec, Canada J0B 3H0
Perkin Elmer Instruments .............................................. (819) 837-2952 PTC Instruments/PTC Metrology
940 Winter St. (819) 578-8580 2301 Federal Ave.
Waltham, MA 02451 ............(800) 762-4000 Fax: (819) 837-3140 Los Angeles, CA 90064 ......(310) 478-1134
(203) 925-4602 Website: www.ppdgroup.com Fax: (310) 312-0826
Fax: (203) 944-4904 Email: jacars@ppdgroup.com Website: www.ptc1.com
Website: www.perkinelmer.com Donald Morrissetle, president Email: info@ptc1.com
Email: customercareus@perkinelmer.com Instrumentation: QA and QC systems Linda A. Wolfe, general manager
Robert F. Friel, chairman, CEO and presi- Services offered: ASTM based tests like Instrumentation: Durometers to measure
dent compression set, heat resistance, liquid the hardness of rubber, plastic, ASTM,
Instrumentation: Analytical instruments resistance and ozone resistance A,B,C,D, DO, O, OO,OOO
used in laboratory analysis Services offered: Technical service, repair,
Services offered: Technical service, training, Precision Measurement Company durometer calibration and certification with
software programs P.O. Box 7676 standards traceable to NIST design custom
Ann Arbor, MI 48107............(734) 995-0041 durometers, A2LA accredited laboratory for
Piedmont Polymer Equipment Website: www.pmctransducers.com durometer calibration (1896.01)
1220 Olde Oaks Dr. Email: info@pmctransducers.com
Grays, TN 37615..................(423) 753-7811 Samuel K. Clark, president Pyromation, Inc.
Fax: (423) 753-7911 Instrumentation: Pressure transducers 5211 Industrial Rd.
Robert Myers Fort Wayne, IN 46825..........(260) 484-2580
Instrumentation: Fatigue, tensile, process- Precision Quincy Ovens Website: www.pyromation.com
ability, ozone resistance testing 602 East Blackhawk Dr. Email: scott@pyromation.com
Byron, IL 61010....................(302) 602-8738 Scott Farnham, sales and marketing
PLV Systems Inc. Website: www.pqovens.com manager
116 Viceroy Rd., Bldg. D, Unit 5 Email: sales@pqovens.com Instrumentation: Thermocouples and
Concord, Ontario, Canada L4K 2M4 Troy F. Berg, president thermocouple assemblies, temperature
..................................(905) 761-7234, ext. 24 Instrumentation: Dryers, ovens, tempera- measuring devices
Fax: (905) 760-1473 ture measuring devices
Website: www.plv.com Pyrometer Instrument Company
Email: sm@plv.com Prescott Instruments Ltd. 92 North Main St.
Sam Melamed Unit F, Northway Trading Estate P.O. Box 479
Instrumentation: FS200 - family of profile Tewkesbury, Gloucester, UK GL20 8JU Windsor, NJ 08561-0479
extrusion measurement instruments for on- .......................................... 44 0 1684 274300 ...............................................(609) 443-5522
line and off-line dimensional characteristics; Fax: 44 0 1684 293223 Fax: (609) 443-5590
FS200-DOC (digital optical comparator). Website: www.prescott-instruments.com Website: www.pyrometer.com
Email: sales@prescott-instruments.com Email: sales@pyrometer.com
Polymer Machinery Company Instrumentation: Physical testing raw David Crozier, CEO
154-B Potomac Ave. materials, vulcanized and unvulcanized; Instrumentation: Temperature measuring
Tallmadge, OH 44278..........(330) 633-5734 processability testing devices, thermal line scanners, temperature

FOLLOW US ON TWITTER @rubberworld 59


Instrumentation, Test Equipment Suppliers
controllers, recorders, transmitters, NLW- RCMA Americas, Inc. (Ohio) ...............................................(631) 234-0500
laser pyrometer to measure emissivity 1507 Boettler Rd. Fax: (631) 234-0691
Services offered: Technical service, training, Uniontown, OH 44685 ........ (330) 896-5900 Website: www.mixers.com
calibration Fax: (330) 896-9943 Email: mail@mixers.com
Website: www.rcma.com Ann Marie Pappas, vice president
Q-Lab Corporation Email: rubber@rcma.com Instrumentation: Dryers, mills, mixers
800 Canterbury Rd. Chris Shephard, president
Westlake, OH 44145-1419 Instrumentation: Aging apparatus, baths, RWC Testing & Lab Supplies
...............................................(440) 835-8700 computers, durometers, laboratory equip- 1821 N. Zaragosa Rd.
Fax: (440) 835-8738 ment, measuring equipment, microscopes, El Paso, TX 79936 ...............(915) 852-3375
Website: www.q-lab.com mills, monitors, physical testing equipment, Fax: (915) 852-4084
Email: info@q-lab.com refractometers, scales, temperature meas- Website: www.rwctesting.com
James Gauntner, sales manager uring devices, test chambers, testers and Email: customerservice@rwctesting.com
Instrumentation: QUV accelerated weather- testing equipment, abrasion testers, adhe- Christy Huizar, product sales
ing tester, Q-Sun xenon arc test chambers, sion testers, burst testers, compression Instrumentation: Worldwide distributor for
Q-Panel standard test substrates, Q-Fog testers, density testers, flammability testers, many laboratory and measuring instru-
cyclic corrosion test chambers, Q-Trac flexing machines testers, flow index testers, ments, to include: tachometers, strobo-
natural sunlight concentrator hardness testers, non-destructive testers, scopes, pH meters, conductivity meters,
Services offered: Contract testing lab, permeability testers, viscometers turbidity meters, oxygen meters, refracto-
accelerated weathering testing, outdoor meters, tension meters, wall mount/por-
weathering testing Rex Guage Company, Inc. table gas detectors, etc. Industries served
1250 Busch Pkwy. include the scientific, industrial, military and
Qualitest USA, LLC Buffalo Grove, IL 60089.......(847) 465-9009 commercial sectors, as well as educational
1323 SE 17th St., Unit 200 Fax: (847) 465-9229 institutions
Ft. Lauderdale, FL 33316 Website: www.durometer.com
.............................................. (877) 884-8378 Email: info@durometer.com Sanyo Corporation of America
Fax: (954) 697-8211 JC Blum, vice president 500 Fifth Ave., Ste. 3620
Website: www.worldoftest.com; Instrumentation: Durometer hardness New York, NY 10110............(212) 221-7890
www.qualistore.mybigcommerce.com. gauges (for checking the hardness of non- Fax: (212) 221-7828
Email: info@qualitest-inc.com metallic surfaces), accessories Website: www.sanyocorpusa.com
A. Bezadi Services offered: Repair and calibration Kenichi Shindo, president
Instrumentation: Testing technologies for (durometer sales) Instrumentation: Physical testing equip-
rubber, including universal testing ma- (See our ads on pages 72 and 76) ment, testers - tensile strength
chines, durometers/IRHD hardness testers,
densimeter, brittleness testers, rebound RKC Instrument Satra Technology Centre
resilience tester, dies, DIN abrasion tester, 4245 Meghan Beeler Ct., Ste. Wyndham Way
clicker presses, flexometers, stress relaxa- South Bend, IN 46628 .........(877) 599-1990 Kettering, Northamptonshire, U.K.
tion tester, block oven/aging oven, fogging (574) 273-6099 NN16 8SD ................... +44 (0)1536 410000
tester and more Fax: (574) 247-9657 Fax: +44 (0)1536 410626
Services offered: Instrumentation/equip- Website: www.rkcinst-usa.com Website: www.hampden-test.com
ment for the testing of rubber Email: info@rkcusa.com Email: info@satra.co.uk
(See our ad on page 8) Yoshi Unno, president Austin Simmons, CEO
Instrumentation: Controllers, temperature Instrumentation: Ozone test cabinets,
Quest Integrated, Inc. measuring devices abrasion testers, resilience testers, IFD and
19823 58th Place S., Ste. 200 CFD foam hardness testers, porosity, rise
apparatus
Kent, WA 98032 .................. (253) 872-9500 Rockwell Automation, Inc.,
Services offered: Service and calibration
Fax: (253) 872-8967 Allen-Bradley
Website: www.qi2.com 1201 S. 2nd St.
Scanco USA, Inc
Email: contactqi2@qi2.com Milwaukee, WI 53204 ..........(414) 382-2000
985 Old Eagle School Rd.
Jonathan Kniss, director, business develop- Fax: (414) 382-4444
Wayne, PA 19087 ................(610) 688-1440
ment Website: www.rockwellautomation.com
Fax: (610) 688-4976
Instrumentation: Lotis QC-20 hose meas- Email: webmaster@rockwellautomation.
Website: www.microct.com
urement system com
Email: sales@scanco.ch
Services offered: Sales and service Keith Nosbusch, chairman and CEO
Rasesh Kapadia, president
Instrumentation: Computers, inspection Instrumentation: X-ray micro-computer
R&C Roll Grinding, Inc. systems, laboratory equipment (miscel- tomagraphy systems
P.O. Box 14190 laneous), measuring equipment, monitors, Services offered: Non-destructive scanning/
Bradenton, FL 34280...........(941) 778-7655 software systems, temperature measuring microscopy
Fax: (941) 896-8720 devices
Website: www.rcrollgrinding.com Schenck Corporation
Email: rollgrinding@gmail.com Charles Ross & Son Company 535 Acorn St.
Ken Bowers, owner 710 Old Willets Path Deer Park, NY 11729 ......... (631) 242-4010
Instrumentation: Calenders Hauppauge, NY 11788 Fax: (631) 242-4147

60 RUBBERWORLD.COM ‡ JANUARY 2018


Instrumentation, Test Equipment Suppliers
Website: www.schenck-usa.com Starrett Bytewise Tavdi Co., Inc.
Email: sales@schenck-usa.com 1150 Brookstone Centre Pkwy. 140 Beacon Park Dr.
Bertram Dittmar, president and CEO Columbus, GA 31904 ......... (706) 323-5142 Riverside, RI 02915 .............(401) 432-7086
Instrumentation: Universal and specialized Fax: (706) 323-0178 Fax: (401) 432-7183
balancing machines for the production, main- Website: www.starrett.com Website: www.tavdico.com
tenance and repair of virtually any rotating Email: dreynolds@bytewise.com Email: tavdi@tavdi.com
component; vibration analyzers, field balanc- Dennis Reynolds, vice president, sales Ismail Saltuk, president
ers and condition monitoring systems Instrumentation: On-line and off-line laser Instrumentation: Advanced Yerzley oscil-
measurement solutions for the tire industry lograph (AYO-IV) for testing physical prop-
Shimadzu Scientific Instruments and rubber extrusion industries. Measure- erties of rubber specimens as per ASTM
7102 Riverwood Dr. ment systems for the tire industry include D-945-16
Columbia, MD 21046 ..........(410) 381-1227 belt and ply width monitors, extrusion Services offered: Equipment sales, mainte-
...............................................(800) 477-1227 profile monitors, calender thickness and nance and repair services, consulting and
Fax: (410) 381-1222 width monitors, tire building machine runout testing
Website: www.ssi.shimadzu.com measurement systems, automatic tire iden-
Email: webmaster@shimadzu.com tification systems, cured tire profile meas- Tensitron, Inc.
Kevin McLaughlin, marketing 733 South Bowen St.
urement systems and treadwear analyzers.
Instrumentation: Hardness testers, univer- Longmont, CO 80501 ....... (303) 702-1980
Profile360 Generation 3 is widely used by
sal/tensile testers, capillary/flow testers, Fax: (303) 702-1982
all types of rubber extruders to monitor rub-
thermal analyzers, endurance/fatigue Website: www.tensitron.com
ber extrusion geometry on-line Email: orderdesk@tensitron.com
testers, UV-VIS and FTIR spectrometers, Services offered: Equipment, installation
balances, gas and liquid chromatography Ellen-Alisa Saxl, manager
and training Instrumentation: Cord, filament, wire, strap,
(See our ads on pages 10 and 11) band and cable tension testers, tension
Signature Control Systems
transducers, sheet-tension, rubber thread
25 Manzanita Herman H. Sticht Company, Inc. tension testers, digital, mechanical and
Littleton, CO 80127 ..............(720) 641-1131 45 Main St., Ste. 701 electronic tension meters
Fax: (810) 494-5022 Brooklyn, NY 11201-1075 Services offered: Custom instrumentation
Website: www.signaturecontrol.com .............................................. (718) 852-7602 available if your application requires a prod-
Email: info@signaturecontrol.com Fax: (718) 852-7915 uct not in our regular line of instrumentation
Tom Trexler, direct sales manager Email: stichtco@aol.com
Instrumentation: Intellegent process control Website: www.stichtco.com Testing Machines Inc.
system featuring SmartTrac expert system Paul Plotkin, president 40 McCullough Dr.
software to monitor and control process in Instrumentation: Tachometers, testers and New Castle, DE 19720 ........(302) 613-5600
real-time testing equipment (800) 678-3221
Fax: (302) 613-5619
Sikora International Corporation TA Instruments, Inc. - Waters LLC Website: www.testingmachines.com
215 Prospect Pk., Ste. C 159 Lukens Dr. Email: info@testingmachines.com
Peachtree City, GA 30269 New Castle, DE 19720 ....... (302) 427-4000 Instrumentation: Physical testers
.............................................. (770) 486-1233 Fax: (302) 427-4001 Services offered: Technical service, training
Fax: (770) 486-1201 Website: rubber.tainstruments.com
Website: www.sikora.com Email: info@tainstruments.com Testo, Inc.
Email: sales@sikora.net Ed Moriarty, marketing manager 40 White Lake Rd.
John Dognazzi, managing director Instrumentation: Thermal analysis, dynamic Sparta, NJ 07871.................(973) 252-1720
Instrumentation: On-line measuring and mechanical analysis, dielectric analysis, rub- Fax: (973) 252-1729
control systems for polymeric tubes and ber process analyzers, moving die rheom- Website: www.testo.us
hoses, controllers, gages, thickness gages, Email: info@testo.com
eters, Mooney viscometers, automated
laser equipment (includes laser/micropro- Marko Bruinsma, president
hardness and density testers, rheometers
cessor measuring products), measuring Instrumentation: Temperature-based instru-
for fluids and soft solids.
equipment and machines, process systems mentation
Services offered: Technical service, contract
and equipment Services offered: Technical service
testing
(See our ads on pages 15 and 77)
SP Industries Thermal Product Solutions (TPS), a divi-
935 Mearns Rd. sion of SPX Corporation
Taber Industries 2821 Old Route 15
Warminster, PA 18974
455 Bryant St. New Columbia, PA 17856-9396
.............................................. (215) 672-7800
North Tonawanda, NY 14120 .............................................. (800) 586-2473
Fax: (215) 672-7807
Website: www.spscientific.com ...............................................(716) 694-4000 (570) 538-7200
Email: info@spscientific.com (800) 333-5300 Fax: (570) 538-7380
Bill Downs, CEO Fax: (716) 694-1450 Website: www.tenney.com
Instrumentation: Ovens, environmental test Website: www.taberindustries.com Email: tpsinfo@tps.spx.com
chambers, incubators Email: sales@taberindustries.com Ron Cozean, CEO
Services offered: Technical services, train- Alan Jaenecke, vice president, marketing Instrumentation: Industrial ovens, environ-
ing, manufacturing Instrumentation: Destructive tests - abrasion mental test chambers and curing ovens

FOLLOW US ON TWITTER @rubberworld 61


Instrumentation, Test Equipment Suppliers
Thermo Scientific ity; products include gauges for measuring Email: info@unitedtesting.com
81 Wyman St. diameter, speed and length, flaw detection, Carol Watson, president
Waltham, MA 02451 ........... (781) 622-1000 profile, 100% length inspection systems Instrumentation: Materials testing systems
Fax: (781) 622-1207 Services offered: Technical service Services offered: Calibration of test systems
Website: www.thermo.com and assorted force equipment
Douglas Wright, marketing U-Can
Instrumentation: Torque rheometer for poly- No. 26, Houkou S. Rd., Houli Township, United Testing Systems
mer flow measurements using miniaturized Central Taiwan Science Park 2245 N. Cleveland-Massillon Rd.
production equipment; all units microproces- Taichung City 421, Taiwan Bath, OH 44210 ..................... (330) 659-6422
sor controlled; viscometers; Seiko instru- .......................................... 886-4-255913519 Fax: (330) 659-6433
ments thermal analysis; circulator products, Fax : 886-4-25591362 Website: www.unitedtestingsystems.net
melt flow testers, capillary rheometers, E-mail: ucan@u-can.com.tw Email: unitedtestingsystems@gmail.com
DSC, TGA, DMA, TMA and DCR Website: www.ucandyna.com Joseph Augustyn, president
Services offered: Technical service, training, Instrumentation: Rheometer, viscometer, Instrumentation: Magnetic particle, pene-
software program testers; fatigue, dynamic, flex-cracking, trant, ultrasonic and eddy current equipment,
ozone chamber, aging oven, tire plunger, air digital radiometer/photometer
Thermotron Industries permeability, oil bath, carbon black disper-
291 Kollen Park Dr. sion, electronic tensile, tensile strength, United Testing Systems, Inc.
Holland, MI 49423............... (616) 393-4580 abrasion resistance; electronic densimeter, 1375 S. Acacia Ave. Ste. A
Fax: (616) 392-5643 tire cutting machine, constant temperature Fullerton, CA 92831 .............. (800) 765-9997
Website: www.thermotron.com and humidity chamber Website: www.utsflint.com
Email: info@thermotron.com Email: info@unitedtesting.com
Clint Peterson, president; Kevin Ewing, vice Ueshima Seisakusho Co., Ltd. Cliff Schaffer, vice president
president of sales c/o Nishiyama Corporation of America Instrumentation: Materials testing systems
Instrumentation: Controllers, environmental Great Neck, NY 11021 ........(516) 466-7570 for hardness, tensile and compression
chambers, test chambers, testers and test- Fax: (516) 466-7572 Services offered: Calibration and certifica-
ing equipment Website: www.ueshima-seisakusho.co.jp/ tion of hardness and various force testing
top_en.html systems
Thwing-Albert Instrument Co. Email: kokusai@nishiyama.co.jp
14 W. Collings Ave. Instrumentation: Laboratory testing equip- Visco Technologies USA, Inc.
West Berlin, NJ 08091.........(856) 767-1000 ment to measure dynamic properties of 511 West Golf Rd.
Fax: (856) 767-2615 rubber and plastic for use in research and Arlington Heights, IL 60005
Website: www.thwingalbert.com development and/or production ................................................. (773) 332-3775
Email: sales@thwingalbert.com Services offered: Installation, training and Website: www.visco-tech.com/usa
Steven Berg, vice president of sales and support services Email: owakizono@visco-tech.com
marketing Osamu Wakizono
Instrumentation: Universal materials tensile Ultra Electronics, Nuclear Sensors & Instrumentation: image processing algorithm,
testing machines, tear testers, sample Process Instrumentation optical technology and cosmetic (appear-
cutters 707 Jeffrey Way ance) inspection solution
Services offered: Technical service, training, Round Rock, TX 78680-2408
calibration ...............................................(512) 434-2900 Vindum Engineering, Inc.
Fax: (512) 434-2901 1 Woodview Ct.
Tinius Olsen Testing Machine Co. Website: www.ultra-nspi.com San Ramon, CA 94582 ......... (925) 275-0633
1065 Easton Rd. Troy Johnson, vice president of operations Fax: (925) 275-9697
Horsham, PA 19044 ............(215) 675-7100 Instrumentation: Resistance temperature Website: www.vindum.com
Fax: (215) 441-0899 detector Email: info@vindum.com
Jorgen Vindum, president
Website: www.tiniusolsen.com
Union Process, Inc. Instrumentation: Analysis equipment, labora-
Email: info@tiniusolsen.com
1925 Akron-Peninsula Rd. tory equipment, testers viscometers
Wayne Hayward, marketing manager
Akron, OH 44313 .................(330) 929-3333
Instrumentation: Tension, compression test-
Website: www.unionprocess.com VTEC Laboratories Inc.
ing machines
Email: unionprocess@unionprocess.com 212 Manida St.
Services offered: Technical service, soft-
Emery Li, sales manager Bronx, NY 10474 ................... (718) 542-8248
ware programs
Instrumentation: Laboratory attrition mills, Fax: (718) 542-8759
fine grinding and dispersion equipment Website: www.vteclabs.com
TSI Incorporated Services offered: Chemical analysis and Email: neil@vteclabs.com
500 Cardigan Rd. physical testing Neil Schultz
Shoreview, MN 55126 .........(866) 266-5919 Instrumentation: Flammability test equipment
Fax: (651) 490-3824 United Calibration Corporation
Website: www.tsi.com 5802 Engineer Dr. Wabash MPI
Email: info@tsi.com Huntington Beach, CA 92649 1569 Morris St.
John R. Ross, president ...............................................(714) 638-2322 Wabash, IN 46992-0298 ....... (260) 563-1184
Instrumentation: Dimesional measurement (800) 765-9997 Fax: (260) 563-1396
products designed to improve manufactur- Fax: (714) 897-8496 Website: www.wabashmpi.com
ing productivity and enhance product qual- Website: www.unitedcalibration.com Email: wabashmpi@corpemail.com

62 RUBBERWORLD.COM ‡ JANUARY 2018


Instrumentation, Test Equipment Suppliers
David Singer, marketing manager Cresskill, NJ 07626 ..............(866) 945-5742 ber/wheel
Instrumentation: Manufacturer of compres- Fax: (201) 567-5770 Instrumentation: Provider of x-ray inspec-
sion, vacuum and transfer presses for Website: www.willrich.com tion equipment for industrial applications
various rubber molding applications. Force Email: customerservice@willrich.com Services offered: Non-destructive testing
ranges from .5 to 1,200 ton and platen sizes Rich Chitos, president (NDT), computed tomography (CT), highly
up to 6’ by 10’, presses can be supplied in Instrumentation: Analytical and torsion dynamic radioscopy (HDR), microfocus
standard configurations or customized to balances, cord testers, coating testers, x-ray, automatic defect recognition (ADR);
your specifications compression testers, durometers, elasticity applications include tire, rubber, wheel, cast
testers, dimensional gauges, other labora- parts, electronics, fiber-reinforced materials
Wallace Instruments, a brand of tory and testing equipment and more
Elektron Technology
Broers Building Winters Instruments Carl Zeiss, Inc., Microscope Division
JJ Thomson Ave. 121 Railside Rd. One Zeiss Dr.
Cambridge, U.K. CB3 0FA Toronto, Ontario, Canada M3A 1B2 Thornwood, NY 10594
.......................................+44 (0)1803 407756 ...............................................(416) 444-2345 ...............................................(800) 233-2343
Website: www.wallaceinstruments.co.uk Fax: (416) 444-8979 Fax: (914) 681-7446
Email: info@wallaceinstruments.co.uk Website: www.winters.com Website: www.zeiss.com
David Reynolds, sales manager Email: sales@winters.com Email: micro@zeiss.com
Instrumentation: Hardness testers H14 Barry Phillips, executive vice president; James Sharp, president
(IRHD); H17A (Shore), micro hardness test- Desmond Khor, marketing and communica- Instrumentation: Microscopes to examine
ers H12 (IRHD), H17M (Shore); densimeter tions manager surface characteristics, image analysis
X22B; rapid plastimeter P14; compression Instrumentation: Controllers, gauges, labo- equipment.
stress relaxometer C11; aging chamber ratory equipment (miscellaneous), measur- Services offered: Technical service, training,
O7E, O14; DeMattia flex testing machine ing equipment, temperature measuring software programs
F15/16, Mooney viscometer V3, thickness devices, testers and testing equipment
gauges; compression set, plasticity and Zumbach Electronics Corp.
resilience; specimen preparation equipment WSF Industries, Inc. Worldwide Headquarters
Services offered: Calibration, service and 7 Hackett Dr. Hauptstrasse 93
repair of all Wallace instruments Tonawanda, NY 14150 ........(800) 874-8265 2552 Orpund
(716) 692-4930 .................................... +41 (0) 32 356 04 00
Divisions: Fax: +41 (0) 32 356 04 30
Fax: (716) 692-4135
Americas Email: sales@zumbach.ch
Website: www.wsfindustries.com
Wallace USA Office
Email: sales@wsfindustries.com
5856 Corporate Ave., Ste. 220 140 Kisco Ave.
John L. Hettrick, chairman; Gary R.
Cypress, CA 90630 ............. (760) 343-3650 Mount Kisco, NY 10549-1407
Fornasiero, president; Patrick J. Barrett,
Email: info@wallaceinstruments.co.uk .............................................. (914) 241-7080
production manager
Instrumentation: Autoclaves, process Fax: (914) 241-7096
Wallace Website: www.zumbach.com
3 Temasek Ave. simulators
Email: sales@zumbach.com
Centennial Tower Level 34 Keith F. Donahue
Singapore 039190 ...............+65 6549 7164 Wyoming Test Fixtures, Inc.
2960 E. Millcreek Canyon Rd. Instrumentation: Non-contact diameter
Email: info@wallaceinstruments.co.uk gauges, ultrasonic, eddy current based
Salt Lake City, UT 84109..... (801) 484-5055
Fax: (801) 484-6008 wall thickness monitoring/control systems
Webber Manufacturing Co. for hose, cable jackets, tubes, pipes; bench
8498 Brookville Rd. Website: www.wyomingtestfixtures.com
Email: wtf@wyomingtestfixtures.com top diameter measuring instruments for
Indianapolis, IN 46219 ..........(317) 357-8681 QC; non-contact sheet thickness gauges;
Fax: (317) 357-8685 Donald F. Adams, president
Instrumentation: Dies, laboratory equip- OD/ID/wall monitoring, control systems
Website: www.webbermfg.com
ment, physical testing equipment, testers with color display, optical lump/neckdown
Email: info@webbermfg.com
and testing equipment, adhesion testers, detector, spark testers for cables, inductive
Dave Lovett, president
coefficient of friction testers, compression wire preheaters; SQC/SPC data acquisition
Instrumentation: Ovens, environmental
testers, cord tensile testers, creep rupture reporting, logging systems, plus PC link
chambers
testers, fatigue testers, flexing machines, networking software
Williamson impact testers, plasticity testers, shear test-
ers, tack testers, tensile tear testers, tensile Zwick of America, Inc.
70 Domino Dr.
Concord, MA 01742 .............(978) 369-9607 strength testers, tire testers, torsion testers, 2125 Barrett Park Dr., Ste. 107
Fax: (978) 369-5485 universal testers Kennesaw, GA 30144..........(770) 420-6555
Website: www.williamsonir.com Fax: (770) 420-6333
Email: sales@williamsonir.com Yxlon/Comet Technologies USA Website: www.zwick.com
W.R. Barron, vice president; T.F. Larrick, 5675 Hudson Industrial Pkwy. Email: info@zwickusa.com
technical manager Hudson, OH 44236.............(877) XRAY-100 Bill Becker, director
Instrumentation: Radiation pyrometers Fax: (234) 284-7886 Instrumentation: Materials testing instru-
Website: www.yxlon.com ments, equipment for measuring tensile,
Willrich Precision Email: yxlon@yxlon.com shear, compression, hardness, rebound,
80 Broadway Tom Swanger, account manager, tire/rub- abrasion, rheological properties

FOLLOW US ON TWITTER @rubberworld 63


"ENZ-ATERIALS4ESTING)NSTRUMENTS
!TLAS-ATERIAL4ESTING4ECHNOLOGY
4HE FOLLOWING GRID LISTS THE TYPES OF INSTRU
MENTATION AND TEST EQUIPMENT OFFERED BY
SUPPLIERS %QUIPMENT FOR TESTING RUBBER

!PPLIED4EST3YSTEMS )NC
,EVERETT!!NDERSON#O
!METEK 53'AUGE$IV
VULCANIZATES HAS BEEN BROKEN DOWN INTO
STRESSSTRAIN TESTS TIME DEPENDENT TESTS

!UTOMATION0RODUCTS
!CU 'AGE3YSTEMS

!LPHA4ECHNOLOGIES
DESTRUCTIVE TESTS DURABILITY AND ELECTRICAL

!SYLUM2ESEARCH
PROPERTIES)NSTRUMENTSANDTESTEQUIPMENT

#7"RABENDER
"ETA,ASER-IKE
"#!MES#O

!3- (ASBACH
FOR THE CHEMICAL ANALYSIS OF RAW MATERIALS

"ASLER6ISION
!CROLAB,TD
VULCANIZEDANDUNVULCANIZEDRUBBERINCLUDE

2$!BBOTT

!DMET)NC
SPECTROSCOPY CHROMATOGRAPHY THERMAL
ANALYSISANDMICROSCOPY

0ERMEABILITY s s
$URABILITY
)NSTRUMENTATIONEQUIPMENTFORTHETESTINGOFRUBBERVULCANIZATES

&LUIDRESISTANCE s s
(EATRESISTANCESTATIC s s s

(EATBUILD UP s s s s
$ESTRUCTIVE

&ATIGUE s s s s
TESTS

!BRASION s s s
#RACKANDCUTGROWTH s s s
$YNAMICTHERMOMECHANICAL s s s
4IME DEPENDENT

2EBOUNDANDRESILIENCE s s
TESTS

#REEPANDSTRESSRELAXATION s s s s
Set s s s
!DHESION s s s s s
3TRESSSTRAIN

(ARDNESS s s s s
TESTS

4EAR s s s s s
4ENSILE s s s s s
s s s
-ICROSCOPES

$IMENSIONS s s s s s s
0HYSICALTESTINGOFRUBBER

2AWMATERIALS VULCANIZEDAND s s s s s
UNVULCANIZEDRUBBERTESTING

0ROCESSABILITYTESTING s s s s s s

$ISSIPATIONFACTOR s
%LECTRICAL
PROPERTIES

$IELECTRICSTRENGTH s
$IELECTRICCONSTANT s
"RITTLENESS s s
$URABILITY

7EATHERINGRESISTANCE s
/ZONERESISTANCE s

64 RUBBERWORLD.COM ‡ JANUARY 2018


s
s
s
s
s
Brookhaven Instruments

s
CDS Analytical, Inc.

s
s
s
s
Cober, Inc.

s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
Corporate Consulting Services

s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
Dek-Tron Scientific Instruments

s
Despatch Industries

s
s
s
s
s
s
s
Dewes Gumbs Die and Presses

s
s
s
s
Dillon

s
s
Eagle Polymer Equipment

s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
Ektron Tek Co.

s
s
s
s
s
s
s
s
s
s
s
Elastocon AB

s
s
Electronic Development Labs

s
s
s Electro Standards Laboratories

s
Emerson Apparatus

s
s

Endurica, LLC

s
s
Exova

s
FISA North America

s
Forte Technology

s
s
s
s
s
s
s
s
s
s
s

Goettfert

s
s
s

Gomaplast Machinery, Inc.

s
s
s
GreCon

s
s
Hamamatsu Corporation

s
Harris Instruments

s
s
s
s

Hoto Instruments

s
s
s
s
s
s

Hydramotion

FOLLOW US ON TWITTER @rubberworld


s
s

Imada, Inc.

s
s
s
s

Imass, Inc.

65
The following grid lists the types of instru-
mentation and test equipment offered by

Mesabi Control Engineering


suppliers. Equipment for testing rubber

Indy Tech Lab Equipment

Malvern Instruments, Inc.


vulcanizates has been broken down into
stress/strain tests; time-dependent tests;

ISRA Surface Vision

J&L Tool & Machine

Leica Microsystems
Instron Corporation
destructive tests; durability and electrical

LMI Technologies
properties. Instruments and test equipment

Maag Automatik
J.M. Machinery

Mast/Keystone
for the chemical analysis of raw materials,

Malcam, Ltd.
Kokusai, Inc.
KLA-Tencor

Meeco, Inc.
vulcanized and unvulcanized rubber include
spectroscopy; chromatography; thermal

Indusco
Impakt
analysis; and microscopy.

Permeability s s
Durability
Instrumentation/equipment for the testing of rubber vulcanizates

Fluid resistance s
Heat resistance (static)
s s

Heat build-up s s
Destructive

Fatigue s s
tests

Abrasion s s

Crack and cut growth s s

Dynamic/thermomechanical s s s s s
Time-dependent

Rebound and resilience s s s


tests

Creep and stress relaxation s s s s s

Set s s s s s

Adhesion s s s
Stress/strain

Hardness s s s
tests

Tear s s s s s

Tensile s s s s s s

Microscopes s s
Dimensions s s s s s
Physical testing of rubber

Raw materials, vulcanized and s s s s s


unvulcanized rubber testing

Processability testing s s s s s s s s

Dissipation factor s
properties
Electrical

Dielectric strength s s
Dielectric constant s s
Brittleness s
Durability

Weathering resistance s
Ozone resistance s s

66 RUBBERWORLD.COM ‡ JANUARY 2018


s
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Mettler-Toledo, Inc.

s
s
s
s
Micromeritics Instrument Corporation

s
s
Micro-Vu

s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
MonTech USA

s
s
s
s
MTI Instruments

s
MTS Systems

s
s
s
NDC Infrared Engineering

s
s
s
s
s
s
s
s
s
s
s
s
s
Netzsch Instruments North America

s
Newage Testing Instruments

s
s
s
s
s
Nikon, Inc.

s
OAI (Optical Associates Inc.)

s
s
s
s
s
ODC Tooling and Molds

s
s
OHMIC Instruments

s
Olympus-NDT

s
s
Ontario Die International

s
s
s
s
s

Ontario Die International (USA)

s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s
s

Orec Ozone Chambers and Monitors

s
Oxford Instruments

s
Pacific Transducer

s
Perkin Elmer Instruments
s
s
s

Piedmont Polymer Equipment

s
PLV Systems

s
s
s
s

Polymer Machinery Company

s
s
s
s
s
s

PPD Group

s
s
Precision Quincy Ovens

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s
s
s
s
s
s

Prescott Instruments

s
s
Princo Instruments

67
PTC Instruments/PTC Metrology

Shimadzu Scientific Instruments

Sikora International Corporation


The following grid lists the types of instru-

RWC Testing & Lab Supplies


mentation and test equipment offered by

Signature Control Systems


suppliers. Equipment for testing rubber

Rockwell Automation, Inc.

Satra Technology Center


vulcanizates has been broken down into

Quest Intergrated, Inc.


stress/strain tests; time-dependent tests;

Schenck Corporation
Rex Guage Co., Inc.

TA Instruments, Inc.
Qualitest USA, LLC
destructive tests; durability and electrical

Q-Lab Corporation

Starrett Bytewise
properties. Instruments and test equipment

Taber Industries

Tavdi Co., Inc.


for the chemical analysis of raw materials,

Scanco USA
vulcanized and unvulcanized rubber include
spectroscopy; chromatography; thermal
analysis; and microscopy.

Permeability s s s s
Durability
Instrumentation/equipment for the testing of rubber vulcanizates

Fluid resistance s s s
Heat resistance (static) s s

Heat build-up s s s
Destructive

Fatigue s s s s
tests

Abrasion s s s s
Crack and cut growth s s
Dynamic/thermomechanical s s s
Time-dependent

Rebound and resilience s s s


tests

Creep and stress relaxation s s s


Set s s s s
Adhesion s
Stress/strain

Hardness s s s s s s s
tests

Tear s
Tensile s s

Microscopes s s s
Dimensions s s s s s
Physical testing of rubber

Raw materials, vulcanized and s s s s s


unvulcanized rubber testing

Processability testing s s s
Dissipation factor s
properties
Electrical

Dielectric strength s
Dielectric constant s
Brittleness s s s
Durability

Weathering resistance s s
Ozone resistance s

68 RUBBERWORLD.COM ‡ JANUARY 2018


s
Tensitron, Inc.

s
s
s
s
s
s
s
Testing Machines, Inc.

s
s
s
Testo, Inc.

s
s
s
Thermo Scientific

s
s
s
Thermotron Industries

s
s
s
s
s Thwing-Albert Instruments Co.

s
s
s
Tinius Olsen Testing Machine Co.

s
s
s
TSI Incorporated

s
s
s
s
s
s
s
U-Can

s
s
s
United Calibration Corporation

s
s
s
s
s
s
s
s

United Testing Systems

s
s
s
s
United Testing Systems, Inc.

s
s
s
Vindum Engineering, Inc.
s
s

VTEC Laboratories, Inc.

s
s
Wabash MPI

s
s
s
s
s
s
s

Wallace Instruments

s
s
Webber Manufacturing Co.

s
s
s
s
s

Williamson

s
s

Willrich Precision

s
s

Winters Instruments

s
s
s
s
s
s
s

Wyoming Test Fixtures, Inc.

FOLLOW US ON TWITTER @rubberworld


s
Carl Zeiss, Inc.

s
s
s
s

Zumbach Electronics Corp.

69
Rubber Division, ACS 2018 Courses
Elastomer Training Center in Akron, OH
Advanced Rubber Technology – February 13-15
Natural Polymers, Renewable Resources – February 27-March 1
Introduction to Compounding, Testing and Mixing of Elastomers –
rubber.org classroom March 6 & 7, tours March 8
Silicone Basics – March 8
Intro to Rubber Technology for
Training and education are essential to Non-Technologists – March 20
Molding of Rubber – March 21
maintaining a qualified workforce and for a
Introduction to Rubber Bonding – March 22
student to be competitive when searching Intermediate to Advanced Compounding and
Testing of Rubber – classroom April 10-12,
for a job in the industry. Procedures and best tours April 13

practices are continuously changing within Understanding Raw Materials, the Building Blocks
of Rubber Compounding – April 23
our industry and to stay ahead or on top of Compounding for Performance – April 24 & 25

trends, Rubber Division, ACS provides you an Solving Problems in Rubber Compounding
and Processing – April 26
opportunity to invest in your company and its Dynamic Rubber Design – May 1 & 2

future and increase the knowledge base of An Introduction to Continuous Vulcanization – May 7
An Introduction to Flexible Cellular Rubber – May 8 & 9
your employees by offering training courses
Chemistry & Technology of Polyurethane Elastomers – May 10
throughout the year. Failure Analysis of Rubber & Plastics by Physical and Chemical
Analysis – May 11
Essentials of Rubber Technology – May 14
Silicone Rubber Chemistry and Technology – May 14
Visit rubber.org/upcoming-training for Compound Mixing and Consistency – May 15
more information about these courses, Establishing a Rubber Molding Process – May 15
including full descriptions, pricing, Applied Rubber Technology – May 16 & 17
CEUs and more.
Educational Symposium during our International
Elastomer Conference in Louisville, KY
Introduction to Rubber Technology for Non-Technologists –
October 9
Essentials of Rubber Technology – October 9
Silicone Rubber Chemistry and Technology – October 9
Introduction to Bonding – October 10
Compound Mixing and Consistency – October 10
Establishing a Rubber Molding Process – October 10
Silicone Basics – October 11
Internal Mixers and Mixing Parameters – October 11
Meetings
Rubber Division offers training rubber industry, including those work-
ing in engineering, sales, administration,
Training and educational opportunities neers and managers, including a new human resources or any other non-techni-
are offered by the Rubber Division of the generation, to polymer science from a cal area, looking for a very basic, easy to
American Chemical Society throughout bio-based approach. understand introduction to the jargon of
the year. Upcoming training opportuni- s Introduction to Compounding, the rubber trade.
ties, to be held at the Elastomer Training Testing and Mixing of Elastomers (March s Molding of Rubber (March 21): This
Center in Akron, OH, will include the 6-8): This seminar will present an over- course is an introduction to one of the
following: view of compounding elastomers. Topics main processes in the industry, the form-
s Advanced Rubber Technology will include elastomers, fillers, oils/plasti- ing and vulcanization of rubber products
(February 13-15): This course will pro- cizers and curing agents. Also discussed by use of molds. After an introduction
vide professionals with an in-depth under- will be the mixing and testing of elas- to basic rubber technology, participants
standing of rubber products. In addition to tomer compounds and how to select an will explore the major variations of the
learning the science, practical topics such elastomer for a given application. molding process, which are compression,
as production-scale synthesis, character- s Silicone Basics (March 8): This transfer and injection molding.
ization, processing and curing will be cov- course will cover silicone characteristics s Introduction to Rubber Bonding
ered, along with biomedical applications and benefits, different types, how it is (March 22): This course is designed for
of rubber. made, curing, silica powders, additives, those whose operations include or will
s Natural Polymers, Renewable HCR processing and LSR differences. include the bonding of rubber compounds
Resources (February 27 - March 1): This s Introduction to Rubber Technology to solid substrates (metals, plastics, etc.)
course with a textbook strives to intro- for Non-Technologists (March 20): This wanting to learn about the chemistry,
duce, educate and inspire scientists, engi- course is geared towards those new to the mechanics and overall methods for

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Meetings
achieving and evaluating such bonds. es. Further information on these training Paper calls
Continuing Education Units are opportunities is available from Christie
awarded for those completing the cours- Robinson at crobinson@rubber.org. Rubber Division, American Chemical
Society. The Rubber Division, ACS, is
accepting abstracts for the 194th Technical
Rubber Group News FWRPG will hold a technical meeting at the
same location on April 12. Further informa-
Meeting, Student Colloquium and Poster
Session, to be held during the International
The Bourbon Trail Elastomer Group will tion is available at www.fwrpg.org.
hold its spring technical meeting April 19 The Los Angeles Rubber Group will Elastomer Conference, October 9-11 at
in Cincinnati, OH. Details are available at hold its TIPS Meeting and Casino Night the Kentucky International Convention
www.bourbontrailelastomergroup.org. February 6 at The Phoenix Club in Anaheim, Center in Louisville, KY.
The Chicago Rubber Group will hold CA. Details are available at www.tlargi.org. Symposia for the 194th Technical
the course, Basics of Rubber Technology, The Michigan Rubber Group will hold
March 13-15 at SKF Sealing Solutions in a technical meeting March 14 in Grand
Meeting will include the following: Tire
Elgin, IL. The course fee is $375 and the Rapids, MI. Details are available at www. Processing, Manufacturing and Testing
deadline to sign up is February 20. The michiganrubbergroup.com. Equipment; Heat, Fluid and Flame
CRG is also taking applications and nomi- The New England Rubber & Plastics Resistant Elastomers; Thermoplastics
nations, respectively, for the Harold Stark Group will hold its 2018 spring technical and Specialty Elastomers; Advances in
Memorial Scholarship and Robert Kann meeting on April 3. Further information is
Education Award. The deadline is March available at www.nerpg.org.
Material and Processes of Car and Truck
1. Further information is available at www. The Ohio Rubber Group will hold Tires; Aging and Stability of Rubber -
chicagorubbergroup.org. its spring technical meeting April 10 at Additives and Mechanisms; Contributed
The Fort Wayne Rubber & Plastics the Hilton Garden Inn in Twinsburg, OH. Session; Plasticizers and Processing
Group will hold a technical meeting on Details are available at www.ohiorubber- Promoters; Natural and Renewable
February 8 at Ceruti's in Fort Wayne, IN. The group.org.
Materials for Rubber; Advances in
Synthetic Elastomers; New Commercial
Developments; Nano Fillers for Rubber
Reinforcement; Rubber Testing and

Full Line of Durometers Analog / Digital


Characterization; Rubber Industry in
China; Reducing Carbon Footprint;
Rubber Friction and Abrasion; and
Standardization.
Test Block Kits The abstract deadline is April 16.
Constant Load Weights Papers are due September 10. Further
information is available from Linda
Durometer Stands McClure at (330) 595-5543; or at www.
Calibrators rubberiec.org.
Software M.R. Mold & Engineering. Silicone
Printers experts and industry leaders will convene
at LSR 2018, to be held September 11-13
Material Thickness Gauges at the Sheraton Park Hotel in Anaheim,
O-Ring Fixture Set CA, to discuss technological and scien-
tific developments and new commercial
Complies with ASTM D2240 uses for liquid silicone rubber (LSR) and
related materials. Participants will learn
Models for A, D, B, C, DO, O, OO, OOO, M about new silicone chemistry, novel pro-
cessing and manufacturing techniques,
emerging technologies, market dynamics
REX GAUGE COMPANY, INC. and new business directions for LSR.
A DIVISION OF SCHULTES PRECISION MANUFACTURING Companies interested in presenting
1250 Busch Parkway Buffalo Grove, IL 60089 a paper should submit their abstracts by
Visit our Web Site @www.rexgauge.com March 1 to Amos Golovoy at agolovoy@
gmail.com. Further informaton on the
800/927-3982 conference is available at www.executive-
LOCAL: 847/465-9009 FAX: 847/465-9229 conference.com/conferences/lsr2018/.

72 RUBBERWORLD.COM ‡ JANUARY 2018


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2018 Rubber Division, ACS Events
!.(-,,' ,!* *,,!&"$%,"& '*1'-,!"++(*"& *&
*'%0(*,+"&'-*"&-+,*1+-(('*,,! 
 !*$+''1*$"+,&
',!*'-,+,&"& /*/"&&*++,!1**' &"2'*,!"*!".%&,+
&'&,*"-,"'&+&,/'*#/",!,!+,%"&+"&,!-+"&++&%'*

193rd Technical Meeting Technical Meeting Session Topics Include:


May 8-10, 2018 4 *'*,!"$#+ '$$')-"-%*'%,*-,-*,'*'(*,"+
Indianapolis, IN, USA 4 /*&+"& *'&,*"$+
Hyatt Regency Indianapolis 4 -*!&"+," -&+,"&
1 S. Capitol Ave. 4 .&+"&1&,!+"+'$+,'%*+")-"-*+&$,,*"$+
Indianapolis, IN 46204 4 & "&*"& /",!-*
4 '&,*"-,++"'&
4 "&!&'$' 1 /*"&&*+*+&,,"'&+

Visit rubber.org for more information and to register.

-*International Elastomer Conference"+,!(*%"*($/!*


-+,'%*++-(($"*+'%,*"$+)-"(%&,,''$+&+*."+&-,'*+
'%,' ,!*!"+.&,"+,!'&($'&,"%'1*/!*1'-3&,!
+,',!+,''-*"&-+,*1$$-&*'&*''

,,!International Rubber Expo/'*.*",1'0!"",+(+"2+


October 9-11, 2018 '&'/!"!"++-*,'3,1'-*'%(&1+&+-*,,&+,$$-+,!,,!1
."+",,!0(','!$(,!%"%(*'. -+"&++$'*,'*1'(*,"'&+&
Kentucky International %&-,-*"& (*'++++/$$+$*&'-,&/,!&'$' "+&,!&")-+
Convention Center "&"&+,*-%&,,"'&)-"(%&,+',/*!*/*&&$1,"$+*."+!1
Louisville, KY $+',,&"&'**,'3&,!*" !,-+"&++(*,&*'*/!,.*,!"**''-+

Visit rubberiec.org to Industry Professionals & Students - Call for Abstracts


learn more or to secure Rubber Division, ACS is accepting abstracts for the 194th Technical
your exhibit space today! Meeting, Student Colloquium & Poster Session. Deadline is April 16th,
2018. Visit rubberiec.org to view the Technical Meeting session topics
and to submit an abstract.
Calendar For additional calendar
information click here:

Rubber Division, ACS, Introduction to Adsale Exhibition Services Ltd.,


Future Compounding, Testing and Mixing of Chinaplas 2018, National Exhibition and
Meetings/ Elastomers, Elastomer Training Center, Convention Center, Hongqiao, Shanghai,
Akron, OH, www.rubber.org/upcoming- China - www.chinaplasonline.com - April
Expos training - March 6-8. 24-27.
2018 Rubber Division, ACS, Silicone Basics, Rapid Medtech Communications
Indianapolis May 8-10 Elastomer Training Center, Akron, OH, Ltd., Med-Tech Innovation Expo: The
Louisville October 9-11 www.rubber.org/upcoming-training - Medical Technology Event, Ricoh Arena,
March 8. Coventry, U.K., www.med-techexpo.com
2019 University of Akron, Akron Polymer - April 25-26.
Cleveland October 7-10 Technology Services, Rubber Bushing
www.rubber.org Designing for Automotive and Commer-
cial Application course, Akron Polymer May
TechnoBiz, Thermoforming Thin and Training Center, Akron, OH, www.uak-
Thick Gauge, Crowne Plaza Tampa West- ron.edu/apts/ - March 13-14. International Rubber Study Group,
shore, Tampa, FL, www.plastics-industry. Chicago Rubber Group, Basics of World Rubber Summit 2018, Colombo,
org - January 24-25. Rubber Technology 2018, SKF College, Sri Lanka, www.rubberstudy.com - May
Ohio Rubber Group, technical meeting, Elgin, IL, www.chicagorubbergroup.org 7-8.
Hilton Garden Inn, Twinsburg, OH, www. - March 13-15. International Institute of Synthetic
ohiorubbergroup.org - January 30. Michigan Rubber Group, technical Rubber Producers, 59th Annual General
meeting, Grand Rapids, MI, www.michi- Meeting, Madrid, Spain, www.iisrp.com
February ganrubbergroup.com - March 14.
TechnoBiz, GRTE 2018 Global Rubber,
- May 7-10.
Plastics Industry Association, NPE
Latex & Tire Expo, Bangkok, Thailand, 2018: The Plastics Show, Orlando, FL,
Los Angeles Rubber Group, TIPS www.rubbertechnology-expo.com - www.npe.org - May 7-11.
Meeting and Casino Night, The Phoenix March 14-16. Rubber Division, American Chemical
Club, Anaheim, CA, www.tlargi.org - Rubber Division, ACS, Introduction Society, 193rd Technical Meeting, Hyatt
February 6. to Rubber Technology for Non- Regency, Indianapolis, IN, www rubber.
Association of Modified Asphalt Pro- Technologists, Elastomer Training Center, org - May 8-10.
ducers, 19th Annual AMAP Conference Akron, OH, www.rubber.org/upcoming- Chicago Rubber Group, spring techni-
& Workshop, Sheraton Grand, Phoenix, training - March 20. cal meeting, Hawk's View Country Club,
AZ, www.modifiedasphalt.org - February Rubber Division, ACS, Molding of Lake Geneva, WI, www.chicagorubber-
6-8. Rubber, Elastomer Training Center, group.org - May 14.
Fort Wayne Rubber & Plastics Group, Akron, OH, www.rubber.org/upcoming- VBRI Press, International Conference
technical meeting, Ceruti's, Fort Wayne, training - March 21. on Plastics and Rubber Technology,
IN, www.fwrpg.org - February 8. Rubber Division, ACS, Introduction Stockholm, Sweden, www.vbripress.com
University of Wisconsin - Milwaukee, to Rubber Bonding, Elastomer Training - May 14-17.
Silicone Elastomers Technology and Center, Akron, OH, www.rubber.org/ Messe Frankfurt, Techtextil North
Fabrication course, Embassy Suites, upcoming-training - March 22. America, Georgia World Congress
Anaheim, CA, www.uwm.edu/sce-rubber Center, Atlanta, GA, www.messefrank-
- February 12-15.
Rubber Division, ACS, Advanced Rub- April furt.com - May 22-24.
Urethanes Technology International,
ber Technology, Elastomer Training Cen- Utech Europe 2018, MECC, Maastricht,
ter, Akron, OH, www.rubber.org/upcom- Los Angeles Rubber Group, TIPS The Netherlands, www.utecheurope.eu -
ing-training - February 13-15. meeting and dinner, Knott's Berry Farm May 29-31.
UKIP Media & Events Ltd., Tire Hotel, Buena Park, CA, www.tlargi.org Koelnmesse GmbH, The Tire Cologne,
Technology Expo 2018, Deutsche Messe, - April 3. Northern Halls of Koelnmesse, Cologne,
Hannover, Germany, www.tiretechnolo- Ohio Rubber Group, technical meeting, Germany, www.thetire-cologne.com -
gy-expo.com - February 20-22. Hilton Garden Inn, Twinsburg, OH, www. May 29 - June 1.
Tire Industry Association, 63rd Off- ohiorubbergroup.org - April 10. Michigan Rubber Group, golf outing,
The-Road Tire Conference, Sawgrass Automated Imaging Association, AIA East Lansing, MI, www.michiganrubber-
Marriott Golf Resort, Ponte Vedra, FL, Vision Show, Hynes Convention Center, group.com - May 31.
www.tireindustry.org - February 21-24. Boston, MA, www.visionshow.org - April
Rubber Division, ACS, Natural Poly-
mers, Renewable Resources, Elastomer
10-12.
Fort Wayne Rubber & Plastics Group, June
Training Center, Akron, OH, www.rub- technical meeting, Ceruti's, Fort Wayne,
ber.org/upcoming-training - February 27 IN, www.fwrpg.org - April 12. Fort Wayne Rubber & Plastics Group,
- March 1. Institute of Scrap Recycling Industries, annual golf outing, Maxwelton Golf
ISRI Annual Convention and Exposition, Club, Syracuse, IN, www.fwrpg.org -
March Mandalay Bay Resort and Casino, Las
Vegas, NV, www.isri2018.org - April
June 14.
Fort Wayne Rubber & Plastics Group,
14-19. technical meeting, Ceruti's, Fort Wayne,
JEC Group, JEC World 2018 Inter- Bourbon Trail Elastomer Group, spring IN, www.fwrpg.org - June 14.
national Composites Show, Paris-Nord technical meeting, Cincinnati, OH, www. Ohio Rubber Group, golf outing, Yankee
Villepinte, Paris, France, www.jeccom- bourbontrailelastomergroup.org - April Run Golf Course, Brookfield Twp., OH,
posites.com - March 6-8. 19. www.ohiorubbergroup.org - June 19.

FOLLOW US ON TWITTER @rubberworld 75


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Instruments’ products are innovative, accurate, easy-to-use and reli-
able. Each represents an unparalleled investment because it is designed
with the customer in mind, delivers outstanding performance and is
backed by superior customer support.
Discovery TGA 5500, TGA 550 and TGA 55 thermogravimetric
analyzers feature an all-new system design resulting in unprecedented
performance in sensitivity, temperature control, atmosphere control
and baseline drift. At the core of every new Discovery TGA is the
exclusive TA proprietary Tru-Mass balance system, which delivers the highest sensitivity and most accurate real time weight data
in the industry. A new app-style user interface is standard with each model. The Discovery TGA measures sample weight changes
under controlled conditions of temperature, time and atmosphere. It is used to characterize the thermal stability and composition of
a wide range of materials, including polymers, elastomers, composites, pharmaceuticals, electronics and inorganics. It excels in both
research environments and production control processes.
Other products provided by TA Instruments include rheological measurement systems, microcalorimeter systems providing the
ultimate in sensitivity, ruggedness and versatility, ElectroForce mechanical testing instruments for the dynamic characterization of a
range of materials, thermal conductivity meters, flash diffusivity instruments, dilatometers, and a complete line of new instruments
for the measurement of rheological and physical properties of polymers, rubber and rubber compounds at all stages of manufacture.
If you would like your web site featured here contact your sales rep
Dennis Kennelly, dennis@rubberworld.com or Mike Dies, mike@rubberworld.com
FOLLOW US ON TWITTER @rubberworld 77
Suppliers Showcase Testing/Instruments

Thickness and weight measurement system


The Gemini full width measurement system for the web in a video format, including 3D analysis software, so that
industries is a non-traversing x-ray array measurement system defects both on the surface and within the product can be
that combines web inspection and web gauging into a sin- quickly identified for later removal. Real-time displays and
gle platform for full-width, instantaneous, alarms show defect sizes and their locations
100% product inspection and measurement for easy downstream removal. Defect infor-
without electromechanical scanners that mation is captured, categorized and saved
sample just a fraction of the total product. locally and can be exported and archived for
The Gemini system starts measuring at the further analysis.
product's surface and continues through the With instantaneous thickness and weight
entire material to construct and analyze a measurement, the Gemini FWM system
complete picture of quality. is said to offer the ultimate in high-speed
The system is a non-scanning, non-con- quality visibility without data filtering or
tact, full-width measurement array platform measurement delays, as experienced with
utilizing multiple x-ray sources and receivers. Gemini's x-ray conventional scanning equipment. Gemini's instantaneous true
technology is able to immediately detect, display and report weight or thickness measurement is processed with ultra-fast
non-visible defects that are embedded within the product using high resolution to provide insight into quality. Current applica-
high-speed, continuous measurement that can detect defects tions include rubber tires, TPO roofing and fiberglass insula-
down to <1 mm. tion. (AIS Gauging)
The system includes intuitive quality maps that show data www.aisgauging.com

Tangent delta testing Elastomer/polymer testing


Tangent of delta (tan delta) quantifies the way a material This independent elastomer and polymer testing expert is said
absorbs and returns mechanical energy. It is a measure of the to be one of the world's leading contract research organiza-
out-of-phase time relationship between an impact and the tions, providing reliable, high quality testing services to a large
resultant force transmitted to the supporting body. Materials and varied client base since 1984. The firm provides product
that show the highest phase shift, approaching 90°, have the and material testing and analysis, pharmaceutical tesing,
highest capability to dissipate energy. Tan delta is an indica- design and manufacture, failure analysis, tire testing and bio-
tion of the material's effectiveness in damping vibrations. The technology services. The organization's state-of-the-art labo-
higher the tan delta, the greater the damping coefficient, the ratories are based in the United Kingdom, with more than 80
more efficient the material will be in effectively accomplish- scientists, technologists and supporting staff available to assist
ing energy absorption and dispersal. With the installation of a customers. The testing firm also provides in-depth analysis,
load cell, the AYO-IV testing system now measures tan delta interpretation of results and solutions to customer problems.
directly in seconds. (Tavdi Company) (Rubber Consultants)
www.tavdico.com www.rubberconsultants.com

High temperature gel permeation chromatography


The most important attribute of a polymer material is said to sion chromatography (SEC). To evaluate a polymer using
be its basic chemical structure. The composition of the poly- GPC, the polymer must be soluble and is filtered to remove
mer determines basic inherent properties that can be expect- insoluble components such as fillers and additives.
ed, such as chemical compatibility, softening temperature, Many solvents are routinely used to dissolve polymer
melting temperature and mechanical properties, for example. materials. There are some polymers, polyolefins for exam-
Next in importance is said to be molecular weight and ple, that are not soluble at room temperature and therefore
molecular weight distribution. There are methods of analysis require special solvent selection and dissolution at a high
that reveal an average molecular weight. Melt flow rate, melt temperature. Conventional GPC is not an adquate technique.
flow index, membrane osmometry, end-group analysis and The company employs high-temperature gel permeation
dilute solution viscosity are a few examples. chromatography (HT-GPC) in its material testing services,
One of the most common methods used to determine the which must be employed to ensure the successful determi-
molecular weight distribution of polymers is gel permeation nation of molecular weight. (Polymer Solutions)
chromatography (GPC), which is also known as size exclu- www.polymersolutions.com

78 RUBBERWORLD.COM ‡ JANUARY 2018


Suppliers Showcase Testing/Instruments

Automated manufacturing Stress relaxation tester


The third generation ACOMP products is an automated smart The EB 21 LTHTP aging oven has four cells with individual
manufacturing system that continuously analyzes polymers control of both the air exchange rate, as well as the tempera-
during production and produces realtime insights into reaction ture. This is said to be the first oven that can offer individual
kinetics and polymer properties, including residual mono- temperature control for an oven
mer, monomer conversion, polymer composition, molecular with programmable cycling tem-
weight and intrinsic viscosity. Earlier generation ACOMPs, perature. The cooling is done with
by realitme measurement of intrinsic viscoisty and monomer tap water, and to be able to reach
conversion down to low parts per million levels, enabled a standard laboratory temperature,
customer to optimize batch cycle time by an average of 17%. the water temperature should not
Improvements to the third generation ACOMP include an exceed +18°C. Water consumption
enhanced software user interface and analytics functionality, is very low. Maximum temperature is 300°C. This enables
an upgraded detector train and new smart sensors. The newest automatic relaxation tests according to ISO 3384-B and SAE
generation ACOMP also has a higher temperature throughput J2979 where the force measurements are done at standard
which allows it to process a broader range of polymer applica- laboratory temperature, without the need to lift the jigs out
tions. (Fluence Analytics) of the oven for cooling in the ambient temperature. Now
www.fluenceanalytics.com users can test four different single samples/materials in indi-
vidual temperature cycling, in the same oven at the same time.
Analog durometer (Elastocon AB)
www.elastocon.se
The AD-100 analog durometer is said to be the ideal choice for
a wide range of durometer hardness measuring applications. Small batch mixing
The AD-100 is said to be the result of years of experience pro-
viding high quality durometers. Featuring a .79" (18 mm) footer, The MXI 1L laboratory kneader mixer has been installed at the
the AD-100 offers outstanding stability and conforms to all company's analytical laboratory to allow for higher precision
international standards, according to the company. The AD-100 and more efficient mixing of custom compounds. The mixer's
displays hardness readings on an easy-to-read analog scale cali- intermeshing rotors assist with excellent distributive, dispersive
brated in 0-100 durometer units. An optional memory pointer and reactive mixing. With these features, the mixer is said to be
holds the reading until manually reset, allowing the operator to ideal for high viscosity stocks, silica and specialty rubber goods
concentrate on the measurement task. This feature is also said to that require low temperature mixing. Utilizing laboratory-sized
be valuable when using the gauge in a position where viewing mixers is said to allow clients to accurately and cost-effectively
the dial is obstructed. (RWC Testing & Lab Supplies) perform studies on rubber compounding. (Smithers Rapra)
www.rwctesting.com www.smithersrapra.com

High-force dynamic mechanical analyzer


The ElectroForce DMA 3200 is said to combine industry- according to the manufacturer.
leading fatigue and dynamic mechanical analysis (DMA) At the heart of the DMA 3200 is the patented, friction-
technologies into a single mechanical test platform with less ElectroForce motor. With 500 N of force, it extends the
unparalleled performance, according to the manu- range of DMA experiments to much larger samples
facturer. and higher loads. It has high acceleration and is reli-
Mechanical properties are said to often be con- able enough to perform billions of fatigue cycles. It
sidered the most important of all physical proper- is the only motor in any mechanical testing system
ties of materials. These are critical to understanding with a 10-year warranty, according to the company.
material and component applications in nearly every The new platform of the DMA 3200 is said to
industry, including automotive, aerospace, medical combine the strengths of the company's DMA tech-
devices, electronics, polymers, elastomers, compos- nologies with the performance of the ElectroForce
ites and many more. DMA quantifies the modulus motor, acquired from Bose. No two instruments,
and energy loss of materials over a wide range of from any combination of vendors, can match the
temperatures, frequencies or strains. Fatigue testing DMA and fatigue performance of the 3200, accord-
provides insights on how and when materials, com- ing to the manufacturer. The system is available with
ponents or devices fail when subjected to oscillating forces multiple furnace options to accommodate standard and large
or stresses. These insights into material behavior ensure sample sizes, multiple cooling options, etc. (TA Instruments)
reliable product performance and prove out lifetime claims, www.tainstruments.com

FOLLOW US ON TWITTER @rubberworld 79


Suppliers Showcase Testing/Instruments

Test laboratory for customer testing of LIM


A testing laboratory is available for customer testing of composites molding machines for compression, transfer
LIM (liquid injection molding), compression molding and molding, laminating and trimming. The company also offers
other applications. Company presses available for testing custom engineered presses, as well as used and reconditioned
include two MicroLIM machines presses.
with a Graco #622 meter mix; a The company offers two-col-
30-ton Genesis compression press umn and four-column benchtop,
with proportional control of pres- manual and automatic hydraulic
sure and temperature; a Carver laboratory presses with clamp-
30-ton Auto Series press; A ing capacities from 12 to 48 tons.
Carver 12-ton Model C, heated The company's presses are said
and cooled; and a five-ton Sterling to be suited for various materi-
chiller. als research applications, such as
The company is said to be a plastics and elastomers, as well
leading international supplier of as for pharmaceuticals, analyti-
standard and custom presses to cal chemistry, laboratory testing,
the medical, aerospace, recreation, laminating and other applications,
automotive, education and energy including sample preparation.
markets. Applications include ASTM polymer testing, prop- (Wabash MPI/Carver)
pant crush testing, liquid silicone, and rubber, plastics and www.wabashmpi.com

Capillary rheometers Electrical resistance tester


The RH2000 series of benchtop capillary rheometers includes The EKT-2000RES electrical resistance tester method
compact systems said to be capable of most testing requirements describes the measurement of the electrical resistance between
encountered in capillary rheometry. The series is available in the wheel and the conducting surface against which the tire
both single bore or twin bore configurations, the RH2100 and is loaded. Adjustable test voltage ranges from 40 V to 5,100
RH2200, respectively. Both versions are said to incorporate V by increments of 10 or 100 V. The tester measures 270 by
many of the features and attributes found on the floor standing 250 by 180 mm. Available accessories include data viewer Pro
models (Rosand RH 7 and 10). A digital drive system is said PC software, a serial to parallel adapter, user manual, carrying
to give the RH2000 series unsurpassed speed control, accuracy case, ohm probe and a rechargeable battery. Operating tem-
and dynamic operating range. The hardware is supported by perature and humidity range from 0°C to approximately 40°C
Windows based Flowmaster software. (Malvern Instruments) at less than 80% RHD. (Ektron Tek)
www.malvern.com www.ektrontek.com

Visualization of compression molding


Compression molding is said to be a common process in tural mechanics and computational fluid dynamics, is used to
manufacturing complex composite components for industrial predict both the charge's deformation and flow behavior of
applications. Sheet molding compound (SMC), glass mat SMC, respectively.
thermoplastic (GMT) and pre-impregnated (pre-preg) are the To simulate the process, LS-Dyna, commercially avail-
most common compression molding processes used in com- able FEA software, integrated with Moldex3D can be
posite component manufacturing. However, since the rheo- applied. The initial charge's shape, temperature, stress ten-
logical properties of composite materials have both solid and sor and anisotropic material property are first computed
fluid behaviors, simulation is said to become a challenge. by LS-Dyna; then, carrying those physical properties, the
Commercial software is designed to calculate either fluid deformed charge is exported to Moldex3D to continue the
behavior or structure deformation, and those calculations are compression molding analysis. The analysis results of flow
derived from different equations. behavior and warpage show that the proposed integration
SMC, formed using the compression molding process, method can successfully simulate the complex behaviors of
can now be analyzed by integrated numerical simulation. SMC in compression molding. (CoreTech System Co., Ltd.)
The integration method, involving both computational struc- www.moldex3d.com

80 RUBBERWORLD.COM ‡ JANUARY 2018


Suppliers Showcase Testing/Instruments

Rubber testing solutions Elastomer testing systems


Rubber and polymer testing solutions featured in the com- Elastomer testing systems offered by the company include the
pany's brochure include a moving die rheometer and rubber MV Mooney viscometer, Elastograph moving die rheometer,
process analyzer, a Mooney viscometer, laboratory presses, Visco-Elastograph rubber process analyzer, a rubber capillary
sample cutters, bale cutters, laboratory information manage- rheometer, the Rheograph 120 high pressure capillary rheo-
ment systems, upgrades and rebuilds, calibration service and meter, Rubberview software, and various options. In order to
support, and systems for testing dispersion, hardness and fulfill the continuous increasing requirements regarding qual-
density, plasticity, compression set, abrasion and fatigue. The ity and consistency of rubber products, it is essential to make
extensive product range covers instruments for basic to high- a comprehensive characterization of the raw compound while
end testing applications in quality control, as well as research processing, according to the company. The most important
and development, integrated laboratory software systems, processing criteria for the final product are the flow and the
technical and calibration services, as well as world class vulcanization behavior, as well as the filling agent distribution.
application support and consulting, according to the company. While testing these characteristics there should be differences
The firm's testing solutions are engineered and manufactured among the production accompanying testing and the testing
entirely in Germany according to the highest quality standards. during the development phase; for example, to simulate appli-
Products and services are available to customers in more than cation dependent processes. The company's testing machinery
53 countries worldwide with local support and assistance. All is said to be well suited for both testing applications, and is
of the company's products are either available in standard con- said to meet industrial standards by its robust construction,
figurations, or can be adapted and built according to individual each with individual features, providing measuring reliability,
customer requests and requirements. (MonTech USA) especially in continuous operation. The company's testing sys-
www.montechusa.com tems can be configured to specific needs. (Gਸ਼ttfert)

Environmental chambers
www.goettfert.com

Environmental chambers available from the company include


environmental test chambers, a temperature humidity chamber,
climatic chamber, ozone tester/ozone chamber, rain test cham-
ber, UV test chamber, walk-in chamber, xenon test chamber,
thermal shock chamber, ball spray tester and freezing tester. The
TESTING
company's environmental chamber is designed for testing the
capability of heat endurance, cold endurance, dryness endur-
ance and humidity endurance, and is suitable for quality control
INSTRUMENTS
for such industries as electrical equipment, vehicle, chemistry,
building materials, packaging, etc. The company is said to offer
a low price guarantee, efficient logistics, high level standards,
& APPLICATIONS
TO PROVIDE GLOBALLY EFFICIENT AND EFFECTIVE CUSTOM
and centralized service and support coordination. (Qualitest)
www.worldoftest.com SOLUTIONS FOR TESTING PHYSICAL PROPERTIES

Precision material analysis


Instruments and software are designed and manufactured to
deliver advanced precision rubber and elastomeric materials
analysis for production optimization and product compliance
solutions, according to the company. The firm's ISO 9001
registered and ISO 17025 accredited instruments measure the
dynamic, physical and processability characteristics of rubber 73 MAPLEHURST AVE., PROVIDENCE, RI 02908
and polymers. Product lines include material process analyz- PH: 401.331.5650
ers, rheometers, viscometers, dispersion analyzers, density and SALES@BENZTESTERS.COM
hardness testers, physical property testers, universal testers, WWW.BENZTESTERS.COM
sample cutters and laboratory information management sys-
tems. Models offered include the Premier RPA (rubber process
analyzer), Premier Mooney viscometer, Premier moving die
rheometer, Premier high capacity automation module, MDR-C
moving die rheometer, disperGrader aView precision dispersion
testing analyzer, and more. (Alpha Technologies)
www.alpha-technologies.com

FOLLOW US ON TWITTER @rubberworld 81


Suppliers Showcase Equipment

Laser mold cleaning Rotary batch mixer


The MLC 500 by Laselec was developed by the company A rotary batch mixer with integral lump breaker is said to
in cooperation with a laser-specialized partner. The laser provide inline deagglomeration of compacted bulk materials
technology is matched to the cleaning of industrial parts and before blending batches gently with total uniformity in one to
injection and compression molds for the three minutes. Inline stacking of the low profile De-Clumper
rubber and polymer processing markets. model RDC-1515-SS atop the stationary inlet of the Model
This environmentally-friendly ecological 700-TH-50-SS mixer is said to minimize headroom require-
solution is said to guarantee a safe, opti- ments, while eliminating the need for flexible connections or
mal, quick and reproducible cleaning with hard piping between the units. Material entering the system
low operating costs. The operator simply is de-lumped by dual rotors with three-point, single-piece,
loads the mold, clicks the start button and stainless steel breaking heads rotating with minimum clear-
the machine does the job. The company is ance inside a curved, perforated bed screen. The synchronized
a global manufacturer of rubber injection molding machines shafts rotate at 120 rpm to prevent heating and degrading of the
and related equipment. (Rep) product. One-size material passes through bed screen apertures
www.repinjection.com which range from 1/16" to 2-1/2" (25 to 64 mm) in diameter,
immediately prior to entering the stationary inlet of the mixer.
Planetary mixer for testing As the mixer's horizontal drum rotates, proprietary mixing
flights tumble, turn, cut and fold the material, imparting mini-
The company's testing facility for the specialty mixing indus- mal energy to the batch, minimizing or eliminating degrada-
try has added an advanced planetary mixer now available for tion, according to the manufacturer. (Munson Machinery)
no-charge demonstrations. The four-gallon planetary dual www.munsonmachinery.com
disperser (Model PDDM-4) is equipped with two high viscos-
ity blades and two high speed dispersers. All four agitators Rubber post-curing oven
rotate on their own axes while orbiting the vessel, ensuring
rapid powder wet-out and deagglomeration. It is designed for The No. 860 is a 500°F (260°C) truck oven, currently used for
vacuum operation and includes a jacketed mix vessel. The post-cure of rubber parts at the customer's facility. Workspace
mixer is said to be ideal for mixing thick slurries and highly- dimensions of this oven measure 36" wide by 36" deep by
filled pastes, and delivers excellent dispersion and uniformity 60" high. Nichrome wire heating elements
throughout a wide viscosity range up to around 2 million cen- with 34.8 kW installed heat the workspace,
tipoise, according to the company. The PDDM-4 is one of while a 2,000 cfm, 2 hp recirculating blow-
over 40 mixers and blenders showcased in the company's test er provides horizontal airflow to the work-
and development center. (Charles Ross & Son) load. This truck oven features 4" insulated
www.mixers.com walls, a top-mounted heat chamber, an
aluminized steel interior and exterior, plus
double doors front and rear. Other features
For additional equipment include safety equipment for handling
information click here flammable solvents, including explosion venting door hardware
http://www.rubberworld.com/equipment and a 325 cfm powered forced exhauster. Controls on the No.
860 include a digital indicating temperature controller and a 10"
diameter circular chart recorder. (Grieve)
www.grievecorp.com

Shot peening machine


A precise shot peeing machine was completed for a cus-
tomer in the automotive/marine industry. This small footprint
machine is equipped with a spiral separator (media shape
separator) to ensure that the S-70 mil spec media are the cor-
rect spec shape to guarantee the intensity that is required to
adhere to AMS-2431/2E. In unison with the spiral separator,
a 24" vibrating screen classifier and 75/12 cyclone reclaimer
are used. There is a total of six suction blast guns, with two
utilizing individual pressure regulators. The custom fixture
incorporates a spring load feature that allows for seamless
loading/unloading. (Guyson)
www.guyson.com

82 RUBBERWORLD.COM ‡ JANUARY 2018


Materials

Liquid rubber for EPDM


Several liquid rubber grades that are suitable for EPDM
peroxide curing applications have been developed by the
company. Specifically, substituting LBR-361 for TAC as a
coagent will offer similar mechanical properties while reduc-
ing volatile organic compound (VOC) content, according to
the company. Possible applications include plumbing compo-
nents, since the company's liquid rubber/EPDM compounds
can meet local drinking water regulations. Also, LBR-361 is
said to improve compression set, which is beneficial for rub-
ber compounds used to produce automotive parts, hoses, etc.
LBR-361 is said to provide the optimum soft-elasticity ratio
described by hardness versus compression set. (Kuraray)
www.kuraray.com

Butadiene/acrylonitrile
Paracril NBR powder is supplied by the company. Nitrile rubber
is a polar elastomer that can be blended with other elastomers
and thermoplastics. The predominant thermoplastic blend with
NBR is with PVC. These two polymers form a miscible blend
which imparts ozone resistance to the NBR and flexibility to
the PVC. The NBR acts as a high molecular weight plasticizer
to replace the normal monomeric plasticizer used in PVC com-
pounds. This benefits the oil resistance, fuel resistance, tear
strength, abrasion and flex resistance, according to the company.
Since the NBR is not extractable versus the fugitive monomeric
plasticizer, it will remain after heat aging, oil and fuel immersion,
yielding better aged properties and low temperature performance
after aging. The lower level of monomeric plasticizer also is said
to reduce cracking of adjacent thermoplastics due to migration of
the monomeric plasticizer to the thermoplastic, which swells the
plastic, causing crazing. NBR powder is used in friction products
such as brake pads and clutch discs. (Dynasol Group)
www.dynasol.com

Polybutene products
Indopol polybutenes are non-drying synthetic hydrocarbon
polymers made by polymerization of C4 olefins (primarily
isobutene), and are available in a wide range of viscosities. By
controlling the polymerization conditions, polymer chains of
varying length are manufactured providing polybutene grades
with a unique set of physical properties, according to the com-
pany. Short chain-length polybutenes are characterized as low
viscosity fluids with free-flowing oil-like properties; medium
chain-length polybutenes are sticky with a honey-like consis-
tency; while those with the longest chain length are very tacky,
semi-solid materials. (Ineos Oligomers)
www.ineosoligomers.com

For additional materials


information click here
http://www.rubberworld.com/materials

FOLLOW US ON TWITTER @rubberworld 83


People in the News
Barna named president of Yokohama Tire
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America. Shinichi Takimoto, also a Yo- Jeff Barna Heiko Kasper Michael Spath Damien Harmon
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0H[LFR6GH5/GH&9 curement and supply chain management VXEVLGLDU\(QJHO,WDOLD
platform for precision parts production. Randy Breaux was promoted to
MANAGEMENT executive vice president of marketing,

BBG, a manufacturer of molds, machin-


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ery and systems, has changed the struc- Bruce Besancon was named vice presi- repair and operation replacement parts.
ture and management of its mold making GHQW RI R൵WKHURDG 275  VDOHV IRU Kevin Storer was promoted to execu-
division to enable international growth. <RNRKDPD 7LUH Dan Funkhouser was tive vice president of U.S. operations and
Heiko Kasper is the head of the mold promoted to vice president of commer- SUHVLGHQWRI0L0H[LFRDQGZLOOPDLQ-
PDNLQJGLYLVLRQ.DVSHULVVXSSRUWHGE\ cial sales. Larry Kull has accepted the WDLQ UHVSRQVLELOLW\ IRU DOO ¿HOG EUDQFK
Michael Spath, who has taken on the role of vice president of consumer sales VDOHV LQ WKH 8QLWHG 6WDWHV DQG 0H[LFR
role of head of the mold manufacturing IRU<RNRKDPD7LUH Andrew Zeisser is Mark Stoneburner was promoted to
department. QRZYLFHSUHVLGHQWRI2(0VDOHVIRUWKH senior vice president of industry seg-
 9\VWDU WKH FUHDWRU RI 9\WH[ QDWXUDO company. Fardad Nikman was promot- ments and business development.
rubber latex, appointed Steven Rotman ed to senior director of consumer product
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of the board of directors. William Doyle,
planning and product marketing for Yo-
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9\VWDU¶V SUHYLRXV &(2 DQG FKDLUPDQ Jim McCrary KDV MRLQHG 7DKRPD 0HVQDF&KLQDDQQRXQFHGWKHUHWLUHPHQW
ZLOO UHPDLQ ZLWK 9\VWDU DV D SURGXFW 5XEEHUDQG3ODVWLFVDVVDOHVPDQDJHUIRU of P. David JonesDVSUHVLGHQWRI0HVQDF
development consultant and has relin- the company. Americas Ltd. Jones spent 50 years in
quished his seat on the board of directors. LaTres Jarrett was named director the tire industry in a variety of leadership
Damien Harmon was named presi- of marketing, Bandag, for Bridgestone positions in several countries, including
GHQW*&57LUHV 6HUYLFHIRU%ULGJH- Americas. Bridgestone’s Bandag busi- (XURSH &HQWUDO $PHULFD WKH )DU (DVW
stone Americas. Harmon succeeds John ness is dedicated to the research, devel- DQG1RUWK$PHULFD+HMRLQHG0HVQDFLQ
Vasuta, who was named senior vice opment and manufacturing of premium 2011 following the acquisition of Wyko
president, global sales, Firestone Build- retreads. 7LUH7HFKQRORJ\ZKLFKDWWKDWWLPHZDV
LQJ3URGXFWV Matteo Terragni is taking over the jointly owned by Jones and Ian Smith.
Gordon Kropp and Stephen Co-
burn have joined the supply chain and
customer service team of Sea-Land
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and customer service specialist, respec-
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employee-owned distributor of specialty
chemicals.
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M. Moricz and Steven Sprague have Dan Funkhouser LaTres Jarrett Matteo Terragni Randy Breaux
been named advisory board members Yokohama Tire Bridgestone/Bandag Engel Italia Motion Industries

84 RUBBERWORLD.COM ‡ JANUARY 2018


People in the News
The Tire Industry Association an-
nounced that senior technical consultant,
Marvin BozarthZLOOR൶FLDOO\UHWLUHDW
WKH XSFRPLQJ  2൵7KH5RDG 7LUH
Conference next month. Bozarth has
been with TIA since 1990 and has served
as the executive director of the American
Retreaders Association and International
Tire and Rubber Association from 1991- Kevin Storer Mark Stoneburner P. David Jones Bruno Pary
2002. Motion Industries Motion Industries Mesnac Americas IISRP

ASSOCIATIONS one of its outstanding leaders at its next tor. Among the most promising technolo-
Annual General Meeting (AGM). Bruno gies is the 3D Dandelion project, dealing
Anne Forristall Luke, president and Pary, retired from ExxonMobil, will with the industrialization of alternative
CEO of the U.S. Tire Manufacturers As- be the recipient of the prestigious Gen- natural rubber production.
sociation, has been elected to serve on eral Award, to be presented during the Steve Maguire, founder of Maguire
the National Association of Manufactur- IISRP’s 59th AGM in Madrid, Spain, Products, has been elected to the Plas-
ers’ (NAM) Council of Manufacturing during the week of May 7. Pary has had tics Hall of Fame. Maguire Products
Association’s (CMA) board of direc- a successful career of more than 35 years was founded in 1977, when Maguire
tors. Made up of more than 260 industry in the synthetic rubber industry, as well SURGXFHG DQG PDUNHWHG KLV ¿UVW LQYHQ-
VSHFL¿F PDQXIDFWXULQJ DVVRFLDWLRQV WKH as being a promoter of its growth and de- tion, a peristaltic pump for dispensing
CMA is said to be a powerful assembly velopment. Pary is a chemical engineer liquid colors. Since then, Maguire has
of manufacturers and a vital arm of the (Lyon), earned a doctorate in polymers R൵HUHGWKH¿UVWJUDYLPHWULFZHLJKVFDOH
NAM. The CMA’s mission is improving at the Pierre and Marie Curie University EOHQGHU WKH ¿UVW XVH RI PLFURSURFHVVRU
the competitiveness of manufacturers in (Paris), and a business degree from the control for plastics auxiliary equipment,
the United States. IAE Paris. Pary is currently an Interna- WKH ¿UVW YDFXXPUHVLQ GU\HUIRUSODVWLFV
tional Fellow of the University of Akron processors, etc. The Maguire weigh scale
AWARDS Research Foundation. In this position, he blender was introduced in 1989 as the
supports a number of initiatives aimed at ¿UVWD൵RUGDEOHDQGHDV\WRRSHUDWHV\V-
The International Institute of Synthetic the commercialization of technologies tem for precisely controlling the compo-
Rubber Producers (IISRP) will honor developed in the Ohio Business Incuba- sition of a raw material blend.

Visit Us At The Show


July 2-5, 2018, the international rubber and
elastomer industry will meet for the
German Rubber Conference DKT 2018 in
Nuremberg.

FOLLOW US ON TWITTER @rubberworld 85


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UXEEHUÀRRULQJSURGXFWV7KH&RPSDQ\SURYLGHVDUDQJHRIUXEEHU
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the Chemical
%LGVWRSXUFKDVHWKHDVVHWVDUHGXHRQ0DUFK Resistance Guide for
If you are interested, contact Charles Deutchman Elastomers. Buy
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RU  IRUIXUWKHULQIRUPDWLRQ
Magazine’s

Blue Book
Materials, compounding ingredients, machinery and services for the rubber industry.
RUBBER
RED
Celebrating 129 years of service to the worldwide rubber industry A Lippincott and Peto Publication
BOOK
A Lippincott & Peto Publication

86 RUBBERWORLD.COM ‡ JANUARY 2018


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FOLLOW US ON TWITTER @rubberworld 87


Index To Advertisers
3N International, Inc. (www.3ninc.com) .............................................................87 Imerys Graphite & Carbon (www.imerys-graphite-carbon.com) ..................88e
AGC Chemicals Americas (www.agcchem.com) ...........................................87 Interbusiness USA, Inc. (www.interbusinessgroup.com) ...................... 87, 88a
AirBoss Rubber Compounding Kenrich (www.4kenrich.com) ............................................................................86
(www.airbossofamerica.com) ............................................................. 2nd cover Lianda (www.liandacorp.com) ...........................................................................73
Akron Rubber Development Laboratory, Inc. LM Containers (www.lmcontainers.com).........................................................87
(ARDL) (www.ardl.com) ......................................................................................45 Marvel Consultants (www.marvelconsultants.com) .........................................87
Allchem (www.allchem-inc.com) .........................................................................87 Mesgo Compounding Solutions (www.mesgo.it) ..................................86 , 88h
APV Engineered Coatings (www.apvcoatings.com) .............................. 87, 88b McLube, Division of McGee Industries (www.mclube.com) ................ 87, 88d
Benz (www.benztesters.com) ........................................................................81, 86 Micro Poise Measurement Systems (www.micropoise.com) ..........................6
Cober Microwave (www.cober.com) ......................................................................86 MonTech (www.montechusa.com) ...................................................................19
Corporate Consulting, Service & Instruments, Inc. Nerpco USA LLC (www.nerpcousa.com) .........................................................18
(www.ccsi-inc.com) ..........................................................................................83 Polymerics (www.polymerics.com) ....................................................................87
Denka Performance Elastomer LLC (sales@denka-pe.com) ...................... 86 Qualitest (www.worldoftest.com) ........................................................................8
Elastocon (www.elastocon.com) ......................................................................82 Release Coatings of New York, Inc. (www.rcony.com) ..................................87
Endurica (www.endurica.com) ..........................................................................20 REP (www.repinjection.com) ................................................................................87
Gerlach Inc. (www.gerlachinc.com) ..................................................................85 Rex Gauge Company, Inc. (www.rexgauge.com) ................................... 72, 76
Gomaplast Machinery, Inc. (www.gomaplast.com)..........................................21 Rubber Division, ACS (www.rubber.org) ......................................................70, 74
H&R Group US, Inc. (www.hur.com) ...................................................... 4th cover Shared Management Resources, Ltd. (www.shrmgtres.com) .....................86
Harwick Standard Distribution (www.harwick.com) ...................................... 13 Smithers Rapra (www.smithersrapra.com) .....................................................77
HB Chemical (www.hbchemical.com) ....................................................... 7, 9, 71 Sprinter Marking (www.sprintermarking.com) ..........................................87, 88c
Holly Frontier Lubricants & Specialty Products Starrett Bytewise (www.starrett.com/bytewise) ........................................ 10, 11
(www.hollyfrontierlsp.com) .................................................................................. 2 Struktol Company of America (www.struktol.com) ............................................1
Hoosier Custom Manufacturing TA Instruments (www.tainstruments.com) .........................................15, 77, 88f
(www.hoosiertirecustommfg.com) ......................................................................86 TechnoBiz (www.technobiz-asia.com) ...........................................85, 3rd cover
Hotlinks Directory (www.rubberworld.com) ................................................76, 77 Vanderbilt Chemicals (www.vanderbiltchemicals.com) .................................88g
Hoto Instruments (www.hoto-instruments.com) ................................................87 VMI (www.vmi-group.com) .....................................................................................5

Rubber World
SALES STAFF
DENNIS J. KENNELLY UTPAL PAUL
Senior VP-Associate Publisher 203, Dheeraj Gaurave Heights-I
1741 Akron-Peninsula Rd. New Link Road, Andheri-West,
Akron, OH 44313-5157 Mumbai (Bombay) - 400053, India
Ph: 330-864-2122 - Fx: 330-864-5298 Ph: 91-22-26744747 - Mobile: 91-9892614102
Email: dennis@rubberworld.com Email: u_paul2002@yahoo.co.in

MIKE DIES RINGIER TRADE PUBLISHING


Sales Representative East China - VIVIAN SHANG
1741 Akron-Peninsula Rd. Phone: +86-21 6289-5533 EXT 169
Akron, OH 44313-5157 vivian@ringiertrade.com
Ph: 330-864-2122 - Fx: 330-864-5298
Email: mike@rubberworld.com North China and South China - MAGGIE LIU
Phone: +86-20 8732-3316 EXT 9332
ANDRE JAMAR maggieliu@ringiertrade.com
International Marketing Consultant
Avenue Nicolai 49 A / Bte 4 Hong Kong - MIKE HAY
4802 Heusy Phone: +852 2369 8788 ext 11
Belgium mchhay@ringier.com.hk
Ph: +32(0)-87-225385 Taiwan - KELLY WONG
Mobile: + 32(0)-496-510513 Phone: +886 4 2329 7318
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88 RUBBERWORLD.COM • JANUARY 2018


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Rubber World full page 7x10.indd 1 7/9/15 1:39 PM


TechnoBiz TRAINING
RUBBER TECHNOLOGY Calendar 2018
WWW.RUBBER-INDUSTRY.ORG

Date Training Topic Location Date Training Topic Location

DEUTSCHE Kautschuk-Technik Trainings Woche 2018 5-7 June 18 Rubber Compounding & Processing Vienna,
Instructor: Dr. Hans-Joachim Graf Language: English Austria
5-6 Feb 18 Mischungsentwicklung und Verarbeitung von
Elastomeren: Vom Auftrag bis zum Produkt.
Instructor: Dr. Hans-Joachim Graf Language: German
24-25 July 18 Rubber Mixing and Property Improvement
Instructor: Prof. Robert Schuster Language: English Dallas,
5 Feb 18 Moderne Klebstoffe und Ihre Anwendung Texas, USA
26 July 18 Rubber Reinforcement with Fillers
Instructor: Dr. Juergen Finter Language: German
Instructor: Prof. Robert Schuster Language: English
6 Feb 18 Die Vulkanisation und Vulkanisations- Mechanismen. Schlüchtern,
Instructor: Prof. Robert Schuster Language: Germany 3-4 Sept 18 Rubber Vulcanization - Science and Practice
7 Feb 18 Versuchsplan - Technik in Material- Entwicklung Instructor: Prof. Robert Schuster Language: English Ann Arbor,
5-7 Sept 18 Rubber Compounding & Processing Michigan,
und Fertigung von Gummi. USA
Instructor: Hans-Joachim Graf Language: German Instructor: Dr. Hans-Joachim Graf Language: English
7 Feb 18 Verstärkung von Elastomeren mit Füllstoffen 6-7 Sept 18 Rubber Engineering and Product Failure Analysis Kuala Lumpur,
Instructor: Robert Schuster Language: German Instructor: Karthik Srinivas Language: English Malaysia
12-14 Feb 18 Compression Molding of Rubber
Instructor: Van Walworth Language: English Bengaluru, Europe Rubber Processing Training Week 2018
12-14 Feb 18 Tyre Technology India 8-9 Oct 18 Rubber Compounding Principles
Instructor: Dr. Majumdar & V. Rao Language: English Instructor: Dr. Hans-Joachim Graf Language: English
10 Oct 18 Rubber Compound Formulation – Optimization &
GRTE 2018 – Rubber Technology Courses Case Studies
Instructor: Dr. Hans-Joachim Graf Language: English
13-15 Mar 18 Applied Rubber Technology
Instructor: Thailand Rubber Experts Language: Thai 11 Oct 18 Practical Rubber Rheology Strassburg,
13 Mar 18 Rubber Reinforcement with Carbon Black and Silica
Instructor: TBC Language: English France
Instructor: Prof. Robert Schuster Language: English 11 Oct 18 Rubber to Metal Bonding
Instructor: Dr. Hans-Joachim Graf Language: English
13 Mar 18 Rubber Compounding Formulation - Case Studies
Instructor: Dr. Hans-Joachim Graf Language: English 12 Oct 18 Rubber Extrusion
Instructor: TBC Language: English
13 Mar 18 Reverse Engineering and Life Prediction of Rubber
Products 12 Oct 18 Rubber Injection Molding
Instructor: Dr. Raj Kumar Language: English Instructor: Dr. Hans-Joachim Graf Language: English

13 Mar 18 Compression Rubber Molding


Instructor: Van Walworth Language: English Africa Rubber Processing Training Week 2018
14 Mar 18 Rubber Vulcanization - Science and Practice Bangkok, 19 Nov 18 Rubber Compounding Principles
Instructor: Prof. Robert Schuster Language: English Thailand Instructor: Dr. Hans-Joachim Graf Language: English
15 Mar 18 Rubber Testing & Quality Control for Process 19 Nov 18 Rubber Vulcanization - Science and Practice
Improvement Instructor: Prof. Robert Schuster Language: English
15 Mar 18 Instructor: Prof. Robert Schuster Language: English 19 Nov 18 Rubber Technology for Non-Technologists Johannesburg,
Physical and Chemical Testing of Rubber Products Instructor: Terry Chapin Language: English
South Africa
15 Mar 18 Instructor: Dr. Raj Kumar Language: English 20 Nov 18 Rubber Testing and Quality Control
Applied Latex Technology Instructor: Prof. Robert Schuster Language: English
15 Mar 18 Instructor: Prof. CC Ho Language: English 20 Nov 18 Rubber Molding Technology
Rubber Injection Molding Instructor: Terry Chapin Language: English
16 Mar 18 Instructor: Van Walworth Language: English 21 Nov 18 Rubber Reinforcement with Fillers
Specialty Rubbers Instructor: Prof. Robert Schuster Language: English
16 Mar 18 Instructor: Prof. Robert Schuster Language: English 21 Nov 18 Master Class for Rubber Chemists
Rubber Extrusion Instructor: Dr. Hans-Joachim Graf Language: English
16 Mar 18 Instructor: Dr. Hans-Joachim Graf Language: English
Specialized Rubber Mold Design Techniques India Rubber Processing Training Week 2018
Instructor: Van Walworth Language: English
3 Dec 17 Synthetic Rubbers - Types, Properties and Selection
16-18 Apr 18 Rubber Compounding & Processing Jakarta, Instructor: Dr. Samir Majumdar Language: English
Instructor: Hans-Joachim Graf Language: English Indonesia 4 Dec 17 Rubber Chemicals – Types, Properties and Selection
Instructor: Dr. Samir Majumdar Language: English Bengaluru,
15-16 May 18 Rubber Vulcanization - Science and Practice Kraków, India
5 Dec 17 EPDM Compounding & Processing
Instructor: Prof. Robert Schuster Language: English Poland Instructor: Dr. Samir Majumdar Language: English
28-29 May 18 Rubber Mixing and Property Improvement Hiedelberg, 6-7 Dec17 Rubber Injection Molding
Instructor: Prof. Robert Schuster Language: English Germany Instructor: Van Walworth Language: English

Contact Address 2521/27, Lardprao Road, Khlongchaokhunsingha


Wangthonglang, Bangkok 10310 Thailand
Peram Prasada Rao, Executive Director Tel: +66-2-933 0077 WHATSAPP / LINE / WECHAT:
TechnoBiz Communications Co., Ltd. Fax: +66-2-955 9971 +66-89-489 0525
Email: peram@technobiz-asia.com
Web: www.technobiz-group.com
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