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Measurement 44 (2011) 2129–2137

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Measurement
journal homepage: www.elsevier.com/locate/measurement

Mechanics analysis and simulation of material Brinell


hardness measurement
Ge Leyi a, Zhao Wei a, Zhou Jing b, Huang Songling a,⇑
a
Department of Electrical Engineering, Tsinghua University, Beijing 100084, China
b
Center for Information Science, Peking University, Beijing 100871, China

a r t i c l e i n f o a b s t r a c t

Article history: Material Brinell hardness values are usually measured by force loading Brinell hardness
Received 31 August 2010 testers. In this paper, firstly, based on experiment data and theoretical analysis, not only
Received in revised form 15 July 2011 the relationship between Brinell hardness and mechanical properties of the measured
Accepted 29 July 2011
material is discussed, but also all measurement uncertainty sources are precisely cali-
Available online 11 August 2011
brated. Secondly, force loading characteristics of the Brinell hardness measurement are
described and a finite element analysis for the whole Brinell hardness measurement
Keywords:
process is introduced. Thirdly, to acquire theoretical measurement uncertainties and the
Measurement uncertainty
Displacement error
reliable Brinell hardness values of the material under analysis, Monte Carlo method is
Finite element analysis applied to simulate Brinell hardness experiments. At last, several sets of experiments are
Monte Carlo method carried out on HB-3000C, the Brinell hardness results acquired by this proposed novel
Indentation mechanics analysis method and practical experiments shown to be consistent, and the
validity of the proposed method is attained.
Ó 2011 Elsevier Ltd. All rights reserved.

1. Introduction The relationship between material Brinell hardness and


material stress–strain behaviors has been extensively
Mechanical hardness testing is fundamental in the eval- studied. Both ISO/TR 10108 and GB/T 1172-1999 (Chinese
uation of the mechanical properties of metallic materials national standard) have elaborated a conversion of hard-
[1]. In recent years, the related researches of Brinell hard- ness values and tensile strength values for steel [1,2]. In
ness measurement have been extensively made, and some 2007, Janosec used the same strip steel as the measured
new measurement methods are presented, such as ultra- material both in a tensile test and a Brinell hardness test.
sonic Brinell hardness measurement and electromagnetic He gained the results of Brinell hardness, yield stress, ten-
Brinell hardness measurement. However, because of its sile strength and their ratio at the room temperature,
high precision, the force loading Brinell hardness measure- respectively [3]. In 2008, Tien discovered that the relation-
ment is still currently the most authoritative measurement ship between the tensile strength and Brinell hardness va-
method in the measurement community. Using different lue of a material is very intensive [4].
force loading modes such as weight loading, hydraulic Uncertainty evaluation of material Brinell hardness
loading, lever loading or linear motor loading, Brinell hard- measurement is usually a difficult problem. A probability
ness tester applies a rated stress to the surface of the mea- and statistics methodology (type A method of ‘‘Guide to
sured material, and then survey crew measure the the expression of uncertainty in measurement’’ [5]) is
diameter of corresponding indentation and calculate the often used to evaluate the measurement uncertainty, for
material Brinell hardness based on mechanical equations. example, in 2005, Herrmanzinn synthesized the uncer-
tainty of hardness measurements according to the error
propagation law [6]. Different from the conventional meth-
⇑ Corresponding author. od above, some new uncertainty evaluation methods have
E-mail address: Huangsling@tsinghua.edu.cn (H. Songling). been developed: Roberts applied Neural Network theory to

0263-2241/$ - see front matter Ó 2011 Elsevier Ltd. All rights reserved.
doi:10.1016/j.measurement.2011.07.024
2130 G. Leyi et al. / Measurement 44 (2011) 2129–2137

analyze Brinell hardness measurement results [7], Xia ap- (6) Get material Brinell hardness and measurement
plied Fuzzy theory to evaluating the material Brinell hard- uncertainty by a statistical analysis for the results
ness measurement uncertainty [8], Ge applied Grey System of step 5.
theory to uncertainty evaluation for a general hardness (7) Verify the stress got in the step 3 and Brinell hard-
measurement [9]. Leire carried out a complete study of ness measurement results got in the step 6 by prac-
the uncertainty components in direct emissivity determi- tical Brinell hardness measurements, and validate
nation [10]. Monti addressed the evaluation of dynamic this mechanics analysis method.
uncertainty in dynamic measurements via polynomial
chaos theory (PCT) [11]. In Section 2 of this paper, we discussed several factors:
Many recent studies have focused on material Brinell Brinell hardness measurement principle, Brinell hardness
hardness measurement process. Fazil established an ana- measurement uncertainty components, stress–strain char-
lytical relation between hardness and effective strain in- acteristics of the measured material, relationship between
duced in a metal during cold working. He hold that for stress–strain characteristics and Brinell hardness, force
each of the two most commonly used measures of indenta- load characteristics of Brinell hardness measurement.
tion hardness, Vickers’ and Brinell’s, a separate analytical These factors should be considered in the process of finite
relation was proposed relying on the previous empirical element analysis of Brinell hardness measurement. In Sec-
and numerical studies, the results of the analytical models tion 3, a specific example was used to prove the novel
compared well with the data obtained from the practical mechanics analysis and simulation method proposed. In
experiments [12]. Rosenberger developed a finite element Section 4, principle of this Brinell hardness measurement
model to quantify the effect of the depth and diameter of mechanics analysis and simulation method was
the reinforcement in the hardness number of metal matrix summarized.
composite [13]. Filho et al. have shown that the semi-auto-
matic measurement of Brinell hardness by computational 2. Mechanics analysis and simulation of Brinell
approach is easier, faster, and less dependent on the oper- hardness measurement
ator’s subjectivity [14].
In this paper, the whole Brinell hardness measurement 2.1. Brinell hardness measurement principle
process was discussed from viewpoint of theoretical
mechanics. At first, a universal material testing machine The hardness of forged steel, cast steel, cast iron, non-
was employed to acquire material stress–strain character- ferrous and nonmetallic materials is usually measured by
istics, then, indentation depth and diameter by finite ele- force loading Brinell hardness testers. Namely, under some
ment analysis were calculated; in order to get the most experimental conditions, engineers and technicians apply
reliable Brinell hardness results and evaluate the practical a normal force load F on the surface of measured material,
measurement uncertainty, the main measurement influ- after a force holding time, unloading the material, they use
encing factors such as all error sources and external condi- the average stress of the indentation spherical surface area
tions were calibrated by other high precision instruments, as the Brinell hardness value of the measured material. The
and the practical Brinell hardness measurement process ideal Brinell hardness measurement principle can be de-
was simulated by Monte Carlo method. This novel method scribed in Fig. 2.
consists of the following seven steps, as described in Fig. 1: HB expresses the Brinell hardness measured value:
  qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
(1) Acquire the stress–strain characteristics of the mea-
sured material. We should use authoritative mate-
HB ¼ 0:102  2F pD D  D2  d2 ð1Þ
rial properties data directly or experimentize in a
material testing machine. where units of the F, the D and the d are N, mm and mm,
(2) Make some quantitative analysis for the main Brinell respectively. Let us define HB0 to be the true Brinell hard-
hardness measurement conditions such as tempera- ness value, then the error of Brinell hardness measurement
ture, force holding time, force value. result is
(3) Use the results of step 1 and step 2 to make a finite DHB ¼ HB  HB0 ð2Þ
element analysis for the whole measurement pro-
cess. The analysis should base on material Brinell
hardness measurement principle. In this step, maxi- 2.2. Brinell hardness measurement uncertainty analysis
mum stress, minimum stress, indentation diameter
and indentation depth can be calculated by The sources affecting the final Brinell hardness mea-
computer. surement uncertainty include measurement error of the
(4) Calibrate all the types and distribution intervals of indentation diameter, force load error, measurement er-
measurement error sources. ror of the indenter diameter, hardness measurement
(5) Generate random numbers to simulate all measure- long term stability error, the surface quality of the
ment error sources according to Monte Carlo sample. All these sources should be calibrated by
method, we set initial values for practical measure- experiments.
ment environmental variables, and then carry out
simulation calculations for the whole Brinell hard- (1) Measurement uncertainty U1 resulted from the mea-
ness measurement process many times. surement error of the indentation diameter.
G. Leyi et al. / Measurement 44 (2011) 2129–2137 2131

Stress-strain
Maximum stress
characteristics of the
measured material Finite element analysis Minimum stress
for the whole
Quantitative analysises
measurement process
of the measurement Indentation diameter
conditions
Indentation depth

Material
Brinell hardness Statistical Monte Carlo Stress
analysis simulation verification
Measurement
uncertainty
Calibrate all
measurement error sources

Measurement Practical Brinell


result verification hardness measurement

Fig. 1. Mechanics analysis principle of material Brinell hardness measurement.

Fig. 2. Ideal Brinell hardness measurement principle. F is the force load, d Fig. 3. Indentation of Brinell hardness measurement.
is the indentation diameter, / is the indentation angle, and D is the
indenter diameter.

Usually, there are some convexes in the indentation


edges of the measured material surface after force unload- Initial Position
ing [15,16], as described in the yellow area1 of Figs. 3 and 4. Indenter
These convexes often result in actual indentation diam- Force holding Position
eter slightly larger than the ideal one, and lead to a nega- Surface of the measured material
tive deviation of Brinell hardness. The convexity of
different measured material is different significantly. Convex
R
The measurement error of the indentation diameter R1
usually includes displacement error of microscope workta-
ble and eye’s error in aiming at measuring indentation. Fig. 4. Indentation generation. R is ideal indentation radius, R = d/2, R1 is
the actual indentation radius.

1
For interpretation of color in Figs. 3, 4, 7–10, the reader is referred to
(1) Measurement uncertainty u2 resulted from the error
the web version of this article. of the force load.
2132 G. Leyi et al. / Measurement 44 (2011) 2129–2137

This error of the force load is mainly reflected in three


aspects: the practical force is not meet measurement
requirements, force direction is not perpendicular to the
sample surface, positive or negative deviation of the force
load velocity.

(1) Measurement uncertainty u3 resulted from diame-


ter, hardness, surface roughness and surface round-
ness of the indenter (steel ball or carbide ball) do
not meet measurement standard.
(2) Measurement uncertainty u4 resulted from these
error sources such as surface roughness error and
shape error of the measured sample, distance error
between two adjacent indentation, sample tempera-
ture error. Fig. 5. Stress–strain characteristics of the measured material. r is the
(3) Measurement uncertainty u5 resulted from mea- stress, e is the strain, rp is the elastic limit, rs is the yield limit, rb is the
strength limit.
surement long term stability.
  qffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
Before make mechanical analysis and simulation for the 2
HB ¼ 0:102  d0 r 2D D  D2  d
2
ð4Þ
whole Brinell hardness measurement process, we should
calibrate these uncertainties. sffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffi
 2  2
D D
2.3. Stress–strain characteristics of the measured material d¼2  h ð5Þ
2 2

In this section, the elasto-plastic dynamic response of where h is the ideal indentation depth, and h, D and d are in
shock on the measured material surface is studied and mm.
the corresponding diagram of the stress–strain state is
presented. 2.5. Force load characteristics of Brinell hardness
On the standard measurement conditions, a universal measurement
material testing machine was used to apply a continuously
changing force on the measured material surface, and In the process of Brinell hardness measurement, force
some experiment data of the amount of compression can load increases from F0 at moment T0 until its value reaches
be acquired. A stress which equals to the force divided by to F1 at moment T1, then the force load F1 is hold for time
cross sectional area of the measured material was used T2. Finally, it is unloaded completely at moment
as ordinate, and a strain which equals to the amount of T1 + T2 + T3, as described in Table 1.
elongation divided by original length of the measured If the indentation force F1 is small, the material elasti-
material is used as abscissa, and then a stress–strain curve cally deforms and upon unloading the surface recovers to
as can be depicted in Fig. 5. its original shape, therefore, in order to acquire an indenta-
In elastic stage, the variance of stress and strain, not the tion, F1 should increase gradually to a certain value so that
stress and strain themselves, satisfies the Hooke Law, an indentation can be generated on the measured material
namely, the strain increases linearly in proportion with surface:
the increase of stress [17]. However, in plastic stage the
strain changes irregularly with the stress increase and in
pd20 rs =4 6 F 1 6 pd20 rb =4 ð6Þ
yield stage the strain changes nonlinearly [18]. In plastic domain, because the relationship between
The stress of the measured material can be calculated stress and strain is usually nonlinear and nonunqiue, the fi-
by the following equations: nal hardness measurement results may be different if one
uses different levels of force load and indenter.
r ¼ f ðF; d0 Þ ¼ F=S ¼ 4F=pd20
2
ð3Þ 2.6. Finite element analysis of Brinell hardness measurement
F ¼ pd0 r=4
process

where F is the force, S is cross sectional area of the mea- Finite element analysis of Brinell hardness measure-
sured sample, d0 is diameter of the measured material ment process, namely, firstly we set the measurement con-
upper surface. dition variables in Ansys 10.0. Then establish an entity
model, which is built according to simplifying appropri-
2.4. Relationship between stress–strain characteristics and
Brinell hardness
Table 1
Force loading characteristics.
If one substitute the stress got by Eq. (3) for that in Eq.
Moment (s) T0  T1 T1  T1 + T2 T1 + T2  T1 + T2 + T3
(1), will obtain the Brinell hardness of the measured
Force (Kgf) F0 ? F1 F1 F1 ? 0
material.
G. Leyi et al. / Measurement 44 (2011) 2129–2137 2133

Fig. 6. Finite element analysis results of Brinell hardness measurement.

Fig. 7. Stress–strain characteristics.

ately the original model, selecting the element type, mesh- element analysis. According to this finite element analysis,
ing and defining the boundary conditions. Furthermore, we we can calculate maximum stress, minimum stress, inden-
should add many random numbers to the force load when tation depth and indentation diameter. The interface of fi-
define many force loading steps and surface contacting nal results is depicted in Fig. 6.
type during the force loading course, and these random Analyzing a large sample of the maximum stress, mini-
numbers are generated by Monte Carlo method in terms mum stress, indentation depth and indentation diameter,
of all measurement uncertainty information. Finally, we using Eqs. (1), (3)–(5), we get the most reliable Brinell
solve it with the multi-step load solution method of finite hardness value.
2134 G. Leyi et al. / Measurement 44 (2011) 2129–2137

Fig. 8. Force loading characteristics.

Table 2
Calibrating the uncertainty U1.

Hardness Reference Indenter Force Indentation Diameter measurement deviation (%)


(HB) block diameter (Kgf) diameter
NIM- SCIM- SCIM- HB- I304 SDHY NXIM GDIM NIM-
(mm) (mm)
01 01 02 3000C 02
250 7991/ 2.5 187.5 0.951 0.26 0.07 0.17 0.17 0.10 0.04 0.46 0.34 0.27
25AW
7992/ 5 750 1.891 0.13 0.06 0.02 0.14 0.02 0.15 0.13 0.24 0.38
25AW
350 7996/ 2.5 187.5 0.837 0.41 0.16 0.18 0.10 0.09 0.15 0.40 0.38 0.37
35AW
7997/ 5 750 1.664 0.23 0.13 0.09 0.49 0.19 0.38 0.13 0.42 0.05
35AW
7998/ 10 3000 3.316 0.22 0.07 0.12 0.13 0.08 0.01 0.15 0.16 0.13
35AW
450 8015/ 2.5 187.5 0.714 0.54 0.17 0.30 0.25 0.30 0.44 0.45 0.47 0.52
45AW
8016/ 5 750 1.412 0.29 0.07 0.02 0.33 0.09 0.12 0.07 0.37 0.44
45AW
8017/ 10 3000 2.820 0.07 0.15 0.07 0.21 0.03 0.06 0.22 0.13 0.02
45AW

3. Validation of the proposed method

HB-3000C is a high precision force loading Brinell hard- Table 3


Calibrating the uncertainty u5.
ness tester made in Laizhou China. HB-3000C was used to
measure some experimental blocks with different inden- Hardness Indenter Force Long term stability
ters, different force levels and different load holding time. (HB) diameter (mm) (Kgf) deviation (%)
The cylinder blocks were produced by Danqin Corporation 250 2.5 187.5 0.10
China, and their height and diameter are 50 mm and 5 750 0.17
100 mm respectively. 350 2.5 187.5 0.15
At first, we got stress–strain characteristics of the mea- 5 750 0.19
10 3000 0.12
sured blocks by a hydraulic-universal material testing ma-
chine, as the brown curve depicted in Fig. 7. Moreover, we 450 2.5 187.5 0.03
5 750 0.13
described the force loading characteristics of this measure-
10 3000 0.08
ment, as the blue dashed curve depicted in Fig. 8.
G. Leyi et al. / Measurement 44 (2011) 2129–2137 2135

Table 4
Measurement uncertainty components of HB-3000C.

Uncertainties (HB) 0–250 HB 250–450 HB 450–600 HB


Distribution interval Distribution type Distribution interval Distribution type Distribution interval Distribution type
U1 (HB) (0.017, 0.018) Uniform (0.021, 0.021) Uniform (0.023, 0.023) Uniform
U2 (HB) (0.004, 0.003) Uniform (0.007, 0.007) Uniform (0.009, 0.008) Uniform
U3 (HB) (0.015, 0.015) Uniform (0.010, 0.010) Uniform (0.024, 0.023) Uniform
U4 (HB) (0.001, 0.001) Uniform (0.003, 0.003) Uniform (0.004, 0.002) Uniform
U5 (%) (0.135, 0.033) Normal (0.152, 0.073) Normal (0.114, 0.013) Normal

Fig. 9. Brinell hardness comparison.

In order to calibrate the measurement uncertainty U1 of In Fig. 9, the blue curve expresses the average of four
HB-3000C, we used other eight Brinell hardness testers practical Brinell hardness measurement results and the
(NIM-01, NIM-02, SCIM-01, SCIM-02, I304, SDHY, NXIM red curve expresses the results got by Monte Carlo method.
and GDIM) to compare the diameter results measured by In Fig. 10, the green curve expresses actual Brinell hardness
HB-3000C, as depicted in Table 2. measurement uncertainty and the red curve expresses the
Calibrate the uncertainty u5 resulted from measure- measurement uncertainty evaluated by Monte Carlo meth-
ment long term stability of HB-3000C in Table 3. od. Obviously, with the sample size increasing, the devia-
Therefore, under the actual measurement conditions tion of Brinell hardness and measurement uncertainty
that force is 3000 Kgf, indenter diameter is 10 mm, load between Monte Carlo simulation method and practical
holding time is 15 s and temperature is 20 °C, we calibrate measurement decreases gradually.
all the measurement uncertainty components of HB-3000C Under other measurement conditions, we use the same
in Table 4. HB-3000C to measure the Brinell hardness of the same
After compiling and running APDL program in Ansys experimental blocks. Moreover, we make some mechanical
10.0 in terms of the analysis steps introduced in this paper, analysis and simulation for these measurements, and listed
we made a finite element analysis for the whole Brinell the results in Table 5.
hardness measurement process. In Table 5, H1 expresses the Brinell hardness acquired
As can be seen from the data in Table 4, the computer by mechanical analysis and simulation, H2 expresses the
can generate a great deal of random numbers based on Brinell hardness acquired by four repeated measurements,
Monte Carlo method, simulate the Brinell hardness mea- U1 expresses the measurement uncertainty acquired by
surement process in a large sample size, get many calcula- mechanical analysis and simulation, and U2 expresses the
tion results and finally several Brinell hardness values measurement uncertainty acquired by four repeated mea-
were got by Eqs. (1), (3)–(5), as indicated in Figs. 9 and 10. surements. Under the same measurement conditions
2136 G. Leyi et al. / Measurement 44 (2011) 2129–2137

Fig. 10. Measurement uncertainty comparison.

Table 5
Result comparison of mechanical analysis and actual measurements.

Force (Kgf) 187.5 750 3000


Indenter diameter (mm) 2.5 5 10
Temperature (°C) 20 20 20
Result (HB) H1 H2 U1 U2 H1 H2 U1 U2 H1 H2 U1 U2
Load holding time (s) 10 88.046 88.045 0.217 0.216 88.237 88.241 0.193 0.184 88.762 88.781 0.205 0.212
15 88.021 88.014 0.203 0.207 88.127 88.201 0.183 0.189 88.520 88.522 0.195 0.198
20 88.002 88.009 0.188 0.193 88.032 88.102 0.175 0.179 88.327 88.332 0.179 0.184

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