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ZHANG Lühong (ে)ۿ1, GAO Guohua ()ܟڳغ1, SUI Hong (ഺ)܃1,2, LI Hong (ह)܀1,2
and LI Xingang (ह᳨)ر1,2,**
1
School of Chemical Engineering and Technology, Tianjin University, Tianjin 300072, China
2
National Engineering Research Centre of Distillation Technology, Tianjin 300072, China
Abstract Liquid distributor is a very import internal for distillation columns. Pre-distributor is usually set on the
top of distributor for initial distribution. Fluid flow in pre-distributor is a complex system of variable mass flow
with many orifices and sub-branches. Consequently, the two phase modeling of pre-distributors was carried out and
the homogeneous model with free surface model was applied. The numerical method was validated by comparing
with experimental data. Using the simulated results for different pre-distributors, the impacts of inflow rate, location
and orientation upon the outflow distribution were investigated. Furthermore, influences of the outflow distribution
for pre-distributor on liquid uniformity in trough were also analyzed. The conclusions can be adopted for the struc-
tural design of liquid distributor and pre-distributor of large scale.
Keywords pre-distributor, computational fluid dynamics, orifices, trough, outflow distribution
¦ rD 1 (5)
D 1
Pressure constraint:
pD p (6)
For free surface flow, the following equation is
used for interfacial area density:
2 rD rE
ADE (7)
rD rE
Figure 3 Compare of simulated mass flow through the
If there are just two phases in the simulation, it is outlet orifices and experimental data
ƵCFD results;ƽexperimental data
simplified to
ADE rD (8)
still exist especially at the end of pre-distributor. It is
The standard k-İ turbulence model was used for assumed that the disagreement is particularly caused
the turbulence simulation. As for boundary conditions, by the remaining air bubbles in the vessel that is un-
velocity for water inlet, pressure for outlet and avoidable during the test setup. On the other hand, the
non-slip setting for walls were applied in accordance numerical model employed in this study focuses on
with operation conditions. As for the initial condition, the liquid phase, but the gas phase is neglected by de-
computational domains were filled with immobile air. activating the cells containing gas only.
Experiments were carried out to validate the per- 5.1 Liquid feed rate
formances of modelling including physical model,
multiphase model and boundary conditions setting. Kister [7] pointed out that variable mass flow
Fig. 2 shows the setup for hydrodynamics test of with multi-orifices can be divided into five general
Pre-distributor I. The volume flow rate at the liquid flow patterns due to different inlet flow rates for the
inlet was 14 m3·h1 (UL 0.5 m·s1) and the corre- same flow channel. Therein, the outflow increases
sponding Reynolds number was about 5.6×104. Drain- from the first orifice to the last one for large inflow
age pipe was used to prevent liquid spills from di- velocity, while it tends to be decrease due to small
rectly outflow near orifices. Liquid mass flux of each inflow velocity and the resulting lower pressure drop
outflow was measured to compare with modeling re- at orifices.
sults for validation. The simulation results for the Pre-distributor II
with different inflow velocities are presented in Fig. 4.
As for the smaller velocity (UL 1.5 m·s1), the out-
flow distribution is consistent with Kister’s clarifica-
tion, whereas the outflow increases for first several
orifices and then decreases for the remaining ones for
Figure 5 Simulated results of distribution planes of water volume fraction for different inflow velocities
the same pre-distributor with larger inflow velocities Figure 6 shows the simulation results for these
(UL 2.0 m·s1, 2.5 m·s1, 3.0 m·s1). Furthermore, the four pre-distributors with the same inflow velocity (1
larger the velocity is, the more orifices in the increas- m·s1). The outflow distributions are apparently dif-
ing trend there are. ferent for these 4 types of pre-distributors. A trend of
In simulation, the distributions of liquid volume decreasing is clearly observed for the straight pipe
fraction are different from inflow velocities. The first with lateral feeding. But for the pre-distributors with
part of pre-distributor close to inlet is full of water horizontal feeding and 45° feeding from the central
(Fig. 5), but the water layer is gradually thinner for the pipe, the outflow distributes with increasing trend in
remaining part. Additionally, the length of this full both left and right ends of the pipe. Moreover, mass
filled part increases with the increase of inflow veloc- flows of outlets for the left segment are mostly larger
ity. Combination of Figs. 4 and 5 helps to conclude than the right ones due to the bias flow caused by the
that the outflow increases for the orifices in the fully orientation of entrance. For the pre-distributor with ver-
filled section of pipe and the outflow for orifices un- tical feeding in the centre, the outflow is low for the
der half filled pipe is vice versa. This result is in ac- centre orifices 6 and 7 due to the central inflow of the
cordance with Kister’s viewpoint. pre-distributor. However, it is the most uniform dis-
When the inflow velocity is above 2.0 m·s1, liq- tribution for the outlet orifices in vertical feeding pipe.
uid mass flow is large enough to fill the whole pipe at
the beginning and a layer distribution occurs for the
rest pipe segment. As for the segment full of liquid,
the outflow increases due to the decreasing of liquid
velocity caused by decreasing liquid mass flow and
the resulting higher static pressure at first orifices. As
for the segment covered by a layer of liquid, the out-
flow presents a downward trend because of decreasing
height of the layer and the resulting lower pressure
along the pipe.
Figure 7 Simulated results of distribution of water volume fraction for feed pipes with different feeding directions
Pre-distributor with multi-orifices is the common Figure 9 Outflow distribution for the shunts of upper
type of inflow for the top row of trough of a large trough with different inflow velocities
scale liquid distributor. Therefore, the uniformity of 1.5 m·s1; 2.0 m·s1; 2.5 m·s1; 3.0 m·s1
liquid level within the upper troughs is directly related
to the outflow distribution of pre-distributor. Fig. 8
shows a distribution of the height of free surface in the feeding; this results in the nonuniformity of outflow
upper trough for the pre-distributor II which indicated through the shunts. Furthermore, an uneven distribu-
that the height of liquid level increased with the in- tion of the upper trough may further affects the distri-
crease of inflow velocity. However, liquid levels are butional performance of liquid in the trough below.
all decreasing for different velocities; this leads to a The computational domain of Fig. 1 (c) including
same decreasing trend for outflow of the shunt troughs, both pre-distributor and troughs was modelled for the
which can be found from Fig. 9. In a word, liquid study whether the pre-distributor with central feeding
level presents serious inconsistencies for the first is better for uniform liquid level of the trough. The
trough under the pre-distributor with long lateral simulated distribution for water volume fraction is
presented in Fig. 10. As shown in this figure, these
two troughs located on both sides are almost full of
water with small bubbles scattered, while these two
close to the entrance are only half full with a serious
fluctuation in the centre. The reason is that impact on
the wall for the inflow makes large lateral velocity;
this leads to smaller outflow through the outlet pipes
near entrance.
Figure 11 is for the outflow distribution within
those four troughs. It is shown that there is a very
large outflow in the centre of trough 1 and 4 resulted
from high liquid level. On the contrary, the outflow
through the central outlets is very small for trough 2
and 3 due to the serious fluctuation and the resulting
thinner liquid layer. In addition, the outflow of the
remaining outlets has an increasing trend.
Figure 8 Simulated liquid level within the trough for Since the central feeding still can not obtain more
different inflow velocities uniform liquid distribution, it is suggested for structural
UL/m·s1: 1ü1.5; 2ü2.0; 3ü2.5; 4ü3.0 optimization with tapered design for the troughs or
820 Chin. J. Chem. Eng., Vol. 19, No. 5, October 2011
Figure 10 Simulated planes for water volume fraction within different troughs
NOMENCLATURE
6 CONCLUSIONS
REFERENCES
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