Sample No : PKM-S2-Ⅱ-05 Request No: PKM-S2-2018-II- 34286

Grade : 60/70 Test date : 12-01-2018

Source : Parco Oil Refinery Sample date :12-01-2018

Specification
Test Items
Obtained Required

Needle penetration ( 25°C , 100g , 5s) ( 0.1mm) 68.3 60 ~ 70

Softening point ( ring and ball method ) °C 47.3 >46

Ductility ( 5cm/min, 25°C ) >100 >100

Flash point ( °C ) 353 >232

Solubility (%) / > 99

Wax contant ( % ) / < 2.2

Film heating test Quality change ( % ) / < 0.8

( 163 C 5h )
Residual penetration ( % ) / > 61

Specific Gravity ( 25 C ) / 1.01 ~ 1.06

Conclution:

o
 SOFTENING POINT OF BITUMEN

AASHTO M-20 & T- 53

LAB No. :PKM-S2-Ⅱ-01180001 Request No: PKM-S2-2018-II- 34286

SAMPLE: PKM-S2-Ⅱ-05 BITUMEN SOURCE : Parco Oil Refinery

SAMPLE DATE : 31-03-2018 BITUMEN GRADE : 60/70

ELAPSED TIME min

THERMOMETER
START 1 2 3 4 5 6 7 8 9 10 11 12 13

5.0 10.0 15.2 19.9 25.0 30 35.1 40 45 47.2

TEMPERATURE 5.0 10.0 15.2 19.9 25.0 30.0 35.1 40.0 45.0 47.3

BALL1 47.2

TOUCHES THE BOTTOM PLATE **

BALL 2 47.4

SOFTENING POINT ASTM D 36 MEAN 47.3

MEAN + 2.5
SOFTENING POINTAASHTO M-20 & T 53 49.8
C

Max variation of temperature rise after first 3 minutes : ±0.5 C .

If the difference between the temperature exceeds 1 ºc, repeat test

REMARKS:
 34286

Oil Refinery

14 15

47.2

47.4

47.3

49.8
 Ductility Test

AASHTO T- 51

Lab No : PKM-S2-Ⅱ-03180001 Request No: PKM-S2-2018-II- 34286

Bitumen Source : Parco Oil Refinery Sample NO: PKM-S2-Ⅱ-05

Bitumen Grade : 60/70 Test Date: 31-03-2018

TEST temperature 25℃

TEST No. 1 2 3

Ductility cm >100 >100 >100

Average Ductility cm >100

Remarks
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Project No. Project Name PKM

Penetration Test
AASHTO T- 49

Lab Ref No. PKM-S2-Ⅱ-12170002

Request No : PKM-S2-2018-II- 34286

Bitumen Grade 60/70 Sample No PKM-S2-Ⅱ-01

Sample Date 31-03-2018 Test Date 31-03-2018

Source Of Bituman Parco Oil Refinerry

(1) Penetration (0.1mm) 63.2

Temp.Of Testing 25 °C

(2) Penetration (0.1mm) 61.5

Load Of Testing 100 gm (3) Penetration (0.1mm) 62.5

Time Of Testing 5 Sec Mean (0.1mm) 62.4

Remarks
 FLASH AND FIRE POINT BY CLEVELAND OPEN CUP

AASHTO M-20 ,T-79

Lab No : PKM-S2-Ⅱ-03180001 Request No: PKM-S2-2018-II- 34286

Bitumen Source : Parco Oil Refinery Sample NO: PKM-S2-Ⅱ-05

Bitumen Grade : 60/70 Test Date: 31-03-2018

Sample Date : 31-03-2018

SAMPLE PREPARATION

POURING OF SAMPLE Fill The Cup With Max 100C0 OR Above Expacted Softening Point

TEST No. 1 2

FLASH POINT 338 340

AVERAGE FLASH POINT 339

AT ROOM TEMPERATURE 25

REMARKS: Flash Point minimum =2320C Fire Point 3550C

 Customer
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Project No. Project Name Pkm

Specific Gravity of Bitumen

Bitumen Grade 60/70 Source of bitumen Parco Oil Refinery.

Sample Date 12-12-2017 Lab No PKM-S2-Ⅱ-12170002
Tested Complete 14-12-2017 Test N0 : CL 85

Test No. 1 2 3 Average

A Mass Of Pycnometer (Plus Stopper) g 25.64 25.35 25.40

B Mass Of Pycnometer Filled With Water g 49.86 51.28 50.45

C Mass Of Pycnometer Partially Filled With Asphalt g 37.34 32.19 35.20

D Mass Of Pycnometer + Asphalt + Water g 50.18 51.48 50.7

Specific Gravity + [ C-A/(B-A)-(D-C)] 1.028 1.030 1.026 1.028

Reference No.

Remarks:
Description : Date : 14-12-2017
Grade :60/70 Sample : PKM-S2-Ⅱ-01
Source :Parco Oil Refinery Test No. Cl-26

Solubility of Bitumen

Wt of flask ( gm ) A 150.93

Mass of flask + sample ( gm ) B 155

Mass of sample (gm ) B-A=C 4.07

Mass of filter paper ( gm ) D 1.43

Mass of filter paper after drey oven E 1.45

Mass of insoluble bit. % E-D=F 0.02

Insoluble bit.% F/C*100=G 0.49

Solubility % 100-G 99.5

Remarks:
 LOSS ON HEATING OF ASPHALTIC COMPOUNDS
AASHTO M-20 ,T-47

SAMPLED : 1 BITUMEN SOURCE : Parco oil refinery

DATE SAMPLED : 26-12-2017 BITUMEN GRADE : 60/70

TEMPERATURE MAINTAINED : 163℃ TIME FOR SAMPLE AT 163℃ : 85mins

SAMPLE PREPARATION

TEMPERATURE TO HEAT THE SPECIMEN TO POURING TEMMax 100C0 OR Above Expacted Softening Point

POURING OF SAMPLE : 35+0.5g in a Container

TEST No. 1 2

CONTAINER NUMBER 1 2

MASS OF CONTAINER A 153.422 150.869

MASS OF CONTAINER PLUS SAMPLE BEFORE PLACING

B 188.318 185.748
IN OVEN,AT ROOM TEMPERATURE

MASS OF SAMPLE C=B-A 34.896 34.879

MASS OF CONTAINER PLUS SAMPLE AFTER 5Hr IN

D 188.183 185.614
OVEN, AT ROOM TEMPERATURE
LOSS IN WEIGHT E = B- D 0.135 0.134

%age OF LOSS ON HEATING E×100/C 0.387 0.384

AVERAGE LOSS ON HEATING 0.385%

AT ROOM TEMPERATURE 25℃

REMARKS:
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Project No. Project Name PKM

Residue Penetration Test
Lab Ref No. central lab Source of bitumen Attack Refinery.

Bitumen Grade 60/70 Serial No: 16

Sample Date 3/4/2017 Sample 1

Tested Complete 3/4/2017 Tested Date 9-.4.-17

Softening Temp

(1) Penetration (mm) = 6.23,61.9,6.7=6.37

Temp.Of Testing 25°C

(2) Penetration (mm) =

Load Of Testing 100 gm 6.12,6.09,5.98=6.06

Mean (mm) =
Time Of Testing 5 Sec 6.23

Remarks / Recommendations

penetration on residue at 163°c for 5hours in oven = 6.23