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Installation b. Insert and tighten the fixing screw.

1. Unpack the meter, power supply, electrode, c. Turn the meter and base the right way up and
electrode arm, buffer sachets, Guide Book and locate the electrode arm onto the base fixing
calibration certificate. Store the calibration post. Press down to snap into place.
certificate in a safe place.
2. Check the power supply unit is the correct
voltage for your local supply. If it is not, contact
your distributor.
3. Attach the electrode arm to the left or righthand
side of the meter:
a. Turn the meter upside down and seat the
dome of the electrode arm base into the left
or righthand meter recess.

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Input and Output Connections Display
power supply recorder output reference stability/auto
unit socket socket electrode endpoint indicator
socket

prog. menu
sample ID and data
icon shown transfer
here icons shown
data output pH or automatic
here
socket combination temperature
electrode compensation
electrode
socket probe socket automatic or
condition
shown manual
1. Disconnect the shorting clip from the pH socket memory,
here temperature
cal and
and retain it by clipping it over the socket. compensation
error
indicator
2. Connect the electrode to the pH socket. If you temperature, number
electrode shown here
are using an electrode incorporating ATC
offset/slope
connect the other lead to the ATC socket. shown here
3. If you are using a separate ATC probe connect it
to the ATC socket.
4. Connect the power supply unit to the DC socket.
Calibrating 3. Repeat steps 1 and 2 using other buffers for a
2 point or 3 point calibration.
1. 1-point calibration
Electrode Condition Indicator
Example
95.0 - 105.0% 90.0 - 94.9% 85.0 - 89.9%
↓ 2 seconds electrode in electrode electrode
buffer good needs needs
condition cleaning conditioning

n When you press Cal the pH buffer you selected for


cal 1 (Program Menu) is displayed for 2 seconds, and
then the meter starts measuring. If you want to use
Use auto endpoint or another pH buffer (choice of 3) press Cal again. Press
to freeze the reading. Cal repeatedly to exit the calibration routine.
n The decimal point flashes during calibration
measurement. When the electrode output
has stabilized the stability indicator appears.
2. Rinse the electrode and blot dry Manual endpoint - press Read to endpoint.
Auto endpoint - the meter automatically endpoints.
n When a calibration has endpointed you can press
to return to sample measurement, or Mode to display the absolute mV value and tempera-
ture of the buffer. The display reverts to the buffer
continue with step 3 for further cal points
and E0 values, or buffer and slope values for a 2 or 3
point calibration after 2 seconds.
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Measuring Samples n If you press Mode to select pH or mV mode the meter
begins measuring immediately. You will not need to
1. Select pH or mV mode press Read to start the reading.
n The decimal point flashes during sample
measurement. When the electrode output
has stabilized the stability indicator appears.
2. Measure sample
Manual endpoint - press Read to endpoint.
Auto endpoint - the meter automatically endpoints.
n If you have the RS232 cable connected to the Data
socket, sample data is transmitted at endpoint.

Use auto endpoint or


to freeze the reading.

3. Rinse, blot and store the electrode.


Operating Hints n When you select the calibration buffers
(Program Menu), set the buffer you will use
n Remove the wetting cap from the end of the
most frequently for 1-point calibrations as cal 1,
electrode and the rubber cap from the fill hole (if
the one you will use most frequently for the
fitted) before using the electrode.
second calibration point as cal 2, and the one
n Calibrate using buffers with values that bracket you will use most frequently for the third
that of the sample. With a new pH electrode, or calibration point as cal 3.
after maintenance, we recommend you use a
buffer close to pH 7 for the first calibration point.
Using Auto Endpoint
n For greatest accuracy, buffers and samples The auto read feature can be used in pH and
should be at the same temperature. mV mode to automatically determine a stable
n Do not use solutions after the expiry date. endpoint during calibrations and sample measure-
ments.
n When transferring the electrode from one
solution to another, rinse it with distilled water Press A . The display shows the auto endpoint
and blot dry with tissue paper - do not wipe the indicator . The display will freeze automatically
electrode as this may cause polarization and when a stable endpoint is reached. To manually
slow response. freeze the display press Read. To turn auto endpoint
off press A again.

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Recalling Calibration Data Recalling Memory
Calibration data can be recalled to the display (last You can only recall stored memories if the current
calibration only) and to the printer (last 10 measurement has endpointed.
calibrations). Press R - the last stored memory is displayed.
You can only recall cal data if the current measure- Press M or R to scroll through memories.
ment has endpointed - press Read if necessary. RM 1 to RM 20 indicates which memory is being
Press and hold Cal for 2 seconds. The display displayed. M 0 indicates no memories stored.
shows the date and time of the last calibration, the
buffer value, the mV offset (E0) for 1-point Clearing the Memories
calibrations, and the slope value (%) for 2 (3) point Press M then press M or R until M C is displayed.
calibrations. Press Mode to clear the memories, M 0 indicates
the memories have been cleared. (Press Read to
Using the Memory exit without clearing the memories).
Entering a Reading into Memory
The MP230 can store up to 20 endpointed results.
Press M when the measurement has endpointed.
M 1 is displayed (or M 2 to M 20 if readings have
already been stored).
M 20 indicates the memory is full.
Using Continuous Data Using Sample ID
Transfer Mode The sample number counter increments 1 every
In continuous data transfer mode readings are sent time a sample measurement is endpointed.
to the data output approximately every second. If To change or reset the sample ID number, press ID.
the measurement endpoints (manually, or using
Enter your required sample number using the
auto endpoint) data transfer stops. If you recall
keypad (enter 0 if you want to reset the number)
memories all stored readings are output, (from the
and press ID again.
first to the last stored).
n If you press the ID key while measuring, the
To select continuous data transfer mode press and
sample number is assigned to that sample.
hold R for 2 seconds.
If you press ID when the measurement has
n To maintain continuity of sample readings endpointed, the number will be assigned to the
calibration data is only output at endpoint. next sample.

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Program Menu Time and date are displayed during
The Program Menu allows you to set date and time, calibration recall, and will be sent to the
manual temperature compensation, pH calibration serial output. Time is shown on the main
buffers and to adjust the display resolution. It also display, the date is shown on the lower part
allows you to set the following GLP functions: of the display.
calibration reminder, hi/lo limits, and to adjust the Set the time and date using M and R .
offset and slope limits. Press Prog to enter the value and move on.
You can only enter the Program Menu if the current MTC You can enter temperature manually
measurement has endpointed - press Read if between –5.0 and 130.0°C. (An ATC probe
necessary. will override manual compensation.) The
Press Prog to access the Program Menu - MP230 has a preset temperature of 25°C.
appears. Use M and R to change temperature. Press
Prog to enter the value and move on.
Press Prog to scroll through the options and press M
and R to change the value (press and hold to scroll
quickly). Press Read to exit the Program Menu at
any time. If you press Read when a value is flashing
that value will not be entered.
Program Menu (continued) dP The resolution of the meter can be set to
You can select three pH calibration buffers. display 3, 2 or 1 decimal places. The MP230
The buffers are grouped in sets (b=1, b=2, has a preset resolution of 3 decimal places.
b=3); select your required set first using M Use M and R to change the number of
and R : decimal places displayed. Press Prog to
set 1 = 7.000, 4.000, 10.010, 1.679 enter the value and move on.
set 2 = 7.000, 4.010, 9.210, 2.000, 11.000 The MP230 now enters the GLP functions setup. If
set 3 = 6.865, 4.006, 9.180, 1.679 you know the GLP code continue, otherwise press
Press Prog to enter the set and move on. Read to exit the Program Menu.
NOTE: Check buffer set 2 is selected to use the Press Prog to scroll through the options and use the
buffers supplied. numeric keypad to enter values. Press Read to exit
Choose three buffers (cal 1, cal 2, cal 3) from the Program Menu at any time.
the set for calibration. For ease of use, set the
buffers in the order that you will use them.
GLP Enter the GLP code using the keypad and
cal 1 press Prog to move on. The MP230 will not
cal 2 For example: Set 2 (factory settings)
cal 3 cal 1=7.000, cal 2=4.010 and cal 3=9.210 allow you to access the GLP set up unless
the code is entered correctly.
2.000 and 11.000 not selected.
These can be rearranged in any order using
M and R . Press Prog to enter the value
and move on.
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Program Menu (continued) E0 mV The acceptable E0 (offset) value can be set.
The calibration reminder interval can be If an electrode calibration produces an
set, in hours, between 0 and 9 (where 0 = offset value outside the E0 range an Err1
no reminder). When the selected time has error is displayed. The MP230 has a preset
elapsed the calibration reminder symbol E0 limit of ± 35.0 mV. The limit can be set
will appear. The MP230 has a preset between 0 and 35 mV.
reminder interval of 1. Change the interval Change the E0 limit using the keypad and
using the keypad. Press Prog to enter the press Prog to enter the value and move on.
value and move on. The acceptable low slope value can be set.
Lo
Hi/lo limits for pH readings can be set. If a % slope If an electrode calibration produces an
reading is outside these limits the display electrode slope value below the set value
is flagged and an alarm sounds. an Err2 error is displayed. The MP230 has
The MP230 has preset limits of lo = –2.000 a preset low slope limit of 85%. The limit
and hi = 19.999. can be set between 85 and 104.9%.
The lo limit can be set between –2.000 and Change the low slope value using the
19.999. Change the lo limit using the keypad and press Prog to enter the value
keypad and press Prog to enter the value and move on.
and move on. The hi limit can be set
Press Read to exit the Program Menu.
between the lo limit setting and 19.999.
Change the hi limit using the keypad and
press Prog to enter the value and move on.
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Interfacing n Data is sent to the Data socket at measurement
endpoint (manual or automatic), calibration recall and
Serial Output memory recall.
The MP230 can interface with computers, printers n To use the output to monitor continually, you need to
(GA42), Acquire Data Acquisition software and select continuous data transfer mode.
other RS232 compatible devices via the RS232
cable. The maximum source or sink current Recorder Output
available is ± 10mA. An output is available for both modes. The polarity
of the output is the same as the polarity of the input
Pin Signal Pin Signal
1 device enable (link to pin 5) 6 not used
signal.
2 RS232 Tx (signal transmit) 7 not used Approximate Recorder Outputs
3 not used 8 not used pH - Output follows display and provides approxi-
4 CTS (clear to send) 9 not used mately 60 mV output/pH unit. This value varies with
5 protective ground (0V)
changes in electrode slope and temperature.
Data Socket mV - Output follows display, i.e. output varies from
protective ground (0V)
CTS
–1999.9 to 1999.9 mV.
signal transmit Recorder output is not available for temperature.
5 1
Rec Socket Polarity
0V
9 6
Type of communication - uni directional, baud rate 2400, output
data format - 7 data bits : 1 stop bit : even parity
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Problem Solving Err 3 - pH buffer outside temperature limits
Err 1 - offset value (E0) out of range pH buffers must be between 5°C and 50°C for
Check correct buffer is used. accurate calibration.
Check the E0 mV setting (in Program menu). •
Displayed (out of range)
Check mV reading for pH 7 buffer is 0 ± the set Check electrode is connected and immersed in
value (default 35 mV). If it is not, clean or replace sample. Check wetting cap is removed.
the electrode. Data Entry Errors
Err 2 - slope out of range Date flashes and reverts to previous setting - invalid
Slope less than the set value (default 85%), or date entered.
not calculable. Entered temperature value changes to –5.0 or 130.0
Electrode needs cleaning, conditioning or - the MP230 will not accept values outside this
replacing. Check correct buffers are used. range.
Slope more than 105.0%. Dashes displayed instead of buffer value during
Check calibration buffers. calibration buffer set up - that buffer has already
been selected for a cal point. Cal points must have
NOTE: Where 0 mV/pH unit = 0%, and different values.
59.16 mV/pH unit = 100% (at 25°C)
Entered E0 value changes to 35 - the MP230 will not
accept values greater than 35.
Problem Solving (continued) Electrode Maintenance
Data Entry Errors (continued) Refer to the electrode product insert for full details
on maintaining your electrode.
Entered lo/hi limits change to –1.999 or 19.999. The
MP230 will not accept lo limits greater than the hi
limits.
Entered lo slope value changes to 85 or 104.9 - the
MP230 will not accept values outside this range.
MP230 will not allow access to the GLP setup -
correct GLP code must be entered.

Maintenance
There are no user replaceable parts in the MP230 or
power supply unit. Do not remove the covers.
The MP230 requires very little maintenance.
Occasionally wipe the meter with a damp cloth. The
casework is made of ABS/PC which is known to be
affected by some organic solvents, including toluene,
xylene and methyl-ethyl-ketone. It is good practice to
wipe away any spillages as soon as they occur.
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Spares and Accessories
52000100 InLab 413 ‘3 in 1’ pH Electrode
52000118 InLab 410 pH Electrode
51300164 30KΩ NTC Probe
51302118 Electrode Arm and Base
51302152 Recorder Cable
51302125 RS232 Cable
00229170 GA42 Printer
00229119 LC - P45 GLP Printer
51300047 Guide to pH Measurement
51302069 pH 4.01 Buffer Sachets, 30/pack
51302047 pH 7.00 Buffer Sachets, 30/pack
51302070 pH 9.21 Buffer Sachets, 30/pack
51302068 Rainbow Pack Buffer Sachets (10 each
of pH 4.01, 7.00 and 9.21)
51340058 pH 4.01 Buffer Solution, 250 mL x 6
51340060 pH 7.00 Buffer Solution, 250 mL x 6
51300194 pH 9.21 Buffer Solution, 250 mL x 6

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Buffer Tables
The MP230 automatically corrects pH buffers for
temperature using the values shown in the table.

1.679 2.000 4.000 4.006 4.010 6.865 7.000 9.180 9.210 10.010 11.000
5°C 1.668 2.020 4.000 4.004 4.010 6.951 7.090 9.395 9.450 10.250 11.720
10°C 1.670 2.010 4.000 4.000 4.000 6.923 7.060 9.332 9.380 10.180 11.540
15°C 1.672 2.000 4.000 3.999 4.000 6.900 7.040 9.276 9.320 10.120 11.360
20°C 1.675 2.000 4.000 4.001 4.000 6.881 7.020 9.225 9.260 10.060 11.180
25°C 1.679 2.000 4.000 4.006 4.010 6.865 7.000 9.180 9.210 10.010 11.000
30°C 1.683 1.990 4.010 4.012 4.010 6.853 6.990 9.139 9.160 9.970 10.820
35°C 1.688 1.990 4.020 4.021 4.020 6.844 6.980 9.102 9.110 9.930 10.640
40°C 1.694 1.980 4.030 4.031 4.030 6.838 6.980 9.068 9.060 9.890 10.460
45°C 1.700 1.980 4.040 4.043 4.040 6.834 6.970 9.038 9.030 9.860 10.280
50°C 1.707 1.980 4.060 4.057 4.060 6.833 6.970 9.011 8.990 9.830 10.100

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Specifications Input Conditions
Measurement pH –1.999 to 19.999 Impedance >1012 ohms
Ranges mV ± 1999.9 Operating Conditions
Temp. -5.0 to 130.0°C Temperature 5 to 40°C
Resolution pH 0.001 (adjustable) Humidity 5 to 80% at 35°C (non condensing)
mV 0.1 Installation Category 2
Temp. 0.1 Pollution Category Degree 2
Relative pH ± 0.001 Size/Weight 10 1/2 x 7 1/2 x 2 1/2 inches
Accuracy* mV ± 0.1 mV (265 x 190 x 65 mm)
Temp. ± 0.2°C 2lb (0.9kg)
Memory 20 memories
Power Requirements
Isopotential Point pH 7.000
The MP230 is supplied with an appropriate power
pH Calibration Buffers 3 sets of buffers supply unit.
Calibration Points pH 3 of 3 selectable USA/Japan 100 - 120V, 50/60Hz, 0.85VA
Temp. Compensation -5.0 to 105.0°C, automatic Europe 230V, 50Hz, 1.1VA
and manual
Output from PSU: 9V DC
Display LCD
Outputs Recorder MP230 Power Rating: 0.3VA
Serial NOTE: The MP230 should only be used with the
* ± 1 least significant digit power supply unit supplied.

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