VHG Labs, Inc.

Standards and Supplies for Spectrochemical Oil Analysis

Section 1 Petroleum Standards

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Multi-Element Coolant Standard

Coolant Standard
The following standard is intended for use in the analysis of metals in ethylene glycol or other coolants. It can be diluted 1:1 with ethylene glycol (for matrix matching) or in dilute nitric acid. Matrix: 1% HNO3, tr. HF . Volume (mL ) 500 Element Al B Ca Cu Fe K Mg Conc. (g/mL ) 50 1,000 50 50 50 1,000 50 Product No. GLYCOLSTD-500 Element Mo Na P Pb Si Zn Conc. (g/mL ) 500 1,000 2,500 50 500 50

Custom single element or multi-element standards are available (please inquire).

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Fuel Dilution Standards

F uel Dilution Standards

These standards are intended for use in the determination of fuel (diesel fuel or gasoline in motor oil) by fuel dilution meter (fuel sniffer), IR, GC analyzer or flash point. They are prepared gravimetrically from high purity fuels added to high purity motor oil and certified by GC-FID in accordance with ASTM Methods D3524 and D3525. Description 5% Virgin Diesel Fuel in 15W40 Motor Oil 5% Devolatilized Diesel Fuel in 15W40 Motor Oil 5% Virgin Gasoline in 10W30 Motor Oil 5% Devolatilized Gasoline in 10W30 Motor Oil Application Fuel Dilution Meter GC or IR Fuel Dilution Meter GC or IR Product No. DSL5%VIR-100 DSL5%DEV-100 GAS5%VIR-100 GAS5%DEV-100

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Analyzing

Biodiesel?

Call for more information on standards for biodiesel.

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Crackle Test References

Petroleum Standards

Section 1 Petroleum Standards

Crackle T est references for determining water in oil (all values nominal). The crackle test is a visual test performed by placing a small drop of oil onto a hot plate (usually around 300C). The amount of water present in oil samples is estimated by comparison to these standards. certified by gravimetric preparation. All values Standards for Used Oil Analysis Wear Metals
Nominal Water Concentration (% ) Blank 0.1% 0.5% 1.0% Volume (mL) 250 250 250 250 Product No.

Coolant Fuel Dilution Water in Oil Soot Standards for S, N, Cl and Metals Petroleum Physical Test Standards

CT-BLK-250 CT-0.1%-250 CT-0.5%-250 CT-1.0%-250

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K arl Fischer Titration Cer tified Reference Standards

Karl Fischer Titration certified reference standards for determining water in motor oil (all values certified by Karl Fischer Titration). This test determines the amount of water present in the oil and is the most commonly-used test for this type of determination, with a high degree of accuracy. For use with ASTM D6304.
Nominal Water Concentration (% ) Blank 0.1 0.5 1.0 Volume (mL) 100 100 100 100 Product No. KF-BLK-100 KF-0.1%-100 KF-0.5%-100 KF-1.0%-100

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Soot Content Standards

Reference standards for use in the determination of soot content in 15W40 diesel motor oil by infrared spectroscopy or other technique. All values certifed by thermogravimetric analysis (TGA).

Nominal Soot Content Range (% ) Blank 0.5-2 2-4 4-6 6-9 9-12 Set of all 6

Volume (mL) 50 50 50 50 50 50 6 x 50

Product Number SOOT-BLK-50 SOOT-A-50 SOOT-B-50 SOOT-C-50 SOOT-D-50 SOOT-E-50 SOOT-SET

Section 1 Petroleum Standards

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Polysulfide Oil Standards

Sulfur QC Samples, Drift Monitors and Calibration Standards Made from Polysulfide oil
VHG Labs' polysulfide oils have been formulated for long shelf life and optimal stability even when exposed to x-rays from modern high wattage XRF spectrometers. In addition, our polysulfide oil products offer high purity, low volatility, and minimal diffusion through sample films.

These standards are well suited to ultra low level sulfur analysis, quality control, drift correction, blank measurement and calibration standards for XRF and other sulfur analysis techniques. Our polysulfide oil standards are intended for use in accordance with the newly revised ASTM D2622, D4294, D5453, D7039, D7212, D7220 and others.

Description
QC Samples Sulfur @ 5g/g, Polysulfide oil, 1L Sulfur @ 10 g/g, Polysulfide oil, 1L Sulfur @ 2 5g/g, Polysulfide oil, 1L Drift Monitors Sulfur @ 10 g/g, Polysulfide oil, 1L 0 Sulfur @ 2 50 g/g, Polysulfide oil, 1L Sulfur @ 50 g/g, Polysulfide oil, 1L 0 Sulfur @ 1,0 0 0 g/g, Polysulfide oil, 1L Blank Polysulfide Oil Blank Calibration Sets Sulfur Standard Set (low concentrations). Set of 13 Calibration Standards with Sulfur @ 0, 1, 2.5, 5, 10, 25, 50, 75, 100, 250, 500, 750, 1000g/g, made from high purity polysulfide oil, 50mL each Sulfur Standard Set (high concentrations). Set of 12 Calibration Standards with Sulfur @ 0, 0.1, 0.5, 1, 1.5, 2, 2.5, 3, 3.5, 4, 4.5 and 5wt%, made from high purity polysulfide oil, 50mL each Sulfur Standard Set (low concentrations). Set of 6 Calibration Standards with Sulfur @ 0, 10, 25, 50, 100 and 250g/g, made from high-purity polysulfide oil, 50mL each

Product No.

X3SPS-5-1L X3SPS-10-1L X3SPS-25-1L

X3SPS-100-1L X3SPS-250-1L X3SPS-500-1L X3SPS-1000-1L

X3SPS-BLK-1L

X3SPS-SET1-13X50mL

X3SPS-SET2-12X50mL

X3SPS-SET3A-6X50mL

Petroleum Physical Test Standards

Petroleum Standards

Section 1 Petroleum

Flash Point Reference Materials

VHG Labs Flash Point Reference materials are intended for use with and certified by the appropriate ASTM methods [ ASTM D56, D92, D93] Each standard is supplied with a full Certificate of Analysis (COA). . Volume: 250mL Specification ASTM D93 (Flash Point) Apparatus Pensky-Martens Closed-Cup T ester Nominal Temp. C 27 60 75 93 ASTM D92 (Flash and Fire Point) ASTM D56 (Flash Point) T ag Closed T ester Cleveland Open Cup 200 230 42 55 60 67 Product No. FP27-250 FPPM60-250 FP75-250 FP93-250 FP200-250 FP230-250 FP40-250 FP55-250 FPTC60-250 FP68-250

Standards

Standards for Used Oil Analysis Standards for S, N, Cl and Metals Sulfur-Free MetalloOrganics Nitrogen Sulfur and Metals Sulfur Chlorine Lead in Gas Petroleum Physical Test

Flash Point Certified Reference Materials

VHG Labs Flash Point Reference materials are intended for use in accordance with ASTM methods [ ASTM D56, D92, D93] These certified reference materials are stable, pure hydrocarbons with a method specific flash point . determined by an inter-laboratory study. Each standard is supplied with a full Certificate of Analysis (COA). Volume: 250mL Hydrocarbon N-Decane N-Undecane N-T etradecane N-Hexadecane D92 Flash & Fire Point Cleveland Open Cup D56 Flash Point T ag Closed T ester N-T etradecane N-Hexadecane N-Decane N-Undecane Nominal Flash Point C 54C 70C 114C 134C 116C 140C 50C 67C Product No. FP53-250 FP70-250 FP114-250 FP134-250 FP115-250 FP138-250 FP51-250 FP67-250

Standards Flash Point Viscosity

ASTM Test D93 Flash Point Pensky-Martens Closed Cup T ester

Viscosity Reference Standards

VHG Labs provides viscosity reference standards, intended for use in accordance with standard methods [ e.g. ASTM D445] Each standard is manufactured in our ISO 9001:2000 and ISO/IEC 17025:2005 facility and sup. plied with a full Certificate of Analysis (COA) which states the Certified Viscosity as correlated to the Master Viscometer technique and is traceable to the NIST value of 1.002 mPa-s for water at 20C. Volume: 500mL Nominal Viscosity @ 40(cSt) 9.5 30 54 102 110 130 300 520 920 Nominal Viscosity @ 100(cSt) 2.8 5.3 7.3 15.3 16.8 20 47 57 84 Product Number VISC10-500 VISC30-500 VISC60-500 VISC100-500 VISC110-500 VISC130-500 VISC300-500 VISC500-500 VISC900-500

Section 1 Petroleum Standards

Petroleum Physical Test Standards

ASTM D97 Pour Point Certified Reference Materials

ASTM D97 method for determination of the pour point of petroleum products. Standards are packaged in 250mL bottles and are accompanied with a certificate verifying the determined value. Volume: 250mL Nominal Pour Point (C): Product No.: -5 P5-250 -10 P10-250 -15 P15-250 -20 P20-250 -40 P40-250 -50 P50-250

ASTM D2500 Cloud Point Certified Reference Materials

ASTM D2500 method for determination of the cloud point of petroleum products. Standards are packaged in 250mL bottles and are accompanied with a certificate verifying the determined value. Volume: 250mL Nominal Cloud Point (C): Product No.: +5 C5-250 -2 C2-250 -10 C10-250 -15 C15-250 -20 C20-250

ASTM D2386 Freezing Point Certified Reference Materials

ASTM D2386 method is for determination of the freezing point of aviation fuels. Standards are packaged in

250mL bottles and are accompanied with a certificate verifying the determined value. Volume: 250mL Nominal Freezing Point (C): Product No.: -50 F50-250 -45 F45-250

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ASTM D86 Group 1 & 2 Synthetic Distillation Standard
The automatic distillation apparatus duplicates the distillation conditions of the manual method. The increased reliance on electronic control requires an independent standard to verify that the apparatus is performing correctly. VHG has introduced a synthetic blend of hydrocarbons that boil in the temperature range specified in ASTM D86 distillation groups 1 and 2. The Group 1 and 2 standard covers the boiling range 129 F to 368 F (54 to 187 C) and was verified by , consensus analysis with twelve refinery laboratories. Description Synthetic Distillation Standard 0.5L Product No. D86-500

Group 1 & 2 Distillation Range IBP 10% 50% 90% EP 129 F 180 F 228 F 319 F 368 F

ASTM D86 Group 4 Distillation Standard

The Group 4 standard is a diesel oil whose distillation range is 379 F to 700 F (193 to 371 C) and was , verified by consensus analysis. Description Synthetic Distillation Standard 0.5L Group 4 Distillation Range IBP 10% 50% 90% EP 379 F 439 F 525 F 639 F 700 F Product No. D86-4-500

Petroleum Physical Test Standards

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Total Acid Number (TAN Reference Materials) VHG Labs' TAN Reference materials are intended for use in the determination of T otal Acid Number (TAN) in petroleum products by potentiometric titration. ASTM D644 and IP177. Matrix *Certified Value (mg KOH/g) Mineral Oil Mineral Oil Mineral Oil Mineral Oil Mineral Oil Mineral Oil Mineral Oil 0.1 0.5 1.0 1.5 2.0 2.5 3.0 Size (grams) 125 125 125 125 50 50 50 TAN-0.1 TAN-0.5 TAN-1 TAN-1.5 TAN-2 TAN-2.5 TAN-3 Product Number Our TAN standards are intended for use in accordance with

Petroleum Standards

Section 1 Petroleum Standards

Standards for Used Oil Analysis Standards for S, N, Cl and Metals Petroleum Physical Test Standards Flash Point Viscosity Pour Point Cloud Point Freezing Point Distillation TAN, TBN

Acid number is defined as the quantity of base expressed as milligrams of potassium hydroxide per gram of sample, required to titrate a sample to a well defined inflection point as specified in ASTM D 6 4 4 .

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Total Base Number (TBN Reference Materials)
VHG Labs TBN reference materials are intended for use in the determination of T otal Base Number (TBN) in petroleum products by potentiometric titration. ASTM D2896 and IP276 or ASTM D4739. Matrix *Certified Value (mg KOH/g) Mineral Oil Mineral Oil Mineral Oil Mineral Oil Mineral Oil Mineral Oil 6 10 15 30 40 70 Size (grams) 50 50 50 50 50 50 TBN-6-50 TBN-10-50 TBN-15-50 TBN-30-50 TBN-40-50 TBN-70-50 Product Number Our TBN standards are intended for use in accordance with

*Base number is defined as the quantity of perchloric acid, expressed in terms of the equivalent number of milligrams of potassium hydroxide that are required to titrate 1g of the sample, dissolved in the specific solvent to a well defined inflection point as specified in ASTM D 28 6 9 .