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Recuperation of ancient gypsum plasters: characterization and development of compatible gypsum based materials
Maria Teresa de Almeida Gouveia Geraldes Freire
SUPERVISORS: Rosrio Veiga, Jorge de Brito (IST - ICIST), Antnio Santos Silva KEY WORDS: Historical heritage, Ancient gypsum plasters, Characterization, Compatible restoration products INTRODUCTION: Characterization of ancient gypsum plaster samples belonging to several historical periods, collected from North to South of Portugal. Based on the characterization results it was concluded that only between the second half of the 18th century and the first half of the 20th was the presence of gypsum plasters significant in the Portuguese architecture. The development of compatible gypsum based materials is focused on the results of the samples from this period. MAIN OBJECTIVES: Characterization of the ancient Portuguese gypsum plasters. Development of compatible, ready mix, user-friendly, gypsum based restoration products, to be used even by unskilled workers, in order to improve the preservation of the Portuguese historical heritage. EXPERIMENTAL RESULTS: The characterization of old Portuguese gypsum plasters (18th to middle XX centuries), from different kinds of buildings and regions of the country, showed different compositions according to their function in the building and the application technique: smooth surface plasters are made of similar proportions of lime and gypsum, while precast decorations only binder is usually gypsum, sometimes with organic additions. The physical and mechanical characteristics also vary, in accordance with the lime-gypsum proportions and are affected by the organic additions, sometimes with hydrophobic behaviour. The determination of the physical properties in the samples of the old gypsum plasters collected is almost finished. Based in the results obtained it is possible to identify three classes of restoration products for Portuguese old gypsum based plasters, and to define, in a first approach, the respective compatibility ranges for some parameters. These ranges will, if necessary, be adjusted later, considering all the results obtained. The development and test of the restoration products in now in progress and will proceed until final formulations are achieved. IMAGES
Samples
Optical microscopy
SEM-EDS
ATG-DTA
Higroscopicity
CONTACTS: R. Anselmo Braancamp 198, 4000-078 Porto; tlm. 919003496, email: bfigueiredo.13@gmail.com
Figure 1. Result of a Maximum Likelihood Classification for the lacunae in a wall painting
Figure 2. Orthophotograph of a panel painting and the corresponding thematic map of lacunae, retouching areas and main colours.