To identify the difference between qualitative and
quantitative analysis; To differentiate and familiarize among gravimetric, volumetric and instrumental methods of analysis; To outline the steps involved in a typical quantitative analysis; Participate in class discussion; Appreciate the broad areas in which Analytical Chemistry is commonly involved. Objectives: What is Analytical Chemistry? Chemistry Analytical The science of the composition, structure, properties, and reactions of matter, especially of atomic and molecular systems. Of or relating to analysis or analytics. Dividing into elemental parts or basic principles Is the chemistry that is used in connection with the separation and analysis of chemical substances. What is Analytical Chemistry? Analytical Chemistry provides the methods and tools needed for insight into our material worldfor answering four basic questions about a material sample? What? Where? How much? What arrangement, structure or form? Science of Chemical Measurements Classification Chemical Analysis (Separation) Qualitative Analysis (Identification) What is present? Quantitative Analysis (Quantification) How much is present? A qualitative method yields information about the identity of atomic or molecular species or the functional groups in the sample. A quantitative method in contrast, provides numerical information as to the relative amount of one or more of these components. Nutritional Facts Label Analytical Chemistry Establishing economic value Diagnosing disease Relating properties to composition or structure Quality Control Conducting research Determining health hazards Areas in which Analytical Chemistry is commonly involved Analytical Methods Classical Gravimetric Volumetric Instrumental Spectroscopy Electro analytical method Category of Analytical Methods Methods of Analysis Method in which weight of substance is measured.
Methods of Analysis Refers to measurement of a volume.
Methods of Analysis Methods are based on measurement of some physical and chemical property, through the use of instruments.
Steps in Analysis: An analysis involves several steps and operations which depend on: the particular problem your expertise the apparatus or equipment available. The analyst should be involved in every step. Standards bodieshierarchy
Gary Christian, Analytical Chemistry, 6th Ed. (Wiley)
Different methods provide a range of precision, sensitivity, selectivity, and speed capabilities. Method in testing Chocolate: CODEX STAN 87-1981, Rev. 1 - 2003 Gary Christian, Analytical Chemistry, 6th Ed. (Wiley)
The sample size dictates what measurement techniques can be used. Calculate the result and report Laboratory safety is a must! Learn the rules.