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INTRODUO
MATERIAIS E MTODOS
3.2- Termogravimetria
RESULTADOS E DISCUSSO
3.1- FTIR
Nas figuras 1a e 1b so mostrados os espectros
tpicos obtidos por FTIR para os aditivos das sries A
e B.
T GA
%
CURVA TG - SV's
300.00
MIVCh1
1A
Ch1
MIVCh1
2A
MIVCh1
3A
Ch1
--------- MIV 4A
--- MIV 5A
200.00
110
12-05-2011
06-05-2011
16-05-2011
11-05-2011
09-05-2011
T GA-50
T GA-50
T GA-50
T GA-50
T GA-50
13-16
13-17
14-41
14-12
10-16
2011-05-12.tad
2011-05-06.tad
2011-05-16.tad
2011-05-11.tad
2011-05-09.tad
10
4000
3500
638.20
944.00
698.98
-100.00
3000
2500
2000
1000
TGA
%
300.00
(a)
644.24
1463.46
747.91
1066.31
1241.23
20
100.00
0.00
2854.28
2924.89
30
200.00
CURVA TG - Viscoplex's
Ch1
--------MIVVISCOPLEX
IB
Ch1 VISCOPLEX
--------MIV 2B
Ch1 VISCOPLEX
--------- MIV 3B
1377.71
1730.25
2956.33
40
1271.07
80
1151.14
90
60
600.00
500
70
400.00
T e mp [C]
(a)
1500
-1
Wavenumbers
(cm-1))
Nmero
de onda (cm
100
50
200.00
1493.04
0.00
2925.61
2952.26
30
20
756.60
1154.47
1376.90
3025.83
2857.65
50
40
0.00
1462.04
60
1454.41
3060.20
70
1028.70
1601.40
3373.52
3081.90
80
%%TT
100.00
90
%%TT
140
260
266
270
300
100
110
SV
SV
SV
SV
SV
-100.00
10
0
4000
3500
3000
2500
2000
Wavenumbers
Nmero
de onda(cm-1)
(cm-1)
1500
1000
500
(b)
Figura 1. Espectros tpicos obtidos por FTIR para os MIVs
(a) Srie A e (b) Srie B.
0.00
200.00
400.00
Temp [C]
600.00
(b)
Figura 2. Curvas TGs para os MIVs (a) Srie A e (b) Srie B.
Amostra
1A
2A
3A
4A
5A
1B
2B
3B
Tonset/C
254
280
215
261
274
192
215
172
ONL+2A
2
(mm /s)
ONL+5A
2
(mm /s)
ONM+2A
2
(mm /s
ONM+5A
2
(mm /s)
0,0%
30,27
30,27
52,58
52,58
0,5%
46,40
51,67
78,81
79,23
1,0%
79,75
91,66
125,80
132,10
2,0%
203,90
257,20
341,60
434,90
ONL+2A
2
(mm /s)
ONL+5A
2
(mm /s)
ONM+2A
2
(mm /s
ONM+5A
2
(mm /s)
0,0%
5,21
5,21
7,30
7,30
0,5%
7,75
8,71
10,63
9,46
1,0%
12,45
14,20
15,92
16,73
2,0%
28,65
35,47
38,85
48,51
ONL+2A
ONL+5A
ONM+2A
ONM+5A
0,0%
102
102
98
98
0,5%
136
147
120
95
1,0%
154
160
134
137
2,0%
180
187
164
172
CONCLUSES
AGRADECIMENTOS
REFERNCIAS