Escolar Documentos
Profissional Documentos
Cultura Documentos
INSTITUTO DE QUMICA
PS-GRADUAO
Bibliografia:
1) Fundamentals of Crystallography (IUCr Texts on
Crystallography, 2), G. Artioli, D. Viterbo, G. Ferraris, C.
Giacovazzo. C. Giocovazzo (ed.) Oxford University Press,
1992.
2) The Basics of Crystallography and Diffraction (IUCr Texts on
Crystallography, 5), C. Hammond, Oxford University Press,
2001.
3) Crystal Structure Determination. William Clegg, Oxford
Chemistry Primers, Oxford University Press, 1998.
DISCIPLINAS OFERECIDAS NO 1 SEMESTRE/2013
Bibliografia:
Sugestes para uma reviso dos conceitos bsicos:
R. T. Morrison / R. N. Boyd Organic Chemistry
N. L. Allinger e outros - Qumica Orgnica
Jerry March Advanced Organic Chemistry
T. W. G. Solomons e outros Organic Chemistry
A. Streitwieser e outros Introduction to Organic Chemistry
J. Clayden e outros Organic Chemistry
Para acompanhamento da disciplina:
F. A. Carey / R. J. Sundberg: Advanced Organic Chemistry
Ian Fleming: Frontier Orbitals and Organic Chemical Reactions
E. L. Eliel / S. H. Wilen: Stereochemistry of Organic Compounds
QP031 Qumica Quntica I Crditos: 04
Turma A
Pr-Req: QP124/QP125/AA200 (Autorizao da Coordenadoria de VAGAS:
Segunda: Ps-Graduao). mnimo: 03
14h s 16h mximo: 20
Prof. Rogrio Custodio
Quinta:
10h s 12h Ementa:
Mecnica ondulatria. Operadores e relaes de com incerteza.
Sala H103 (IQ08) Momento angular. Potenciais esfericamente simtricos. tomo
multieletrnico. lgebra matricial. Mtodos de aproximao. Spim.
Estrutura atmica. Mtodo SCF de Hartree-Fock.
Bibliografia:
1) A.K. Chandra, Introductory quantum chemistry, McGraw-Hill
Ed., (1989);
2) Atilla Szabo and Neil S. Ostlund, Modern Quantum Chemistry:
Introduction to Advanced Eletronic Estructure Theory, Dover
Ed.
Bibliografia:
1. J.E. Huheey, E.A. Keiter, R.L. Keiter "Inorganic Chemistry,
Principles of Structure and Reactivity", Harpes Collins College
Publishers, 4a Edio, 1993.
2. G. Herzberg, "Atomic spectra and atomic structure", Dover
publications, 1944.
3. F.A. Cotton, "Chemical Application of Group Theory", J. Willey &
Sons Inc.
4. S.F.A. Kettle, Symmetry and Structure Readable Group Theory for
Chemists, J. Willey & Sons, 2a Ed., 1995.
5. D.C. Harris, M.C. Bertolucci, Symmetry and Spectroscopy, na
Introduction to Vibrational and Electronic
Bibliografia:
1. L.R. SNYDER, J. J. KIRKLAND, Introduction to Modern Liquid
Chromatography, 2a ed., John Wiley & Sons,1979.
2. L.R. SNYDER, J. J. KIRKLAND, J. L. GLAJCH, Practical HPLC
Method Development, 2a ed., John Wiley & Sons,1997.
3. V.R. MEYER, Practical Performance Liquid Chromatography, 4a
ed., John Wiley & Sons, 2004.
4. CAROL H. COLLINS, GILBERTO L. BRAGA, PIERINA S. BONATO
(coordenadores), Fundamentos de Cromatografia, Editora da
Unicamp, Campinas, 2006.
5. A . WESTON, P. R. BROWN, HPLC and CE Principles and Practice,
_Academic Press.
6. C. F. POOLE, S. K. POOLE, Chromatography Today, 2a ed.,
Elsevier Science,1985.
7. D. A. SKOOG, F. J. HOLLER, T. A. NIEMAN, Principles of
Instrumental Analysis, 5a ed. Saunders College Publishing.
1. 8. F.R. de AQUINO NETO, D.S.S. NUNES, Cromatografia
Princpios Bsicos e Tcnicas Afins, Intercincia, Rio de Janeiro, RJ,
2003.
Bibliografia:
1. Vitz E. Redox Redux: Recommendation for improving textbook and
IUPAC definitions. Journal of Chemical Education, 2002, 79(3):397-
400.
2. Barnum DW. Potential-pH diagrams. Journal of Chemical Education,
1982, 59(10):809-812.
3. Skoog DA, West DM, Holler FJ, Crouch SR. Fundamentos de
Qumica Analtica. Trad. M.Grassi; So Paulo: Pioneira Thomson
Learning, 2006.
4. Stumm W, Morgan JJ. Aquatic chemistry. 3rd ed.; Wiley Interscience
Pub.; 1996.
5. Butler JN. Ionic equilibrium: solubility and pH calculations. Wiley
Interscience Pub.; 1998.
6. Butler, J.N., Ionic Equilibrium: A Mathematical Approach, Addison-
Wesley Publish Company, Menlo Park, 1964.
7. Miller, J.C. e Miller, J. N., * *Statistics for Analytical Chemistry, Ellis
Horwood, New York, Prentice Hall, 1993.
8. Harris, DC, Anlise Qumica Quantitativa. Rio de Janeiro: LTC
Livros Tcnicos e Cientficos Editora S.A., 2008.
9. Wnninen EV, Ingman F. Metal buffers in chemical-analysis .1.
Theoretical considerations. Pure and Applied Chemistry, 1987, 59(12):
1681-1692.
10. Hulanicki A, Ingman F, Wnninen EV. Metal buffers in chemical-
analysis .1. Practical considerations Pure and Applied Chemistry,
1991, 63(4): 639-642.
Bibliografia:
1.Enzimas em Biotecnologia, Produo, Aplicaes e
Mercado (Ed. Bon, E. P. S.; Ferrara, M.A.; Corvo, M. L.), Intercincia
Ltda., Rio de Janeiro, 2008.
2.Voet, D.; Voet, J. G.; Pratt, C. W. Fundamentos de
Bioqumica, Artmed, So Paulo, 2010.
3.Alberts, B. e colaboradores; Molecular Biology of the Cell,
4th Ed., Galante Science 2002. [ou mais recente]
4.Lewin, B. e colaboradores. Genes IX (ou mais recente)
Jones and Bartlett Publishers, 2008.
5.Biotechnology: A multi volume comprehensive treatise,
nd
Rehn, H.-J.; Reed, G.; Phler, A.; Stadler, P., Eds.; 2 Ed.; Wiley-
VHC.
6.Biotransformations in Organic Chemistry: A textbook,
th
Faber, K.; 4 Ed.; Springer-Verlag, Berlin, 2000.
7.Artigos Cientficos e Ferramentas da Web.
QP327 Interpretao e Atribuio de Espectro de RMN 1D e 2D Crditos: 04
Turma A
Prof. Dr. Cludio Francisco Tormena VAGAS:
Segunda e Quarta mnimo: 04
14h s 16h Ementa: mximo: 20
RMN de 1H, 13C e outros ncleos: deslocamento qumico,
Sala H102 (IQ07) constantes de acoplamento, efeitos isotpicos, espectros de RMN
2D homo- e hetero-nucleares, interpretao de espectros.
Programa da disciplina:
Bibliografia:
Ementa:
Propriedades termodinmicas e calorimtricas de lquidos inicos e
suas medidas experimentais; solvatao em lquidos inicos;
desenho e modelagem de lquidos inicos; espectroscopia
vibracional de lquidos inicos; aplicaes industriais.
Bibliografia:
Artigos recentes da literatura; revises recentes que sero
fornecidos em cada aula.
Ementa:
Elementos ticos de uma linha de SAXS: noes bsicas de reduo
dos dados; pr-anlises de dados de SAXS; introduo de conceitos
bsicos (Lei de Guinier e leis de potncia); modelagem de sistemas
multi-estruturados; modelagem de nanopartculas; modelagem bsica
de protenas em soluo.
Bibliografia:
1. Small-angle Scattering of X-Rays Guinier A., Fournet, G.,
(Willey), 1955.
2. Small-angle X-Ray Scattering Glatter O., Krak. O. (Academic
Press Inc), 1982.
3. X-Ray Scattering of Soft Matter Stribeck, N. (Springer), 2007.
4. Structure Analysis by Small-Angle X-Ray and Neutron
Scattering Feigin, L.A., Svergun D.I., (Springer), 1987.
Bibliografia:
NMR From Spectra to Structures An Experimental Approach,
Mitchell, Terence N., Costisella, Burkhard Springer; 2ndrev.and
exp.ed. edition (2007).
200 and More NMR experiments, A pratical Course, Stefan Berger
and Segmar Braun, Wiley-VCH, (1997)
High-Resolution NMR Techniques in Organic Chemistry, Timothy
D. W. Claridge, Volume 27, Second Edition Elsevier Science; 2 edition
(2008)
NMR Spectroscopy: Processing Strategies Second Updated
Edition Peter Bigler Wiley-VCH; 2 edition (2000).
NMR Crystallography, Robin K, Harris, Roderick E. Wasylishen,
Melinda J. Duer, Wiley, EMR, 2009.
NMR Spectroscopy in Pharmaceutical Analysis, Ulrike Holzgrabe.
Iwona Wawer, Bernd Diehl, Elsevier, (2008).
Solving Problems With NMR Spectroscopy, Atta-ur-Rahman,
Muhammad Choudhary Academic Press; 1 edition (1996)
Organic Structure Determination Using 2-D NMR Spectroscopy: A
Problem-Based Approach (Advanced Organic Chemistry), Jeffrey H.
Simpson Academic Press; 1 edition (2008).
Introduction to Spectroscopy: A Guide for Students of Organic
Chemistry, Donald L. Pavia, Gary M. Lampman, George S. Kriz
nd
Harcourt College Pub, 2 edition (1996).
Understanding NMR Spectroscopy, Wiley, Chichester, J. Keeler,
(2005).
Spin Dynamics: Basics of Nuclear Magnetic Resonance, Levitt,
M.H, (2002) Pharmaceutical Analysis, Lee, D.C.; Webb, M. Blackwell
(2003).
Ressonncia Magntica Nuclear Fundamentos, Mtodos e
Aplicaes. GIL, V.M.S. & GERALDES, C.F.G.C. Fundao Calouste
Gulbenkian. Lisboa (1987).
Two Dimensional NMR Spectroscopy, Applications for Chemists
nd
and Biochemists Croasmun, W.R.; Carlson, R. M., Editores, 2 .
(2003).
QP446 Crditos: 02
Turma B Tpicos Especiais em Qumica Inorgnica IV Redao de Textos
Cientficos Vagas:
Tera Mnimo: 05
16h s 18h Prof. Dr. Marco-Aurelio De Paoli Mximo: 20
Bibliografia:
- U. Eco, Comme si fa uma tesi de lurea, Bompiani, Milano,
1977.
- E. Schrdingerm
HTTP://www.lecb.ncifcrf.gov/~toms/quotes.html, 01/11/201.
- L. Rey, Planejar e redigir trabalhos cientficos. 2 Edio,
Editora Edgar Blcher, So Paulo, 2000.
- M. OConnor e F.P. Woodford, Writing scientific papers in
english, Elseveier, Amsterdam, 1977.
- T. Scpector, Writing a scientific manuscript, J. Chem. Educ. 71
(1994) 47.
- P. E. Bourne. Ten simple rules for getting publishe PLoS
Computational Biology: Editorial, published 27 Apr 2007
10.1371/jornal.pcbi.0030077.
- P.E. Bourne. Ten simple rules for making good oral
presentations. PLoS Computational Biology: Editorial, published
27 Apr 2007 10.1371/journal.pcbi.0030077
- P.E. Bourne , Ten simple rules for a good poster presentation.
PLoS Computational Biology: Editorial Maio, 2007.
- R. Breretoon, HTTP://suite101.com/article/autorship-orders--in-
scientific-papers-a256157#ixzz22UPNKxFd
Bibliografia:
1. Oficina do Empreendendor - A metodologia de ensino que ajuda a
transformar conhecimento em riqueza -Fernado Dolabela - Ed.
Sextante, 2008;
2. Empreendedorismo - Transformando Idias em Negcios - Jos
Carlos Assis Dornelas - Elsevier - 2. Ed., 2005;
3. Patenteamento & Prospeco Tecnolgica no Setor Farmacutico -
Adelaide Maria de Souza Antunes e Jorge Lima de Magalhes - Ed.
Intercincia, 1. Ed., 2008.
4. Habilidades Diretivas - Aprenda os Segredos do Markiting, E.
Davies & B. Davies, Ed. Planeta, 2005.
QP812 Tpicos Especiais em Qumica Analtica VIII Tcnicas Crditos: 02
Turma B Espectrofotometricas Aplicadas a Bio-anlise e Biomedicina
Ementa:
Absorption and Emission Spectroscopies as Analytical Tools in the
Design of Fluorescent Molecular Sensors.
Essentials in MALDI-TOF-spectrometry applied to Chemosensor.
Basic Concepts and applications
Photophysical Aspects of new Fluorescent Materials, Nanoparticles,
Probes and Sensors for metal detection
Anion recognition using Fluorescent and Colorimetric systems
Nobel Metal Nanoparticles as Protein Label and Free Label
Sensors: A case of Human Plasma Profiling for Medical
Diagnostics
Nanoparticle-toxicity to aquatic environments. From synthesis to
applications
Biomarker Discovery
Overview on modern approaches to speed up protein identification
workflows relying on enzymatic cleavage and mass spectrometry-
based techniques
Nano profiling
Decision Peptide Driven: A novel tool for protein quantification
Analytical proteomics: A challenge for the future
Daily life in a proteomics lab: The experimental design is the base
for successful experiments
Biological Mass Spectrometry from Classic Proteomics to Imaging
Mass Spectrometry
Bibliografia:
Artigos cientficos
Isiah M. Warner et al., Anal. Chem., 1996, 68, 73R-91R A.
Prasanna de Silva, et al., Chem. Rev., 1997, 97, 1515-1566
Knut Rurack, Spectrochimica Acta A, 57 2001, 2161-2195
Anthony W. Czarnik, Acc. Chem. Res., 1994, 27, 302-308
Alberto Credi , Luca Prodi, Spectrochimica Acta A., 1998, 54, 159-
170
Akeeta M. Powe et al., Anal. Chem., 2004, 76, 4614-4634
L. Basabe-Desmonts, et al., Chem. Soc. Rev., 2007, 36, 993-1017
Gianluca Accorsi et al., Chem. Soc. Rev., 2009, 38, 1690-1700
M. D. Allendorf et al., Chem. Soc. Rev., 2009, 38, 1330-1352
Vicenzo Balzani et al., Chem. Soc. Rev., 2009, 38, 1542-1550
Carlos Lodeiro et al., Chem. Soc. Rev., 2010, 39, 2733-3336
JL. Capelo et al., Talanta, 2010, 1476-1486
JL. Capelo et al., Anal. Chim. Acta, 650, 2009, 151-159
C. Lodeiro et al., Coord. Chem. Rev., 253, 2009, 1353-1383
D. Lopez Ferrer et al., Trends in Anal Chem., 25, 10, 2006, 996-
1005
Livros
B. Valeur, JC. Brochon (Eds) New Trends in Fluorescence
Spectroscopy, Applications to Chemical and Life Sciences,
Springer, 2001
D. Fitzpatrick, H. J. Ulrich, Editors, Macrocyclic Chemistry, New
Research Developments, Chemistry Research and Applications,
Nova Publishers, 2010
J. L. Capelo Editor, Ultrasound in Chemistry. Analytical
Applications, Wiley VCH, 2009
Somenath Mitra Editor, Sample Preparation Techniques in
Analytical Chemistry, Wiley Interscience, 2003
Franz Hillenkamp and Jasna Peter-Katalinic, MALDI MS. A
Practical Guide to Instrumentaions, Methods and Applications,
Wiley-VCH, 2007